Crystal structure and solid-state31P CP-MAS NMR spectrum of the bis(trifluoroacetato) (triphenylphosphine)mercury(II) dimer [Hg(CF3CO2)2PPh3]2

1990 ◽  
Vol 20 (2) ◽  
pp. 149-155 ◽  
Author(s):  
Tim Allman ◽  
Francine B�langer-Gari�py ◽  
Andr� L. Beauchamp
Keyword(s):  
Crystal Structure ◽  
Mas Nmr ◽  
Nmr Spectrum ◽  
Cp Mas Nmr

Crystal structure and13C CP/MAS NMR of thep-xylene clathrate of Dianin's compound

1999 ◽  
Vol 97 (11) ◽  
pp. 1193-1196 ◽  
Author(s):  
G. D. ENRIGHT ◽  
C. I. RATCLIFFE ◽  
J. A. RIPMEESTER
Keyword(s):  
Crystal Structure ◽  
Mas Nmr ◽  
Cp Mas Nmr ◽  
Dianin's Compound

scholarly journals Synthesis, structure and characterization of a new noncentrosymmetric Zn(II) complex with the 2-amino-5-chloropyridine ligand (AClPy)

2014 ◽  
Vol 10 (9) ◽  
pp. 3116-3126 ◽  
Author(s):  
Wijdene Nbili ◽  
Kamel Kaabi ◽  
Valeria Ferretti ◽  
Frederic Lefebvre ◽  
Cherif Ben Nasr
Keyword(s):  
Crystal Structure ◽  
Hydrogen Bonds ◽  
Theoretical Calculations ◽  
Mas Nmr ◽  
Coordination Pattern ◽  
X Ray Diffraction ◽  
Absorption Bands ◽  
Cp Mas Nmr ◽  
13C Cp Mas Nmr

A new noncentrosymmetric Zn(II) complex with the monodentate ligand 2-amino-5-chloropyridine (AClPy), ZnCl2(C5H5ClN2)2, has been prepared at room temperature and characterized by single crystal X-ray diffraction, 13C CP-MAS-NMR and IR spectroscopies. The basic coordination pattern of the AClPy coordinated metal cations is slighly distorted tetrahedral. The crystal structure is characterized by ZnCl2N2 tetrahedra interconnected via N-H···Cl hydrogen bonds generated by the NH2 amino group to form chains extending along the (a-c) direction. The exocyclic N atom is an electron receiving center, which is consistent with features of imino resonance as evidenced by bond lengths and angles. The crystal structure is stabilized by sets of intra and intermolecular hydrogen bonds. The 13C CP-MAS NMR spectrum is discussed and the vibrational absorption bands are identified by infrared spectroscopy and theoretical calculations.

Crystal structure and 13C CP/MAS NMR of the p-xylene clathrate of Dianin's compound

1999 ◽  
Vol 97 (11) ◽  
pp. 1193-1196 ◽  
Author(s):  
G. D. Enright, C. I. Ratcliffe, J. A.
Keyword(s):  
Crystal Structure ◽  
Mas Nmr ◽  
Cp Mas Nmr ◽  
Dianin's Compound ◽  
13C Cp Mas Nmr

Crystal Structure, Infrared and Solid State CP MAS NMR Characterization of [(PPh3)2AgO2CH] and of [(PPh3)2AgO2CH].cntdot.2HCO2H, a Complex of the H-Bonded [H2(HCO2)3]- Species

1995 ◽  
Vol 99 (12) ◽  
pp. 3909-3917 ◽  
Author(s):  
Graham A. Bowmaker ◽  
Effendy ◽  
John V. Hanna ◽  
Peter C. Healy ◽  
Graeme J. Millar ◽  
...  
Keyword(s):  
Crystal Structure ◽  
Solid State ◽  
Mas Nmr ◽  
Nmr Characterization ◽  
Cp Mas Nmr

Effect of water in the carbon-13 CP/MAS NMR spectrum of white spruce wood

1987 ◽  
Vol 20 (7) ◽  
pp. 1554-1556 ◽  
Author(s):  
J. M. Willis ◽  
F. G. Herring
Keyword(s):  
White Spruce ◽  
Mas Nmr ◽  
Nmr Spectrum ◽  
Effect Of Water ◽  
Spruce Wood ◽  
Cp Mas Nmr
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