Two‐dimensional nuclear magnetic resonance in rotating solids: An analysis of line shapes in chemical shift‐dipolar spectra

1982 ◽  
Vol 76 (6) ◽  
pp. 2848-2858 ◽  
Author(s):  
Michael G. Munowitz ◽  
Robert G. Griffin
Keyword(s):  
Nuclear Magnetic Resonance ◽  
Magnetic Resonance ◽  
Chemical Shift ◽  
Two Dimensional ◽  
Line Shapes ◽  
Nuclear Magnetic

An improved route to pregna-5,20-dien-3β-ol (muricin aglycone): Carbon and proton nuclear magnetic resonance assignments for the aglycone and a number of related pregnene derivatives

1987 ◽  
Vol 65 (3) ◽  
pp. 666-669 ◽  
Author(s):  
R. D. Dawe ◽  
J. L. C. Wright
Keyword(s):  
Nuclear Magnetic Resonance ◽  
Magnetic Resonance ◽  
Chemical Shift ◽  
Resonance Assignments ◽  
Proton Nuclear Magnetic Resonance ◽  
Two Dimensional ◽  
Chemical Shift Correlation ◽  
Heteronuclear Chemical Shift ◽  
Nuclear Magnetic

Carbon and proton assignments for muricin aglycone (5) and a number of related pregnenes, carried out with the aid of two-dimensional homo- and heteronuclear chemical shift correlation experiments, have resulted in previously reported carbon assignments for the aglycone being revised. An improved route to muricin aglycone is also reported.

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