VAPOR‐LIQUID‐SOLID MECHANISM OF SINGLE CRYSTAL GROWTH

1964 ◽  
Vol 4 (5) ◽  
pp. 89-90 ◽  
Author(s):  
R. S. Wagner ◽  
W. C. Ellis
Keyword(s):  
Crystal Growth ◽  
Single Crystal ◽  
Single Crystal Growth ◽  
Vapor Liquid Solid ◽  
Vapor Liquid Solid Mechanism ◽  
Vapor Liquid

Growth and Raman Spectroscopy of Single Crystal ZnGeN2 Rods Grown from a Molten Zn/Ge Alloy

2007 ◽  
Vol 1040 ◽  
Author(s):  
Timothy J. Peshek ◽  
Shanling Wang ◽  
John C. Angus ◽  
Kathleen Kash
Keyword(s):  
Raman Spectroscopy ◽  
Raman Spectrum ◽  
Single Crystal ◽  
Excellent Agreement ◽  
Spectral Features ◽  
Vapor Liquid Solid ◽  
Present Evidence ◽  
Vapor Liquid Solid Mechanism ◽  
Theoretical Predictions ◽  
Vapor Liquid

AbstractWe present evidence for the growth of ZnGeN2 from a molten Zn/Ge alloy via the vapor-liquid-solid mechanism. Hexagonally faceted, 3-4 microns wide by 20-40 microns long, single crystal rods of ZnGeN2 capped by a polycrystalline dome of ZnGeN2 were formed. A micro-Raman spectrum shows several individually resolved peaks and no spectral features above 825 cm−1, in contrast to a previously published spectrum for polycrystalline ZnGeN2, but in excellent agreement with recent theoretical predictions.

Unsteady 3D and analytical analysis of segregation process in floating zone silicon single crystal growth

2009 ◽  
Vol 45 (4) ◽  
pp. 549-556 ◽  
Author(s):  
K. Lācis ◽  
◽  
A. Muižnieks ◽  
N. Jēkabsons ◽  
A. Rudevičs ◽  
...  
Keyword(s):  
Crystal Growth ◽  
Single Crystal ◽  
Single Crystal Growth ◽  
Silicon Single Crystal ◽  
Floating Zone ◽  
Analytical Analysis ◽  
Segregation Process

scholarly journals Epitaxial Single‐Crystal Growth of Transition Metal Dichalcogenide Monolayers via the Atomic Sawtooth Au Surface

2021 ◽  
pp. 2006601
Author(s):  
Soo Ho Choi ◽  
Hyung‐Jin Kim ◽  
Bumsub Song ◽  
Yong In Kim ◽  
Gyeongtak Han ◽  
...  
Keyword(s):  
Crystal Growth ◽  
Transition Metal ◽  
Single Crystal ◽  
Single Crystal Growth ◽  
Transition Metal Dichalcogenide

Exploring SiC Growth Limitation of Vapor-Liquid-Solid Mechanism when Using Two Different Carbon Precursors

2013 ◽  
Vol 740-742 ◽  
pp. 323-326
Author(s):  
Kassem Alassaad ◽  
François Cauwet ◽  
Davy Carole ◽  
Véronique Soulière ◽  
Gabriel Ferro
Keyword(s):  
Growth Rate ◽  
High Growth ◽  
High Growth Rate ◽  
Carbon Precursor ◽  
Growth Limitation ◽  
Vapor Liquid Solid ◽  
Partial Pressures ◽  
Vapor Liquid Solid Mechanism ◽  
Vls Growth ◽  
Vapor Liquid

Abstract. In this paper, conditions for obtaining high growth rate during epitaxial growth of SiC by vapor-liquid-solid mechanism are investigated. The alloys studied were Ge-Si, Al-Si and Al-Ge-Si with various compositions. Temperature was varied between 1100 and 1300°C and the carbon precursor was either propane or methane. The variation of layers thickness was studied at low and high precursor partial pressure. It was found that growth rates obtained with both methane and propane are rather similar at low precursor partial pressures. However, when using Ge based melts, the use of high propane flux leads to the formation of a SiC crust on top of the liquid, which limits the growth by VLS. But when methane is used, even at extremely high flux (up to 100 sccm), no crust could be detected on top of the liquid while the deposit thickness was still rather small (between 1.12 μm and 1.30 μm). When using Al-Si alloys, no crust was also observed under 100 sccm methane but the thickness was as high as 11.5 µm after 30 min growth. It is proposed that the upper limitation of VLS growth rate depends mainly on C solubility of the liquid phase.

scholarly journals Single Crystal Growth and Physical Properties of Pyroxene CoGeO3

Crystals ◽  
2021 ◽  
Vol 11 (4) ◽  
pp. 378
Author(s):  
Li Zhao ◽  
Zhiwei Hu ◽  
Hanjie Guo ◽  
Christoph Geibel ◽  
Hong-Ji Lin ◽  
...  
Keyword(s):  
High Pressure ◽  
Magnetic Properties ◽  
Magnetic Susceptibility ◽  
Crystal Growth ◽  
Physical Properties ◽  
Single Crystal ◽  
Single Crystals ◽  
Magnetic Moments ◽  
Single Crystal Growth ◽  
The Impact

We report on the synthesis and physical properties of cm-sized CoGeO3 single crystals grown in a high pressure mirror furnace at pressures of 80 bar. Direction dependent magnetic susceptibility measurements on our single crystals reveal highly anisotropic magnetic properties that we attribute to the impact of strong single ion anisotropy appearing in this system with TN∼33.5 K. Furthermore, we observe effective magnetic moments that are exceeding the spin only values of the Co ions, which reveals the presence of sizable orbital moments in CoGeO3.

scholarly journals Single-Crystal Growth of Sr2RuO4 by the Floating-Zone Method Using an Infrared Image Furnace with Improved Halogen Lamps

Crystals ◽  
2021 ◽  
Vol 11 (4) ◽  
pp. 392
Author(s):  
Naoki Kikugawa ◽  
Dmitry A. Sokolov ◽  
Tohru Nagasawa ◽  
Andrew P. Mackenzie
Keyword(s):  
Crystal Growth ◽  
Single Crystal ◽  
Infrared Image ◽  
Single Crystal Growth ◽  
Molten Zone ◽  
Floating Zone ◽  
Unconventional Superconductor ◽  
Zone Method ◽  
Floating Zone Method ◽  
Halogen Lamps

We report the single-crystal growth of the unconventional superconductor Sr2RuO4, on which research has reached a turning point recently. In order to optimize the quality of crystals grown by the floating-zone method using an infrared image furnace, we focus on an improvement of the structure of the filament in the halogen lamps. By reducing the thickness of the total filament, the form of the molten zone was narrowed. More importantly, the molten zone was observed to be more stable during the growth process. Finally, we obtained the crystals with a length of 12 cm. Additionally, the grown crystal has high quality, displaying the 1.5 K transition temperature expected only for the purest crystals. We also discuss the availability of the newly developed halogen lamps.

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