A Graphical Method for Selecting Suitable Radiations for the Precision Determination of Noncubic Lattice Constants and for Indexing Back‐Reflection Lines in Powder X‐Ray Photograms

1940 ◽  
Vol 11 (12) ◽  
pp. 800-805 ◽  
Author(s):  
Louis A. Carapella
1967 ◽  
Vol 22 (1) ◽  
pp. 92-95 ◽  
Author(s):  
W. Witt

An absolute precision determination of lattice constants by electron diffraction is made with thin monocrystalline films of germanium and aluminium, having a thickness between 1000 and 5000 A. The films are prepared from the bulk material by mechanical polishing and subsequent chemical polishing or etching. The obtained values for the lattice constant α of both materials are within the accuracy Δα/α= ±3·10-5 of measurement in full agreement with the corresponding values obtained by X-ray diffraction (Smakula and Kalnajs).


1979 ◽  
Vol 34 (8) ◽  
pp. 1165-1166 ◽  
Author(s):  
Gunter Steinberg ◽  
Hans-Uwe Schuster

The X-ray structure determination of YLiSn showed that Li and Sn form a weakly distorted Wurtzit-type lattice, whose octahedral lacunas are occupied by Y. The lattice constants of the hoxagonally crystallizing compound are a = 929.6 pm and c = 734.6 pm, space group P 63mc, Z = 8


1961 ◽  
Vol 5 ◽  
pp. 355-369
Author(s):  
A. Taylor ◽  
Brenda J. Kagle ◽  
E. W. Beiter

AbstractA simple and accurate graphical method is described for converting the composition of ternary alloys from weight per cent to atomic per cent, and vice versa. By making certain simplifying assumptions, the principles of the method are extended to the approximate determination of ternary alloy compositions from the count fractions obtained from fluorescence X-ray spectra. An example is given for the not-so-favorable system bismuth-germanium-tellurium. On account of the simpler excitation conditions, the same procedures may also be applied to X-ray microprobe analysis.


1975 ◽  
Vol 19 ◽  
pp. 725-734 ◽  
Author(s):  
R. P. Goehner

Computer simulation of back reflection Laue patterns now provides the means to plot Laue patterns for any crystal system in any orientation. This capability makes it possible to determine, rapidly and accurately, the orientation of single crystals and large grains in polycrystalline materials even in cases where little or no symmetry is displayed in the Laue photograph. A set of standard Laue patterns is first simulated to cover the stereographic triangle of the crystal being studied. The Laue photograph obtained from the crystal, or grain, is compared with the set of simulated Laue patterns. The pattern most similar to the photograph is used to determine the (HKL) values of three Laue spots. The (HKL) values of these spots and half their angular separations from the x-ray beam, along with the lattice constants, are used by a computer program to calculate the (HKL) value of the crystallographic plane perpendicular to the x-ray beam. A simulated Laue pattern can now be obtained in exactly the same orientation and it can be drawn directly to the scale of the Laue photograph. Thus the validity of the orientation can be easily verified by direct comparison. The (HKL) value of the crystallographic plane perpendicular to the x-ray beam can also be used to plot a stereographic projection of the crystal poles. Therefore, the complete orientation of the crystal can be determined.


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