High-energy (e, 2e) spectrometer for the study of the spectral momentum density of materials

2000 ◽  
Vol 71 (10) ◽  
pp. 3831 ◽  
Author(s):  
M. Vos ◽  
G. P. Cornish ◽  
E. Weigold
Keyword(s):  
High Energy ◽  
Momentum Density

High-Energy Inelastic-Scattering Beamline for Electron Momentum Density Study

1998 ◽  
Vol 5 (3) ◽  
pp. 208-214 ◽  
Author(s):  
Y. Sakurai
Keyword(s):  
High Resolution ◽  
Inelastic Scattering ◽  
Compton Scattering ◽  
High Energy ◽  
Momentum Density ◽  
High Resolution Spectroscopy ◽  
X Rays ◽  
Circularly Polarized ◽  
Magnetic Structures ◽  
Momentum Resolution

The advent of synchrotron radiation sources for well polarized and high-energy X-rays offers new opportunities for exploiting Compton scattering spectroscopy as a tool for investigating the electronic and magnetic structures of materials. Recent high-resolution Compton scattering experiments show the unique capability for the study of Fermiology-related issues and electron–electron correlation effects. Intense, high-energy and circularly polarized X-ray sources have improved magnetic Compton scattering spectroscopy from the point of statistical accuracy and momentum resolution. As a next advance, a high-energy inelastic scattering beamline dedicated to Compton scattering spectroscopies is being constructed at SPring-8. The light source is an elliptic multipole wiggler with a periodic length of 12 cm. The beamline includes two experimental stations: one is for high-resolution spectroscopy using 100–150 keV X-rays and the other is for magnetic Compton scattering experiments using circularly polarized 300 keV X-rays. The use of such high-energy X-rays makes it possible to carry out experiments efficiently on samples including heavier elements, such as high-T c superconductors and 4f and 5f magnetic materials.

Gamma-Ray Compton Spectroscopy for Determination of Electron Momentum Distributions in Iron

2013 ◽  
Vol 815 ◽  
pp. 8-12
Author(s):  
Samir Ahmed Hamouda
Keyword(s):  
Gamma Ray ◽  
Polycrystalline Sample ◽  
High Energy ◽  
Momentum Density ◽  
Profile Measurement ◽  
Compton Profile ◽  
Γ Radiation ◽  
Theoretical Predictions ◽  
Spectrometer Calibration

Compton profile measurement of iron polycrystalline sample has been performed with 662 keV γ-radiation from a caesium-137 source. The spectrometer calibration and data corrections for the high energy experiment are discussed. The data are compared with the augmented-plane-wave (APW) and linear combination of atomic orbitals (LCAO) band theoretical Compton profiles of iron. Both theoretical predictions show the band theories overestimate the momentum density at low momenta and underestimate it at intermediate momenta.

Electron Momentum Density of Hexagonal Magnesium Studied by Compton Scattering

2006 ◽  
Vol 112 ◽  
pp. 123-132 ◽  
Author(s):  
Marek Brancewicz ◽  
Henryk Reniewicz ◽  
Andrzej Andrejczuk ◽  
Ludwik Dobrzyński ◽  
Eugeniusz Żukowski ◽  
...  
Keyword(s):  
High Energy ◽  
Momentum Density ◽  
Directional Effect ◽  
Electron Momentum ◽  
Electron Momentum Density ◽  
Cubic Metals ◽  
Medium Resolution ◽  
Small Anisotropy ◽  
Directional Difference ◽  
Good Agreement

Directional Compton profiles of single crystal of hcp magnesium have been measured with scattering vectors along the [10 10], [1120] and [0001] directions in reciprocal space (special directions ΓΜ, ΓΚ, ΓΑ) using high-energy (662 keV) gamma radiation from a 137Cs isotope source. The experimental data were compared with corresponding theoretical Korringa-Kohn-Rostoker (KKR) calculations. The directional difference profiles, both experimental (of medium resolution) and theoretical ones, show very small anisotropy of the electron momentum density in magnesium, 2-3 times lower than in zinc and cadmium single crystals, significantly lower than observed in cubic metals. This small directional effect is in good agreement with Compton 60-keV energy experiments and positron annihilation data presented by other authors.

The Spectral Momentum Density of Aluminium, Copper and Gold Measured by Electron Momentum Spectroscopy

2001 ◽  
Vol 215 (10) ◽  
Author(s):  
A. S. Kheifets ◽  
M. Vos ◽  
E. Weigold
Keyword(s):  
Electron Correlation ◽  
High Energy ◽  
Momentum Density ◽  
Correlation Effects ◽  
Many Body ◽  
Electron Momentum ◽  
Aluminium Copper ◽  
Electron Momentum Spectroscopy ◽  
Electron Correlation Effects ◽  
Good Agreement

Electron momentum spectroscopy (EMS) gives direct information of the full energy-resolved electron momentum densities of occupied states (bands) in solids – single crystal, polycrystalline or amorphous. Here we present data from a new high energy EMS spectrometer using 50 keV incident and 25 keV outgoing electrons, on polycrystalline specimens of aluminium, copper and gold. The spectral momentum densities show very significant electron-electron correlation effects which are in good agreement with many-body Green´s function calculations.

The E-ring: interactions with plasma and implications for its evolution

1984 ◽  
Vol 75 ◽  
pp. 599-602
Author(s):  
T.V. Johnson ◽  
G.E. Morfill ◽  
E. Grun
Keyword(s):  
Time Scale ◽  
Particle Density ◽  
High Energy ◽  
Particle Removal ◽  
Density Region ◽  
Drag Forces ◽  
Orbit Evolution ◽  
History Of ◽  
Ring Particle ◽  
Ring Material

A number of lines of evidence suggest that the particles making up the E-ring are small, on the order of a few microns or less in size (Terrile and Tokunaga, 1980, BAAS; Pang et al., 1982 Saturn meeting; Tucson, AZ). This suggests that a variety of electromagnetic and plasma affects may be important in considering the history of such particles. We have shown (Morfill et al., 1982, J. Geophys. Res., in press) that plasma drags forces from the corotating plasma will rapidly evolve E-ring particle orbits to increasing distance from Saturn until a point is reached where radiation drag forces acting to decrease orbital radius balance this outward acceleration. This occurs at approximately Rhea's orbit, although the exact value is subject to many uncertainties. The time scale for plasma drag to move particles from Enceladus' orbit to the outer E-ring is ~104yr. A variety of effects also act to remove particles, primarily sputtering by both high energy charged particles (Cheng et al., 1982, J. Geophys. Res., in press) and corotating plasma (Morfill et al., 1982). The time scale for sputtering away one micron particles is also short, 102 - 10 yrs. Thus the detailed particle density profile in the E-ring is set by a competition between orbit evolution and particle removal. The high density region near Enceladus' orbit may result from the sputtering yeild of corotating ions being less than unity at this radius (e.g. Eviatar et al., 1982, Saturn meeting). In any case, an active source of E-ring material is required if the feature is not very ephemeral - Enceladus itself, with its geologically recent surface, appears still to be the best candidate for the ultimate source of E-ring material.

Analysis of electron-diffraction intensity profiles using a photodiode-array detection system

1983 ◽  
Vol 41 ◽  
pp. 322-323
Author(s):  
J. B. Warren
Keyword(s):  
Electron Diffraction ◽  
Diffraction Pattern ◽  
Detection System ◽  
High Energy ◽  
Photographic Emulsion ◽  
Diffraction Intensity ◽  
Silicon Photodiode ◽  
Photodiode Array Detection ◽  
Analog To Digital ◽  
Photodiode Array

Electron diffraction intensity profiles have been used extensively in studies of polycrystalline and amorphous thin films. In previous work, diffraction intensity profiles were quantitized either by mechanically scanning the photographic emulsion with a densitometer or by using deflection coils to scan the diffraction pattern over a stationary detector. Such methods tend to be slow, and the intensities must still be converted from analog to digital form for quantitative analysis. The Instrumentation Division at Brookhaven has designed and constructed a electron diffractometer, based on a silicon photodiode array, that overcomes these disadvantages. The instrument is compact (Fig. 1), can be used with any unmodified electron microscope, and acquires the data in a form immediately accessible by microcomputer.Major components include a RETICON 1024 element photodiode array for the de tector, an Analog Devices MAS-1202 analog digital converter and a Digital Equipment LSI 11/2 microcomputer. The photodiode array cannot detect high energy electrons without damage so an f/1.4 lens is used to focus the phosphor screen image of the diffraction pattern on to the photodiode array.

Observation of Superlattice Dislocations on Cube Planes in Ni3Al

1973 ◽  
Vol 31 ◽  
pp. 174-175 ◽  
Author(s):  
J. M. Oblak ◽  
W. H. Rand
Keyword(s):  
Nearest Neighbor ◽  
Antiphase Boundary ◽  
Nearest Neighbors ◽  
High Energy ◽  
Cross Slip ◽  
Octahedral Plane ◽  
Trapping Mechanism ◽  
Slip Traces

The energy of an a/2 <110> shear antiphase. boundary in the Ll2 expected to be at a minimum on {100} cube planes because here strue ture is there is no violation of nearest-neighbor order. The latter however does involve the disruption of second nearest neighbors. It has been suggested that cross slip of paired a/2 <110> dislocations from octahedral onto cube planes is an important dislocation trapping mechanism in Ni3Al; furthermore, slip traces consistent with cube slip are observed above 920°K.Due to the high energy of the {111} antiphase boundary (> 200 mJ/m2), paired a/2 <110> dislocations are tightly constricted on the octahedral plane and cannot be individually resolved.

Microfabrication research at the National Submicron Facility

1983 ◽  
Vol 41 ◽  
pp. 86-89
Author(s):  
E.D. Wolf
Keyword(s):  
Integrated Circuits ◽  
Particle Physics ◽  
High Speed ◽  
New Technology ◽  
High Energy ◽  
High Energy Particle ◽  
New Science ◽  
Wide Range ◽  
Intermediate Domain ◽  
Circuit Function

Most microelectronics devices and circuits operate faster, consume less power, execute more functions and cost less per circuit function when the feature-sizes internal to the devices and circuits are made smaller. This is part of the stimulus for the Very High-Speed Integrated Circuits (VHSIC) program. There is also a need for smaller, more sensitive sensors in a wide range of disciplines that includes electrochemistry, neurophysiology and ultra-high pressure solid state research. There is often fundamental new science (and sometimes new technology) to be revealed (and used) when a basic parameter such as size is extended to new dimensions, as is evident at the two extremes of smallness and largeness, high energy particle physics and cosmology, respectively. However, there is also a very important intermediate domain of size that spans from the diameter of a small cluster of atoms up to near one micrometer which may also have just as profound effects on society as “big” physics.

Void-Lattice Formation in Natural Fluorite by Electron Irradiation

1976 ◽  
Vol 34 ◽  
pp. 614-615 ◽  
Author(s):  
L.E. Murr
Keyword(s):  
Electron Microscope ◽  
Electron Irradiation ◽  
Heavy Ion ◽  
High Energy ◽  
Stoichiometric Ratio ◽  
Direct Observations ◽  
Transmission Electron ◽  
Anion Vacancies ◽  
Cation And Anion Vacancies ◽  
Lattice Formation

The production of void lattices in metals as a result of displacement damage associated with high energy and heavy ion bombardment is now well documented. More recently, Murr has shown that a void lattice can be developed in natural (colored) fluorites observed in the transmission electron microscope. These were the first observations of a void lattice in an irradiated nonmetal, and the first, direct observations of color-center aggregates. Clinard, et al. have also recently observed a void lattice (described as a high density of aligned "pores") in neutron irradiated Al2O3 and Y2O3. In this latter work, itwas pointed out that in order that a cavity be formed,a near-stoichiometric ratio of cation and anion vacancies must aggregate. It was reasoned that two other alternatives to explain the pores were cation metal colloids and highpressure anion gas bubbles.Evans has proposed that void lattices result from the presence of a pre-existing impurity lattice, and predicted that the formation of a void lattice should restrict swelling in irradiated materials because it represents a state of saturation.

High energy resolution spectrometer for the dedicated STEM

1984 ◽  
Vol 42 ◽  
pp. 558-559 ◽  
Author(s):  
P.E. Batson
Keyword(s):  
Collection Efficiency ◽  
Core Loss ◽  
Beam Current ◽  
High Energy ◽  
High Energy Resolution ◽  
Acquisition Time ◽  
Good Definition ◽  
Loss Analysis ◽  
Definition Of ◽  
Acceleration Voltage

Use of the STEM to obtain precise electronic information has been hampered by the lack of energy loss analysis capable of a resolution and accuracy comparable to the 0.3eV energy width of the Field Emission Source. Recent work by Park, et. al. and earlier by Crewe, et. al. have promised magnetic sector devices that are capable of about 0.75eV resolution at collection angles (about 15mR) which are great enough to allow efficient use of the STEM probe current. These devices are also capable of 0.3eV resolution at smaller collection angles (4-5mR). The problem that arises, however, lies in the fact that, even with the collection efficiency approaching 1.0, several minutes of collection time are necessary for a good definition of a typical core loss or electronic transition. This is a result of the relatively small total beam current (1-10nA) that is available in the dedicated STEM. During this acquisition time, the STEM acceleration voltage may fluctuate by as much as 0.5-1.0V.

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