In situ monitoring of Raman scattering and photoluminescence from silicon surfaces in HF aqueous solutions

1998 ◽  
Vol 72 (8) ◽  
pp. 933-935 ◽  
Author(s):  
B. Ren ◽  
F. M. Liu ◽  
J. Xie ◽  
B. W. Mao ◽  
Y. B. Zu ◽  
...  
Keyword(s):  
Raman Scattering ◽  
Aqueous Solutions ◽  
In Situ Monitoring ◽  
Silicon Surfaces

Bifunctional Au@Pt core–shell nanostructures for in situ monitoring of catalytic reactions by surface-enhanced Raman scattering spectroscopy

Nanoscale ◽  
2014 ◽  
Vol 6 (15) ◽  
pp. 9063-9070 ◽  
Author(s):  
Zhi Yong Bao ◽  
Dang Yuan Lei ◽  
Ruibin Jiang ◽  
Xin Liu ◽  
Jiyan Dai ◽  
...  
Keyword(s):  
Raman Scattering ◽  
Surface Enhanced Raman Scattering ◽  
In Situ Monitoring ◽  
Core Shell ◽  
Raman Scattering Spectroscopy ◽  
Shell Nanostructures ◽  
Surface Enhanced ◽  
Surface Enhanced Raman ◽  
Enhanced Raman Scattering

Surface-enhanced Raman scattering spectroscopy using bifunctional Au@Pt core–shell nanostructures can monitor the catalytic reaction dynamics in real time.

scholarly journals Network of Palladium-Based Nanorings Synthesized by Liquid-Phase Reduction Using DMSO-H2O: In Situ Monitoring of Structure Formation and Drying Deformation by ASEM

2020 ◽  
Vol 21 (9) ◽  
pp. 3271 ◽  
Author(s):  
Takuki Komenami ◽  
Akihiro Yoshimura ◽  
Yasunari Matsuno ◽  
Mari Sato ◽  
Chikara Sato
Keyword(s):  
Surface Tension ◽  
Liquid Phase ◽  
Aqueous Solutions ◽  
Critical Point ◽  
Synthesis Method ◽  
Three Dimensional ◽  
In Situ Monitoring ◽  
Critical Point Drying ◽  
Micrometer Size

We developed a liquid-phase synthesis method for Pd-based nanostructure, in which Pd dissolved in dimethyl sulfoxide (DMSO) solutions was precipitated using acid aqueous solution. In the development of the method, in situ monitoring using atmospheric scanning electron microscopy (ASEM) revealed that three-dimensional (3D) Pd-based nanonetworks were deformed to micrometer-size particles possibly by the surface tension of the solutions during the drying process. To avoid surface tension, critical point drying was employed to dry the Pd-based precipitates. By combining ASEM monitoring with critical point drying, the synthesis parameters were optimized, resulting in the formation of lacelike delicate nanonetworks using citric acid aqueous solutions. Precipitation using HCl acid aqueous solutions allowed formation of 500-nm diameter nanorings connected by nanowires. The 3D nanostructure formation was controllable and modifiable into various shapes using different concentrations of the Pd and Cl ions as the parameters.

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