Transport measurements at low temperatures in a diamond anvil cell with helium as pressure medium

1997 ◽  
Vol 68 (3) ◽  
pp. 1514-1517 ◽  
Author(s):  
J. Thomasson ◽  
Y. Dumont ◽  
J.-C. Griveau ◽  
C. Ayache
2008 ◽  
Vol 28 (4) ◽  
pp. 627-631 ◽  
Author(s):  
Marius Millot ◽  
Sylvie George ◽  
Jean-Marc Broto ◽  
Bernard Couzinet ◽  
Jean-Claude Chervin ◽  
...  

Crystals ◽  
2018 ◽  
Vol 8 (7) ◽  
pp. 289 ◽  
Author(s):  
Barbara Lavina ◽  
Robert Downs ◽  
Stanislav Sinogeikin

We conducted an in situ crystal structure analysis of ferroselite at non-ambient conditions. The aim is to provide a solid ground to further the understanding of the properties of this material in a broad range of conditions. Ferroselite, marcasite-type FeSe2, was studied under high pressures up to 46 GPa and low temperatures, down to 50 K using single-crystal microdiffraction techniques. High pressures and low temperatures were generated using a diamond anvil cell and a cryostat respectively. We found no evidences of structural instability in the explored P-T space. The deformation of the orthorhombic lattice is slightly anisotropic. As expected, the compressibility of the Se-Se dumbbell, the longer bond in the structure, is larger than that of the Fe-Se bonds. There are two octahedral Fe-Se bonds, the short bond, with multiplicity two, is slightly more compressible than the long bond, with multiplicity four; as a consequence the octahedral tetragonal compression slightly increases under pressure. We also achieved a robust structural analysis of ferroselite at low temperature in the diamond anvil cell. Structural changes upon temperature decrease are small but qualitatively similar to those produced by pressure.


1993 ◽  
Vol 325 ◽  
Author(s):  
S. Mitha ◽  
S. D. Theiss ◽  
M. J. Aziz ◽  
D. Schiferl ◽  
D. B. Poker

AbstractWe report preliminary results of a study of the activation volume for diffusion of arsenic in germanium. High-temperature high-pressure anneals were performed in a liquid argon pressure medium in a diamond anvil cell capable of reaching 5 GPa and 7500 C, which is externally heated for uniform and repeatable temperature profiles. The broadening of an ion-implanted arsenic profile was measured by Secondary Ion Mass Spectrometry. Hydrostatic pressure retards the diffusivity at 575°C, characterized by an activation volume that is +15% of the atomic volume of Ge. Implications for diffusion mechanisms are discussed.


2011 ◽  
Vol 278 ◽  
pp. 012017 ◽  
Author(s):  
N Chigarev ◽  
P Zinin ◽  
D Mounier ◽  
A Bulou ◽  
A Zerr ◽  
...  

Author(s):  
Barbara Lavina ◽  
Robert T Downs ◽  
Stanislav Sinogeikin

We conducted an in-situ crystal structure analysis of ferroselite at non-ambient conditions. The aim is to provide a solid ground to further the understanding of the properties of this material in a broad range of conditions. Ferroselite, marcasite-type FeSe2, was studied under high pressures up to 46 GPa and low temperatures, down to 50 K using single-crystal microdiffraction techniques. High pressure and low temperatures were generated using a diamond anvil cell and a cryostat. We found no evidences of structural instability in the explored P-T space. The deformation of the orthorhombic lattice is slightly anisotropic. As expected, the compressibility of the Se-Se dumbbell, the longer bond in the structure, is larger than that of the Fe-Se bonds. Less obvious is the behavior of the octahedral bonds, the shorter bond is the most compressible determining a small increase in the octahedron distortion with pressure. We also achieved a robust structural analysis of ferroselite at low temperature in the diamond anvil cell. Structural changes upon temperature decrease are small but qualitatively similar to those produced by pressure.


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