Microwave assisted synthesis of β-keto thioethers and furan derivatives by thiol directed multicomponent reactions

2020 ◽  
Vol 44 (20) ◽  
pp. 8442-8453
Author(s):  
Asim Jana ◽  
Prabhas Bhaumick ◽  
Lokman H. Choudhury

A series of β-keto thioethers tethered with cyclic-1,3-dicarbonyls (4) and a tetra-substituted furan derivative (5) has been prepared by multicomponent reaction under microwave heating conditions.

ChemInform ◽  
2007 ◽  
Vol 38 (22) ◽  
Author(s):  
Shujiang Tu ◽  
Bo Jiang ◽  
Runhong Jia ◽  
Junyong Zhang ◽  
Yan Zhang

2006 ◽  
Vol 84 (8) ◽  
pp. 1050-1053 ◽  
Author(s):  
Zhen-Hua Liang ◽  
Ying-Jie Zhu ◽  
Guo-Feng Cheng ◽  
Yue-Hong Huang

Single crystalline β-Co(OH)2 nanosheets have been synthesized from a layered precursor cobalt(II) acetate hydroxide by microwave heating. The average thickness of β-Co(OH)2 nanosheets is ~10 nm, with particle sizes up to 360 nm. The layered precursor was prepared using Co(CH3COO)2·4H2O, ethylene glycol, and H2O in some cases by microwave heating. Co3O4 nanosheets have been synthesized by hydrothermal oxidation of the layered precursor cobalt(II) acetate hydroxide using H2O2.Key words: nanosheets, microwave, cobalt hydroxide, cobalt oxide.


2016 ◽  
Vol 40 (9) ◽  
pp. 7986-7995 ◽  
Author(s):  
Zohre Zarnegar ◽  
Javad Safari

The microwave-assisted synthesis of the first ionic liquid stabilized CNTs–Fe3O4as a novel nanocatalyst for the synthesis of 2-amino-chromenesviaa multicomponent reaction is reported.


RSC Advances ◽  
2017 ◽  
Vol 7 (81) ◽  
pp. 51062-51068 ◽  
Author(s):  
Felicia Phei Lin Lim ◽  
Szy Teng Low ◽  
Elvina Lee King Ho ◽  
Nathan R. Halcovitch ◽  
Edward R. T. Tiekink ◽  
...  

An efficient and highly selective multicomponent synthesis of 4-aminoimidazo[1,2-a]triazines, which are 5-aza-7-deaza-isosteres of adenine, was developed.


2017 ◽  
Vol 2017 ◽  
pp. 1-17 ◽  
Author(s):  
Zubi Sadiq ◽  
Erum Akbar Hussain ◽  
Narjis Naz ◽  
Ambreen Ghani ◽  
Kausar Yasmeen ◽  
...  

A new series of tetrahydrocarbazole coupled 1,2-diazoles 4/5/6(a–o) in moderate to excellent yield was synthesized successfully via multicomponent reaction approach by adopting Michael type-addition of hydrazines on in situ generated α,β-unsaturated ketones via aldol type strategy under synthetic microwave radiations and conventional heating. Structural confirmations of all the prepared compounds were achieved by spectroscopic techniques. The best results were achieved when equal amounts of water-acetic acid were used in microwave conditions in 4 minutes.


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