Laser ablation of microdroplets for copper isotopic analysis via MC-ICP-MS. Analysis of serum microsamples for the diagnosis and follow-up treatment of Wilson's disease

2021 ◽  
Author(s):  
M. Carmen García-Poyo ◽  
Sylvain Bérail ◽  
Anne Laure Ronzani ◽  
Luis Rello ◽  
Elena García-González ◽  
...  
Keyword(s):  
Laser Ablation ◽  
Wilson’S Disease ◽  
Isotopic Analysis ◽  
Wilson's Disease ◽  
Silicon Wafers ◽  
Ms Analysis ◽  
Icp Ms

The deposition of microdroplets onto silicon wafers followed by drying and fsLA is evaluated by MC-ICP-MS Cu isotopic analysis.

scholarly journals Quantitative Determination of the Surface Distribution of Supported Metal Nanoparticles: A Laser Ablation–ICP–MS Based Approach

Chemosensors ◽  
2021 ◽  
Vol 9 (4) ◽  
pp. 77
Author(s):  
Davide Spanu ◽  
Gilberto Binda ◽  
Marcello Marelli ◽  
Laura Rampazzi ◽  
Sandro Recchia ◽  
...  
Keyword(s):  
Spatial Distribution ◽  
Laser Ablation ◽  
Quantitative Determination ◽  
Metal Nanoparticles ◽  
Total Mass ◽  
Functional Materials ◽  
Metal Extraction ◽  
Ms Analysis ◽  
Icp Ms

A laser ablation–inductively coupled plasma–mass spectrometry (LA–ICP–MS) based method is proposed for the quantitative determination of the spatial distribution of metal nanoparticles (NPs) supported on planar substrates. The surface is sampled using tailored ablation patterns and the data are used to define three-dimensional functions describing the spatial distribution of NPs. The volume integrals of such interpolated surfaces are calibrated to obtain the mass distribution of Ag NPs by correlation with the total mass of metal as determined by metal extraction and ICP–MS analysis. Once this mass calibration is carried out on a sacrificial sample, quantifications can be performed over multiple samples by a simple micro-destructive LA–ICP–MS analysis without requiring the extraction/dissolution of metal NPs. The proposed approach is here tested using a model sample consisting of a low-density polyethylene (LDPE) disk decorated with silver NPs, achieving high spatial resolution over cm2-sized samples and very high sensitivity. The developed method is accordingly a useful analytical tool for applications requiring both the total mass and the spatial distribution of metal NPs to be determined without damaging the sample surface (e.g., composite functional materials and NPs, decorated catalysts or electrodic materials).

scholarly journals Matrix effects during laser ablation MC ICP-MS analysis of boron isotopes in tourmaline

2014 ◽  
Vol 29 (5) ◽  
pp. 903 ◽  
Author(s):  
Jitka Míková ◽  
Jan Košler ◽  
Michael Wiedenbeck
Keyword(s):  
Laser Ablation ◽  
Matrix Effects ◽  
Boron Isotopes ◽  
Ms Analysis ◽  
Icp Ms

Two age populations of zircons from the Timber Creek kimberlites, Northern Territory, as determined by laser-ablation ICP-MS analysis

2001 ◽  
Vol 48 (5) ◽  
pp. 757 ◽  
Author(s):  
E. A. Belousova ◽  
W. L. Griffin ◽  
S. R. Shee ◽  
S. E. Jackson ◽  
S. Y. O'Reilly
Keyword(s):  
Laser Ablation ◽  
Northern Territory ◽  
Ms Analysis ◽  
Icp Ms

A new practical isobaric interference correction model for the in situ Hf isotopic analysis using laser ablation-multi-collector-ICP-mass spectrometry of zircons with high Yb/Hf ratios

2019 ◽  
Vol 34 (6) ◽  
pp. 1223-1232 ◽  
Author(s):  
Hai-Ou Gu ◽  
He Sun ◽  
Fangyue Wang ◽  
Can Ge ◽  
Taofa Zhou
Keyword(s):  
Mass Spectrometry ◽  
Laser Ablation ◽  
Isotopic Analysis ◽  
Correction Model ◽  
Isobaric Interference ◽  
Interference Correction ◽  
Icp Ms ◽  
Icp Mass Spectrometry

An isobaric interference correction model was proposed for the in situ Hf isotopic analysis of zircons with high Yb/Hf ratios using LA-MC-ICP-MS.

Spatial investigation of the elemental distribution in Wilson’s disease liver after d -penicillamine treatment by LA-ICP-MS

2017 ◽  
Vol 44 ◽  
pp. 26-31 ◽  
Author(s):  
Oliver Hachmöller ◽  
Andree Zibert ◽  
Hans Zischka ◽  
Michael Sperling ◽  
Sara Reinartz Groba ◽  
...  
Keyword(s):  
Wilson’S Disease ◽  
Wilson's Disease ◽  
Elemental Distribution ◽  
Icp Ms ◽  
Spatial Investigation
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