Addressing regio- and stereo-specificity challenges in the synthesis of nucleoside 2′,3′-cyclic monophosphate analogs – a rapid and facile synthesis of nucleoside-2′,3′-O,O-phosphoro-thioate or -selenoate, and elucidation of the origin of the rare specificity

2020 ◽  
Vol 56 (78) ◽  
pp. 11633-11636
Author(s):  
Molhm Nassir ◽  
Lara Balaom ◽  
Bilha Fischer

A new facile, rapid, stereo- and regio-selective one-pot synthesis of nucleoside-2′,3′-O,O-phosphorothioate and selenoate analogs has been developed.

2009 ◽  
Vol 21 (8) ◽  
pp. 869-873 ◽  
Author(s):  
Chung Yen Ang ◽  
Louise Giam ◽  
Zheng Ming Chan ◽  
Alex W. H. Lin ◽  
Hongwei Gu ◽  
...  

2012 ◽  
Vol 9 (4) ◽  
pp. 2239-2244 ◽  
Author(s):  
Hossein Anaraki-Ardakani ◽  
Maziar Noei ◽  
Mina Karbalaei-Harofteh ◽  
Shahab Zomorodbakhsh

A new and efficient one-pot synthesis of polysubstituted pyrrole derivatives by three-component reaction between dialkyl acetylenedicarboxylates, triphenylphosphine, 2-aminopyridin derivatives in the presence of arylglyoxals is described. The reactions were performed in dichloromethane at room temperature and neutral conditions and afforded high yields of products.


2015 ◽  
Vol 3 (29) ◽  
pp. 15068-15073 ◽  
Author(s):  
Peng Miao ◽  
Yuguo Tang ◽  
Kun Han ◽  
Bidou Wang

A one-pot synthesis approach is used to prepare carbon nanodots by electrochemical carbonization of ethanol under basic conditions. These materials are further applied in the fabrication of a Fe3+ biosensor.


2019 ◽  
Vol 1 (6) ◽  
pp. 2157-2161 ◽  
Author(s):  
Seokyoung Yoon ◽  
Chansong Kim ◽  
Byoungsang Lee ◽  
Jung Heon Lee

Inversion of the role of Au(iii) chloride allows facile synthesis of smooth and spherical AuNPs with nanoscale size tunability.


2015 ◽  
Vol 21 (45) ◽  
pp. 15914-15918 ◽  
Author(s):  
Soundararasu Senthilkumar ◽  
Sure Siva Prasad ◽  
Amrita Das ◽  
Sundarababu Baskaran

The Analyst ◽  
2016 ◽  
Vol 141 (15) ◽  
pp. 4757-4765 ◽  
Author(s):  
Ziyin Yang ◽  
Xiaohui Zheng ◽  
Zhi Li ◽  
Jianbin Zheng

In this study, we described the facile synthesis of carbon nitride dots–reduced graphene oxide nanocomposites (CNDs–rGO) and their application for the enhanced electrochemical determination of dopamine (DA) and uric acid (UA).


2021 ◽  
Author(s):  
Volker Jens Eilrich ◽  
Toni Grell ◽  
Peter Lönnecke ◽  
Evamarie Hey-Hawkins

The cyclo-(P4tBu3) synthon [Li{cyclo-(P4tBu3)}(thf)(tmeda)] (1) (thf = tetrahydrofuran, tmeda = N,N,N′,N′-tetramethylethane-1,2-diamine) is readily accessible in a one-pot synthesis from P4 and LitBu. The use of 1 as a cyclo-(P4tBu3) building block enables the rational...


RSC Advances ◽  
2019 ◽  
Vol 9 (68) ◽  
pp. 39735-39742 ◽  
Author(s):  
Trimurti L. Lambat ◽  
Ahmed A. Abdala ◽  
Sami Mahmood ◽  
Pankaj V. Ledade ◽  
Ratiram G. Chaudhary ◽  
...  

We report an efficient and facile one-pot synthesis of 4-oxo-tetrahydroindoles using sulfamic acid under ball milling conditions.


2020 ◽  
Vol 49 (2) ◽  
pp. 418-430 ◽  
Author(s):  
Mingxin Lv ◽  
Qianghua Xin ◽  
Bing Bian ◽  
Shitao Yu ◽  
Shiwei Liu ◽  
...  

The facile synthesis of yolk–shell-structured nanoparticles (YSNPs) with mobile active metal cores and mesoporous inorganic–organic hybrid silica shells (mHSiO2) is important for their applications.


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