Facile synthesis of cyclo-(P4tBu3)-containing oligo- and pnictaphosphanes

2021 ◽  
Author(s):  
Volker Jens Eilrich ◽  
Toni Grell ◽  
Peter Lönnecke ◽  
Evamarie Hey-Hawkins
Keyword(s):  
Building Block ◽  
Facile Synthesis ◽  
One Pot ◽  
One Pot Synthesis

The cyclo-(P4tBu3) synthon [Li{cyclo-(P4tBu3)}(thf)(tmeda)] (1) (thf = tetrahydrofuran, tmeda = N,N,N′,N′-tetramethylethane-1,2-diamine) is readily accessible in a one-pot synthesis from P4 and LitBu. The use of 1 as a cyclo-(P4tBu3) building block enables the rational...

Facile Synthesis of Fe2O3Nanocrystals without Fe(CO)5Precursor and One-Pot Synthesis of Highly Fluorescent Fe2O3-CdSe Nanocomposites

2009 ◽  
Vol 21 (8) ◽  
pp. 869-873 ◽  
Author(s):  
Chung Yen Ang ◽  
Louise Giam ◽  
Zheng Ming Chan ◽  
Alex W. H. Lin ◽  
Hongwei Gu ◽  
...  
Keyword(s):  
Facile Synthesis ◽  
One Pot ◽  
One Pot Synthesis

scholarly journals A Facile Synthesis of Polysubstituted Pyrroles by One-Pot Three-Component Reaction

2012 ◽  
Vol 9 (4) ◽  
pp. 2239-2244 ◽  
Author(s):  
Hossein Anaraki-Ardakani ◽  
Maziar Noei ◽  
Mina Karbalaei-Harofteh ◽  
Shahab Zomorodbakhsh
Keyword(s):  
Room Temperature ◽  
Facile Synthesis ◽  
One Pot ◽  
Pyrrole Derivatives ◽  
Dialkyl Acetylenedicarboxylates ◽  
One Pot Synthesis ◽  
Three Component Reaction ◽  
High Yields ◽  
Neutral Conditions

A new and efficient one-pot synthesis of polysubstituted pyrrole derivatives by three-component reaction between dialkyl acetylenedicarboxylates, triphenylphosphine, 2-aminopyridin derivatives in the presence of arylglyoxals is described. The reactions were performed in dichloromethane at room temperature and neutral conditions and afforded high yields of products.

Facile synthesis of carbon nanodots from ethanol and their application in ferric(iii) ion assay

2015 ◽  
Vol 3 (29) ◽  
pp. 15068-15073 ◽  
Author(s):  
Peng Miao ◽  
Yuguo Tang ◽  
Kun Han ◽  
Bidou Wang
Keyword(s):  
Carbon Nanodots ◽  
Facile Synthesis ◽  
One Pot ◽  
One Pot Synthesis ◽  
Synthesis Approach

A one-pot synthesis approach is used to prepare carbon nanodots by electrochemical carbonization of ethanol under basic conditions. These materials are further applied in the fabrication of a Fe3+ biosensor.

5-Aminouracil as a Building Block in Heterocyclic Synthesis: Part IV. One-pot Synthesis of 1H-Pyrrolo[2,3-d]pyrimidine-2,4(3H,7H)-dione Derivatives Using Controlled Microwave Heating

2011 ◽  
Vol 66 (8) ◽  
pp. 843-849
Author(s):  
Raafat M. Shaker ◽  
Kamal U. Sadek ◽  
Ebtisam A. Hafez ◽  
Mohamed Abd Elrady
Keyword(s):  
Microwave Heating ◽  
Building Block ◽  
Heterocyclic Synthesis ◽  
One Pot ◽  
H Nmr ◽  
One Pot Synthesis ◽  
Elemental Analyses ◽  
C Nmr

An efficient and direct procedure for the synthesis of pyrrolo[2,3-d]pyrimidine-2,4-dione derivatives using controlled microwave heating has been described. The products were characterized by elemental analyses, IR, 1H NMR, 13C NMR and MS spectra.

scholarly journals From a precursor to an etchant: spontaneous inversion of the role of Au(iii) chloride for one-pot synthesis of smooth and spherical gold nanoparticles

2019 ◽  
Vol 1 (6) ◽  
pp. 2157-2161 ◽  
Author(s):  
Seokyoung Yoon ◽  
Chansong Kim ◽  
Byoungsang Lee ◽  
Jung Heon Lee
Keyword(s):  
Gold Nanoparticles ◽  
Facile Synthesis ◽  
One Pot ◽  
One Pot Synthesis ◽  
Spherical Gold Nanoparticles

Inversion of the role of Au(iii) chloride allows facile synthesis of smooth and spherical AuNPs with nanoscale size tunability.

One-Pot Synthesis of Hydrophobically Modified IminosugarC-Alkynylglycosides: Facile Synthesis of Polyhydroxy Tetrahydroindolizines

2015 ◽  
Vol 21 (45) ◽  
pp. 15914-15918 ◽  
Author(s):  
Soundararasu Senthilkumar ◽  
Sure Siva Prasad ◽  
Amrita Das ◽  
Sundarababu Baskaran
Keyword(s):  
Facile Synthesis ◽  
One Pot ◽  
One Pot Synthesis ◽  
Hydrophobically Modified

A facile one-pot synthesis of carbon nitride dots–reduced graphene oxide nanocomposites for simultaneous enhanced detecting of dopamine and uric acid

The Analyst ◽  
2016 ◽  
Vol 141 (15) ◽  
pp. 4757-4765 ◽  
Author(s):  
Ziyin Yang ◽  
Xiaohui Zheng ◽  
Zhi Li ◽  
Jianbin Zheng
Keyword(s):  
Uric Acid ◽  
Graphene Oxide ◽  
Reduced Graphene Oxide ◽  
Carbon Nitride ◽  
Electrochemical Determination ◽  
Facile Synthesis ◽  
One Pot ◽  
One Pot Synthesis ◽  
Reduced Graphene

In this study, we described the facile synthesis of carbon nitride dots–reduced graphene oxide nanocomposites (CNDs–rGO) and their application for the enhanced electrochemical determination of dopamine (DA) and uric acid (UA).

scholarly journals 5-Aminouracil as a Building Block in Heterocyclic Synthesis: Part III. One-pot Synthesis of Novel Pyrimido[5,4-b]quinoline-2,4,9-triones and Pyrimido[5,4-c]isoquinolines

2010 ◽  
Vol 65 (12) ◽  
pp. 1485-1490 ◽  
Author(s):  
Raafat M. Shaker ◽  
Kamal U. Sadek ◽  
Ebtisam A. Hafez ◽  
Mohamed Abd Elrady
Keyword(s):  
Building Block ◽  
Heterocyclic Synthesis ◽  
One Pot ◽  
H Nmr ◽  
One Pot Synthesis ◽  
Elemental Analyses ◽  
Isoquinoline Derivatives ◽  
C Nmr

An efficient and direct procedure for the synthesis of pyrimido[5,4-b]quinoline-2,4,9-trione and pyrimido[5,4-c]isoquinoline derivatives has been described. The products were characterized by elemental analyses, IR, 1H NMR, 13C NMR and MS spectra.

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