scholarly journals In situ formation of PLA-grafted alkoxysilanes for toughening a biodegradable PLA stereocomplex thin film

RSC Advances ◽  
2019 ◽  
Vol 9 (38) ◽  
pp. 21748-21759 ◽  
Author(s):  
Jieun Jeong ◽  
Muhammad Ayyoob ◽  
Ji-Heung Kim ◽  
Sung Woo Nam ◽  
Young Jun Kim
Keyword(s):  
Thin Film ◽  
Mechanical Properties ◽  
Significant Loss ◽  
Current Work ◽  
Synergistic Approach ◽  
In Situ Formation

Current work provides a synergistic approach to prepare super tough PLA without any significant loss of its excellent intrinsic mechanical properties.

Effect of in situ formation of tungsten semicarbide on the microstructure and mechanical properties of medium carbon steel composites

2021 ◽  
Vol 118 (6) ◽  
pp. 606
Author(s):  
Nandish Girishbhai Soni ◽  
Akash Ganesh Mahajan ◽  
Kaustubh Ramesh Kambale ◽  
Sandeep Prabhakar Butee
Keyword(s):  
Mechanical Properties ◽  
Particle Size ◽  
Wear Resistance ◽  
Carbon Steel ◽  
Sintered Density ◽  
Medium Carbon Steel ◽  
Complete Conversion ◽  
Medium Carbon ◽  
In Situ Formation

Fabrication with the in-situ formation of W2C reinforced medium carbon steel (MCS) MMC’s was attempted using W or WO3 and graphite addition to steel. The P/M route comprising milling, compaction and sintering at 1050 °C and 1120 °C respectively in 90% N2 + 10% H2 atmosphere was adopted. Both SEM and BET studies revealed the particle size to be around 100, 7 and 40 µm for MCS, W and WO3, respectively. A complete conversion of tungsten into tungsten semicarbide (W2C) was noted in XRD for the tungsten additions of ∼6, 9 and 12 wt.% with stoichiometrically balanced C (graphite) addition of 0, 0.2 and 0.4 wt.%. However, WO3 + C addition (balanced as above) revealed the partial conversion of WO3 to W2C. The peaks of Fe3C were observed only for MCS + W + C samples and not for MCS + WO3 + C samples in XRD. In SEM, the WO3 phase appeared porous and partially converted, whereas, W2C phase was dense. Sintered density improved for the addition of W, whereas it monotonically reduced for WO3 addition to MCS + C samples. Higher hardness, compressive strength, and wear resistance was noted for W addition than WO3 to MCS+C samples.

Microstructure Development and Mechanical Properties of Ce-TZP/La- β-Alumina Composites

1992 ◽  
Vol 274 ◽  
Author(s):  
Takashi Fujii ◽  
Hironobu Muragaki ◽  
Hiraku Hatano ◽  
Shin-Ichi Hirano
Keyword(s):  
Mechanical Properties ◽  
Fracture Toughness ◽  
Hydrothermal Treatment ◽  
Fracture Strength ◽  
Sintered Body ◽  
Microstructure Development ◽  
Lanthanum Aluminate ◽  
Alumina Composites ◽  
In Situ Formation

ABSTRACTSimultaneous additions of lanthanum aluminate(LAL) and Al2O3 to Ce-TZP (12mol% CeO2-ZrO2) lead to the in-situ formation of lanthanum- β-alumina(LBA) platelets (∼1.0.μ m in width and 5 ∼10 μ m in length) in the Ce-TZP matrix during sintering. The composites showed a fracture toughness(SEPB method) of 9.5 MPa · m0.5 and fracture strength of 960 MPa. which are remarkably improved from Ce-TZP sintered body (8.5 MPa · m0.5 and 560 MPa).The composites also exhibit the no degradation by hydrothermal treatment.

In-situ formation of thin-film like β′'-alumina layers on α-alumina substrates

Ionics ◽  
1997 ◽  
Vol 3 (3-4) ◽  
pp. 277-281 ◽  
Author(s):  
O. Schäf ◽  
T. Widmer ◽  
U. Guth
Keyword(s):  
Thin Film ◽  
In Situ Formation

scholarly journals Melanocyte pigmentation stiffens murine cardiac tricuspid valve leaflet

2009 ◽  
Vol 6 (40) ◽  
pp. 1097-1102 ◽  
Author(s):  
Kantesh Balani ◽  
Flavia C. Brito ◽  
Lidia Kos ◽  
Arvind Agarwal
Keyword(s):  
Mechanical Properties ◽  
Storage Modulus ◽  
Tricuspid Valve ◽  
Viscoelastic Properties ◽  
Mechanical Analysis ◽  
Current Work ◽  
Valve Leaflet ◽  
Stiffness Measurement ◽  
Proper Functioning

Pigmentation of murine cardiac tricuspid valve leaflet is associated with melanocyte concentration, which affects its stiffness. Owing to its biological and viscoelastic nature, estimation of the in situ stiffness measurement becomes a challenging task. Therefore, quasi-static and nanodynamic mechanical analysis of the leaflets of the mouse tricuspid valve is performed in the current work. The mechanical properties along the leaflet vary with the degree of pigmentation. Pigmented regions of the valve leaflet that contain melanocytes displayed higher storage modulus (7–10 GPa) than non-pigmented areas (2.5–4 GPa). These results suggest that the presence of melanocytes affects the viscoelastic properties of the mouse atrioventricular valves and are important for their proper functioning in the organism.

Microstructure and Mechanical Properties of In Situ Cast Aluminum Based Composites Reinforced with TiC Nano-Particles

2020 ◽  
Vol 985 ◽  
pp. 211-217
Author(s):  
Wojciech Maziarz ◽  
Piotr Bobrowski ◽  
Anna Wójcik ◽  
Agnieszka Bigos ◽  
Łukasz Szymański ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Coefficient Of Thermal Expansion ◽  
Nano Particles ◽  
Cast Aluminum ◽  
Casting Method ◽  
Microstructure And Mechanical Properties ◽  
Transmission Electron ◽  
Cast Composites ◽  
In Situ Formation

This work concerns microstructure and mechanical properties investigations of aluminum based composite strengthened with the TiC particles being in nanometer size. The composites were fabricated by the casting method combined with in-situ formation of TiC particles. Applying a suitable composition of components and moderators of SHS reaction which occur during casting, it was possible to cast the samples with TiC particles of size of 150 nm and faceted shape. Microstructure investigations using scanning and transmission electron microscopy (SEM and TEM) allowed to identified the distribution of TiC particles and their preferred location in the microstructure of composites. Also the additional precipitates with different size and shape were identified in investigated samples. Significant increase of strength was observed in in-situ cast composites in comparison to Al-1000 alloy mainly due mainly due to coefficient of thermal expansion and elastic modulus mismatch between the reinforcements and the metal matrix, Hall-Pecht relation and also in minority the Orowan effect.

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