Nature of the multicomponent crystal of salicylic acid and 1,2-phenylenediamine

CrystEngComm ◽  
2020 ◽  
Vol 22 (4) ◽  
pp. 708-719
Author(s):  
Aniele Z. Tier ◽  
Keli M. Wust ◽  
Jean C. B. Vieira ◽  
Mariana Sardo ◽  
Tomaž Čendak ◽  
...  

The synthesis and characterization of the multicomponent crystal formed by salicylic acid and 1,2-phenylenediamine (a diarylamine) are reported.

ChemInform ◽  
2010 ◽  
Vol 24 (42) ◽  
pp. no-no
Author(s):  
G. GRYNKIEWICZ ◽  
O. ACHMATOWICZ ◽  
J. HENNIG ◽  
J. INDULSKI ◽  
D. F. KLESSIG

Author(s):  
Xenia Lupea ◽  
Mirabela Padure

The synthesis of some N-substituted aromatic amides in the salicylic acid series was achieved, by direct reaction between primary amines and salicylic acid in inert organic solvent, in the presence of PCl3. The compounds that were obtained, partially not described in literature, were characterized by chemical-physical methods.


2018 ◽  
Vol 34 (4) ◽  
pp. 2131-2136 ◽  
Author(s):  
Abdullah Jawad Kadhim ◽  
Ali Chazi Kazim

This research paper deals with the synthesis and diagnose of Benzimidazole rings which were have been prepared by using two different methods in which used starting material o-phenylenediamine with different compounds. The first method is with aldehydes such as 4-Chlorobenzaldehyde, 4-N, N-Dimethylbenzaldehyde, and Formaldehyde. The second is with Carboxylic acids such as Salicylic acid, Acetic acid, and Butanoic acid. ρ-TSOH has been using as a catalyst in the synthesis methods above and used F.T.I.R and HNMR spectroscopy are used for diagnosing the prepared rings in addition to the physical properties.


2006 ◽  
Vol 60 (2) ◽  
Author(s):  
Y. Xuwu ◽  
S. Wujuan ◽  
K. Congyu ◽  
Z. Li ◽  
Z. Hangguo ◽  
...  

AbstractSeven rare-earth complexes with salicylic acid RE(HSal)3·nH2O (HSal = C7H5O3; RE = La-Sm, n = 2; RE = Eu, Gd, n = 1) were synthesized and characterized by elemental analysis, the IR spectrum, and cyclic voltammetry. The constant-volume combustion energies of complexes, Δc U, were determined by a precise rotating-bomb calorimeter at 298.15 K. Their standard molar enthalpies of combustion, Δc H mo, and standard molar enthalpies of formation, Δf H mo, were calculated.


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