The determination of trace free acid content in lithium-ion battery electrolytes by coulometric titration in non-aqueous media

The Analyst ◽  
2020 ◽  
Vol 145 (2) ◽  
pp. 582-587
Author(s):  
Cairui Huang ◽  
Congcong Shen ◽  
Ling Jin ◽  
Deyu Qu ◽  
Xiaosong Hu ◽  
...  

A new quantitative analysis method was proposed, aiming at resolving the difficulty encountered in accurately determining the trace content of a free acid in lithium-ion battery electrolytes in the past 30 years.

Batteries ◽  
2019 ◽  
Vol 5 (3) ◽  
pp. 57 ◽  
Author(s):  
Seyed Madani ◽  
Erik Schaltz ◽  
Søren Knudsen Kær

The determination of coulombic efficiency of the lithium-ion batteries can contribute to comprehend better their degradation behavior. In this research, the coulombic efficiency and capacity loss of three lithium-ion batteries at different current rates (C) were investigated. Two new battery cells were discharged and charged at 0.4 C and 0.8 C for twenty times to monitor the variations in the aging and coulombic efficiency of the battery cell. In addition, prior cycling was applied to the third battery cell which consist of charging and discharging with 0.2 C, 0.4 C, 0.6 C, and 0.8 C current rates and each of them twenty times. The coulombic efficiency of the new battery cells was compared with the cycled one. The experiments demonstrated that approximately all the charge that was stored in the battery cell was extracted out of the battery cell, even at the bigger charging and discharging currents. The average capacity loss rates for discharge and charge during 0.8 C were approximately 0.44% and 0.45% per cycle, correspondingly.


Nanoscale ◽  
2015 ◽  
Vol 7 (21) ◽  
pp. 9919-9926 ◽  
Author(s):  
Wanshuang Liu ◽  
Chenyang Zhao ◽  
Rui Zhou ◽  
Dan Zhou ◽  
Zhaolin Liu ◽  
...  

We disclose that alkali lignin is an excellent surfactant for direct aqueous exfoliation of MoS2and the exfoliated nanosheets have great potential for low-cost lithium-ion battery electrodes.


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