Phase pure Ni3S2 and NiS from bis(N′-ethyl-N-piperazinylcarbodithioato-S,S′)–nickel(ii) via solvent thermolysis and aerosol assisted chemical vapour deposition

2018 ◽  
Vol 42 (8) ◽  
pp. 6203-6209 ◽  
Author(s):  
Charles Gervas ◽  
Sixberth Mlowe ◽  
Matthew P. Akerman ◽  
Neerish Revaprasadu

We report the structure of a triclinic bis(N′-ethyl-N-piperazinylcarbodithioato-S,S′)–nickel(ii) complex and its use as a single source precursor for the synthesis of nickel sulfide thin films and nanoparticles.

2019 ◽  
Vol 48 (1) ◽  
pp. 117-124 ◽  
Author(s):  
Samantha L. Hawken ◽  
Ruomeng Huang ◽  
C. H. (Kees) de Groot ◽  
Andrew L. Hector ◽  
Marek Jura ◽  
...  

Reaction of activated germanium with nBu2Te2 in THF solution was shown to be more effective for the preparation of the germanium(iv) tellurolate compound, [Ge(TenBu)4], than reaction of GeCl4 with LiTenBu in THF.


2016 ◽  
Vol 4 (45) ◽  
pp. 10731-10739 ◽  
Author(s):  
Amanda L. Catherall ◽  
Michael S. Hill ◽  
Andrew L. Johnson ◽  
Gabriele Kociok-Köhn ◽  
Mary F. Mahon

We report the development of a true single source precursor for the growth of zirconia thin films by aerosol-assisted chemical vapour deposition using an original family of zirconium(iv) amidate derivatives.


Polyhedron ◽  
2008 ◽  
Vol 27 (16) ◽  
pp. 3337-3342 ◽  
Author(s):  
Muhammad Shahid ◽  
Muhammad Mazhar ◽  
Mohammad A. Malik ◽  
Paul O’ Brien ◽  
James Raftery

2014 ◽  
Vol 38 (12) ◽  
pp. 6073-6080 ◽  
Author(s):  
Sixberth Mlowe ◽  
David J. Lewis ◽  
M. Azad Malik ◽  
James Raftery ◽  
Egid B. Mubofu ◽  
...  

The pyridine adduct of a cadmium piperidine dithiocarbamate complex was used to deposit CdS thin films and for the synthesis of CdS nanoparticles.


2010 ◽  
Vol 518 (14) ◽  
pp. 3664-3668 ◽  
Author(s):  
Asif Ali Tahir ◽  
K.G.U. Wijayantha ◽  
Muhammad Mazhar ◽  
Vickie McKee

2005 ◽  
Vol 879 ◽  
Author(s):  
P.L. Musetha ◽  
N. Revaprasadu ◽  
M.A Malik ◽  
P. O'Brien

AbstractNickel sulphide (NiS) thin films have been deposited on glass by aerosol assisted chemical vapour deposition(AACVD) using single source precursors of the type, ([Ni(S2COR2)2], R = C2H5 or C3H7). TGA analyses showed that the precursors are highly volatile, making them suitable for AACVD studies. As deposited NiS films were polycrystalline as confirmed by XRD. The films have been characterised by xray diffraction (XRD), scanning electron microscopy (SEM), and Energy dispersive analysis of x-rays (EDAX).


2006 ◽  
Vol 16 (10) ◽  
pp. 966-969 ◽  
Author(s):  
Shivram S. Garje ◽  
Jamie S. Ritch ◽  
Dana J. Eisler ◽  
Mohammad Afzaal ◽  
Paul O'Brien ◽  
...  

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