Fast synthesis of Li2S–P2S5–LiI solid electrolyte precursors

2017 ◽  
Vol 4 (10) ◽  
pp. 1660-1664 ◽  
Author(s):  
Nguyen Huu Huy Phuc ◽  
Tokoharu Yamamoto ◽  
Hiroyuki Muto ◽  
Atsunori Matsuda
Keyword(s):  
Solid Electrolyte ◽  
Ethyl Propionate ◽  
One Pot ◽  
One Pot Synthesis ◽  
Short Time ◽  
Fast Synthesis

A one-pot synthesis of Li2S–P2S5–LiI solid electrolyte precursors in a short time of 30 min is demonstrated by using ethyl propionate as a solvent.

scholarly journals An Efficient One-Pot Multi-Component Synthesis of 3,4-Dihydropyrimidin-2-(1H)-Ones/Thiones Catalyzed by Bismuth (III) Sulfate Trihydrate under Solvent-Free Conditions

2014 ◽  
Vol 2014 ◽  
pp. 1-5 ◽  
Author(s):  
Farhad Hatamjafari
Keyword(s):  
Solvent Free ◽  
One Pot ◽  
Dicarbonyl Compounds ◽  
One Pot Synthesis ◽  
Solvent Free Conditions ◽  
The One ◽  
Short Time ◽  
Derivatives Of

A convenient and efficient protocol for the one-pot synthesis of 3,4-dihydropyrimidin-2-(1H)-one/thione derivatives of aldehydes, and 1,3-dicarbonyl compounds with Bismuth (III) sulfate trihydrate as the catalyst was described. We had the advantages of good performance, simplicity, and short time reaction under solvent-free conditions. The catalyst can be repeatedly reused without loss of its activity.

scholarly journals One Pot Synthesis, Surface and Magnetic Properties of Cu2O/Cu and Cu2O/CuO Nanocomposites

Crystals ◽  
2021 ◽  
Vol 11 (7) ◽  
pp. 751
Author(s):  
Sameerah I. Al-Saeedi ◽  
Ghadah M. Al-Senani ◽  
Omar H. Abd-Elkader ◽  
Nasrallah M. Deraz
Keyword(s):  
Magnetic Properties ◽  
Low Cost ◽  
Synthesis Process ◽  
Transmission Electron Micrograph ◽  
One Pot ◽  
One Pot Synthesis ◽  
Auto Combustion ◽  
Product Displays ◽  
Short Time ◽  
Adsorption Desorption

A series of copper-based systems containing two different nanocomposites (Cu2O/CuO and Cu2O/Cu) was synthesized by the egg white assisted auto-combustion route. This method was distinguished by the simplicity of its steps, low cost, one-pot synthesis process at low temperature and, short time. The characterization of the as prepared nanocomposites was carried out by using X-ray diffraction (XRD), Fourier-transform infrared (FTIR), Scanning electron microscope (SEM) and transmission electron micrograph (TEM), Energy dispersive spectrometry (EDS) techniques. Surface and magnetic properties of the obtained systems were determined by using N2 adsorption/desorption isotherms at 77 K and the vibrating sample magnetometer (VSM) technique. XRD results confirmed the formation of Cu2O/CuO and Cu2O/Cu nanocomposites with different ratios of well crystalline CuO, Cu2O, and Cu phases. FTIR results of the combusted product displays the presence of both CuO and Cu2O, respectively. SEM/EDS and TEM results confirm the formation of a porous nanocomposite containing Cu, O, and C elements. The change in concentration of the oxygen vacancies at the surface or interface of both Cu2O/CuO and Cu2O/Cu nanoparticles resulted in different changes in their magnetization. Based on this study, it is possible to obtain nanocomposite-based copper with multiple valances by a simple and inexpensive route which can be suitable for the fabrication of different transition metal composites.

One-Pot Synthesis and Conformational Analysis of 6-Membered Cyclic Iodonium Salts

2020 ◽  
Author(s):  
Lucien Caspers ◽  
Julian Spils ◽  
Mattis Damrath ◽  
Enno Lork ◽  
Boris Nachtsheim
Keyword(s):  
Conformational Analysis ◽  
Bronsted Acids ◽  
One Pot ◽  
Benzyl Alcohols ◽  
Iodonium Salts ◽  
Efficient Approach ◽  
One Pot Synthesis ◽  
Diaryliodonium Salts

In this article we describe an efficient approach for the synthesis of cyclic diaryliodonium salts. The method is based on benzyl alcohols as starting materials and consists of an Friedel-Crafts-arylation/oxidation sequence. Besides a deep optimization, particluar focusing on the choice and ratios of the utilized Bronsted-acids and oxidants, we explore the substrate scope of this transformation. We also discuss an interesting isomerism of cyclic iodonium salts substituted with aliphatic substituents at the bridge head carbon. <br>

Facile and Convenient Ag/Cd/Cu Nanoparticle Catalysed One-pot Synthesis of Xanthenes

2017 ◽  
Vol 7 (12) ◽  
pp. 1192-1195
Author(s):  
Y. I. Shaikh ◽  
G. M. Nazeruddin ◽  
Khursheed Ahmed
Keyword(s):  
One Pot ◽  
One Pot Synthesis ◽  
Cu Nanoparticle

Microwave-assisted one-pot synthesis of pyrimido［4,5-b］quinolines derivatives

2013 ◽  
Vol 30 (6) ◽  
pp. 636-642
Author(s):  
Xueli Zhang ◽  
Zhilan Lin ◽  
Huiling Hu ◽  
Jiaxin He ◽  
Yuan Gao
Keyword(s):  
One Pot ◽  
Microwave Assisted ◽  
One Pot Synthesis
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