A facile synthetic route for the morphology-controlled formation of triazine-based covalent organic nanosheets (CONs)

2017 ◽  
Vol 8 (37) ◽  
pp. 5655-5659 ◽  
Author(s):  
Min-Sung Kim ◽  
Cheol Soo Phang ◽  
Young Kyu Jeong ◽  
Jin Kuen Park
Keyword(s):  
Film Formation ◽  
Synthetic Route ◽  
New Type

A new type of organic nanosheet was synthesized via two different routes. We found that the morphologies of resulting products can be controlled based on the synthetic route and solvent used for film formation.

N-Substituted tetrahydropentaazadibenzocycloheptafluorenes – a new type of condensed polyazapolycyclic system

2021 ◽  
Author(s):  
Elena B. Rakhimova ◽  
Victor Yu. Kirsanov ◽  
Ekaterina S. Mescheryakova ◽  
Leonard M. Khalilov ◽  
Askhat G. Ibragimov
Keyword(s):  
Synthetic Route ◽  
System P ◽  
New Type

Ni-Catalyzed heterocyclization of octahydro-2,2′-biquinazoline with 1,3,5-triazinanes is an efficient synthetic route to mono-N-substituted tetrahydro-4b,5a,10b,12,13a-pentaazadibenzo[a,h]-cyclohepta[1,2,3,4-def]fluorenes.

Synthetic route to 5-substituted uridines via a new type of desulfurizative stannylation

Tetrahedron ◽  
1986 ◽  
Vol 42 (15) ◽  
pp. 4187-4195 ◽  
Author(s):  
Hiromichi Tanaka ◽  
Hiroyuki Hayakawa ◽  
Kikoh Obi ◽  
Miyasaka Tadashi
Keyword(s):  
Synthetic Route ◽  
New Type

scholarly journals A New Synthetic Route to Organic Aerogels

1990 ◽  
Vol 180 ◽  
Author(s):  
R.W. Pekala ◽  
C.T. Alviso
Keyword(s):  
High Surface ◽  
Sol Gel ◽  
Synthetic Route ◽  
Melamine Formaldehyde ◽  
Resorcinol Formaldehyde ◽  
Surface Areas ◽  
New Material ◽  
New Type ◽  
Organic Aerogel ◽  
Organic Aerogels

ABSTRACTThe aqueous, sol-gel polymerization of melamine with formaldehyde, followed by supercritical extraction, leads to the formation of a new type of organic aerogel. Synthetic conditions (e.g. reaction time, pH) affect the density, transparency, and microstructure of the resultant aerogels. Unlike previous organic aerogels based upon resorcinol-formaldehyde, the melamine-formaldehyde aerogels are both colorless and transparent. Low densities (0.1–0.8 g/cc), high surface areas (∼1000 m2/g), and optical clarity are only a few of the promising characteristics of this new material.

New Type of Photoluminescent Iridium Complex: Novel Synthetic Route for Cationictrans-Bis(2-phenylpyridinato)iridium(III) Complex

2006 ◽  
Vol 2006 (24) ◽  
pp. 4979-4982 ◽  
Author(s):  
Chong Shik Chin ◽  
Min-Sik Eum ◽  
Song yi Kim ◽  
Choongil Kim ◽  
Sung Kwon Kang
Keyword(s):  
Iridium Complex ◽  
Synthetic Route ◽  
New Type

The Microstructure of Shock-Synthesized Diamond

1967 ◽  
Vol 25 ◽  
pp. 324-325
Author(s):  
Lucien F. Trueb
Keyword(s):  
Single Crystals ◽  
Preferred Orientation ◽  
High Magnification ◽  
Texture Pattern ◽  
Shock Process ◽  
New Type ◽  
Diffraction Diagram

A new type of synthetic industrial diamond formed by an explosive shock process has been recently developed by the Du Pont Company. This material consists of a mixture of two basically different forms, as shown in Figure 1: relatively flat and compact aggregates of acicular crystallites, and single crystals in the form of irregular polyhedra with straight edges.Figure 2 is a high magnification micrograph typical for the fibrous aggregates; it shows that they are composed of bundles of crystallites 0.05-0.3 μ long and 0.02 μ. wide. The selected area diffraction diagram (insert in Figure 2) consists of a weak polycrystalline ring pattern and a strong texture pattern with arc reflections. The latter results from crystals having preferred orientation, which shows that in a given particle most fibrils have a similar orientation.

New type electron gun with electrostatic and electromagnetic lenses

1978 ◽  
Vol 36 (1) ◽  
pp. 62-63
Author(s):  
T. Ichinokawa ◽  
H. Maeda
Keyword(s):  
Electron Microscopy ◽  
Electron Beam ◽  
Optimum Condition ◽  
Bias Voltage ◽  
Electron Gun ◽  
Charge Effect ◽  
Micro Fabrication ◽  
Maximum Brightness ◽  
New Type ◽  
The Ideal

I. IntroductionThermionic electron gun with the Wehnelt grid is popularly used in the electron microscopy and electron beam micro-fabrication. It is well known that this gun could get the ideal brightness caluculated from the Lengumier and Richardson equations under the optimum condition. However, the design and ajustment to the optimum condition is not so easy. The gun has following properties with respect to the Wehnelt bias; (1) The maximum brightness is got only in the optimum bias. (2) In the larger bias than the optimum, the brightness decreases with increasing the bias voltage on account of the space charge effect. (3) In the smaller bias than the optimum, the brightness decreases with bias voltage on account of spreading of the cross over spot due to the aberrations of the electrostatic immersion lens.In the present experiment, a new type electron gun with the electrostatic and electromagnetic lens is designed, and its properties are examined experimentally.

A new type of defect structure in 124-superconducting oxide revealed by HREM

1991 ◽  
Vol 49 ◽  
pp. 1092-1093
Author(s):  
R. Sharma ◽  
B.L. Ramakrishna ◽  
N.N. Thadhani ◽  
D. Hianes ◽  
Z. Iqbal
Keyword(s):  
Shock Wave ◽  
Defect Structure ◽  
Neutron Radiation ◽  
Weak Links ◽  
Defect Structures ◽  
New Materials ◽  
New Type ◽  
Current Densities ◽  
Processing Techniques ◽  
Microstructural Studies

After materials with superconducting temperatures higher than liquid nitrogen have been prepared, more emphasis has been on increasing the current densities (Jc) of high Tc superconductors than finding new materials with higher transition temperatures. Different processing techniques i.e thin films, shock wave processing, neutron radiation etc. have been applied in order to increase Jc. Microstructural studies of compounds thus prepared have shown either a decrease in gram boundaries that act as weak-links or increase in defect structure that act as flux-pinning centers. We have studied shock wave synthesized Tl-Ba-Cu-O and shock wave processed Y-123 superconductors with somewhat different properties compared to those prepared by solid-state reaction. Here we report the defect structures observed in the shock-processed Y-124 superconductors.

ESEM - A multipurpose surface Electron Microscope

1986 ◽  
Vol 44 ◽  
pp. 632-633 ◽  
Author(s):  
G.D. Danilatos
Keyword(s):  
Electron Microscope ◽  
Room Temperature ◽  
Environmental Scanning ◽  
Gas Composition ◽  
Saturated Water Vapor ◽  
Surface Electron ◽  
Current State ◽  
Saturated Water ◽  
New Type ◽  
Temperature And Pressure

Over recent years a new type of electron microscope - the environmental scanning electron microscope (ESEM) - has been developed for the examination of specimen surfaces in the presence of gases. A detailed series of reports on the system has appeared elsewhere. A review summary of the current state and potential of the system is presented here.The gas composition, temperature and pressure can be varied in the specimen chamber of the ESEM. With air, the pressure can be up to one atmosphere (about 1000 mbar). Environments with fully saturated water vapor only at room temperature (20-30 mbar) can be easily maintained whilst liquid water or other solutions, together with uncoated specimens, can be imaged routinely during various applications.

Trial production of γ-type energy filtering TEM

1995 ◽  
Vol 53 ◽  
pp. 604-605
Author(s):  
Y. Taniguchi ◽  
E. Nakazawa ◽  
S. Taya
Keyword(s):  
Magnetic Energy ◽  
Electron Optics ◽  
Electron Microscopic ◽  
Mass Spectrometers ◽  
Ion Optics ◽  
Energy Filtering ◽  
New Information ◽  
New Type ◽  
Fringing Fields

Imaging energy filters can add new information to electron microscopic images with respect to energy-axis, so-called electron spectroscopic imaging (ESI). Recently, many good results have been reported using this imaging technique. ESI also allows high-contrast observation of unstained biological samples, becoming a trend of the field of morphology. We manufactured a new type of energy filter as a trial production. This energy filter consists of two magnets, and we call γ-filter since the trajectory of electrons shows ‘γ’-shape inside the filter. We evaluated the new energyγ-filter TEM with the γ-filter.Figure 1 shows schematic view of the electron optics of the γ-type energy filter. For the determination of the electron-optics of the γ-type energy filter, we used the TRIO (Third Order Ion Optics) program which has been developed for the design of high resolution mass spectrometers. The TRIO takes the extended fringing fields (EFF) into consideration. EFF makes it difficult to design magnetic energy filters with magnetic sector fields.

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