scholarly journals Neutron diffraction and gravimetric study of the manganese nitriding reaction under ammonia decomposition conditions

2018 ◽  
Vol 20 (13) ◽  
pp. 8547-8553 ◽  
Author(s):  
Thomas J. Wood ◽  
Joshua W. Makepeace ◽  
William I. F. David
Keyword(s):  
Neutron Diffraction ◽  
Ammonia Decomposition ◽  
Nitriding Reaction ◽  
Kinetic Information

In situ neutron diffraction of ammonia decomposition over manganese reveals the structures of different nitrides and kinetic information about their formation.

scholarly journals Neutron diffraction and gravimetric study of the iron nitriding reaction under ammonia decomposition conditions

2017 ◽  
Vol 19 (40) ◽  
pp. 27859-27865 ◽  
Author(s):  
Thomas J. Wood ◽  
Joshua W. Makepeace ◽  
William I. F. David
Keyword(s):  
Neutron Diffraction ◽  
Decomposition Reaction ◽  
Ammonia Decomposition ◽  
Nitriding Reaction

In situ neutron diffraction of the ammonia decomposition reaction over iron shows the catalyst to be Fe or Fe4N depending on the conditions.

Determination of Internal Stresses During Pearlite Transformation of 0.8c–1.5Mn Steel Through In-Situ Neutron Diffraction

2020 ◽  
Author(s):  
Satoshi Morooka ◽  
Nobuo Nakada ◽  
Yuhki Tsukada ◽  
Wu Gong ◽  
Takuro Kawasaki ◽  
...  
Keyword(s):  
Neutron Diffraction ◽  
Internal Stresses

scholarly journals In Situ Hyperspectral Raman Imaging: A New Method to Investigate Sintering Processes of Ceramic Material at High-temperature

2019 ◽  
Vol 9 (7) ◽  
pp. 1310 ◽  
Author(s):  
Kerstin Hauke ◽  
Johannes Kehren ◽  
Nadine Böhme ◽  
Sinje Zimmer ◽  
Thorsten Geisler
Keyword(s):  
High Temperature ◽  
Raman Imaging ◽  
In Situ Studies ◽  
Kinetic Information ◽  
Novel Approach ◽  
In Situ Investigation ◽  
Dependent Growth ◽  
Micrometer Scale ◽  
Sintering Processes

In the last decades, Raman spectroscopy has become an important tool to identify and investigate minerals, gases, glasses, and organic material at room temperature. In combination with high-temperature and high-pressure devices, however, the in situ investigation of mineral transformation reactions and their kinetics is nowadays also possible. Here, we present a novel approach to in situ studies for the sintering process of silicate ceramics by hyperspectral Raman imaging. This imaging technique allows studying high-temperature solid-solid and/or solid-melt reactions spatially and temporally resolved, and opens up new avenues to study and visualize high-temperature sintering processes in multi-component systems. After describing in detail the methodology, the results of three application examples are presented and discussed. These experiments demonstrate the power of hyperspectral Raman imaging for in situ studies of the mechanism(s) of solid-solid or solid-melt reactions at high-temperature with a micrometer-scale resolution as well as to gain kinetic information from the temperature- and time-dependent growth and breakdown of minerals during isothermal or isochronal sintering.

scholarly journals Temperature Dependence of Electrical Properties and Crystal Structure of 0.29Pb(In1/2Nb1/2)O3–0.44Pb(Mg1/3Nb2/3)O3–0.27PbTiO3Single Crystals

2013 ◽  
Vol 2013 ◽  
pp. 1-5
Author(s):  
Qian Li ◽  
Yun Liu ◽  
Andrew Studer ◽  
Zhenrong Li ◽  
Ray Withers ◽  
...  
Keyword(s):  
Crystal Structure ◽  
Phase Transition ◽  
Electrical Properties ◽  
Dielectric Permittivity ◽  
Neutron Diffraction ◽  
Electrical Measurement ◽  
Temperature Dependent ◽  
Electromechanical Properties ◽  
Polar Order

We characterized the temperature dependent (~25–200°C) electromechanical properties and crystal structure of Pb(In1/2Nb1/2)O3-Pb(Mg1/3Nb2/3)O3-PbTiO3single crystals usingin situelectrical measurement and neutron diffraction techniques. The results show that the poled crystal experiences an addition phase transition around 120°C whereas such a transition is absent in the unpoled crystal. It is also found that the polar order persists above the maximum dielectric permittivity temperature at which the crystal shows a well-defined antiferroelectric behavior. The changes in the electrical properties and underlying crystal structure are discussed in the paper.

Study of tempering behavior of lath martensite using in situ neutron diffraction

2015 ◽  
Vol 107 ◽  
pp. 29-32 ◽  
Author(s):  
Z.M. Shi ◽  
W. Gong ◽  
Y. Tomota ◽  
S. Harjo ◽  
J. Li ◽  
...  
Keyword(s):  
Neutron Diffraction ◽  
Lath Martensite ◽  
In Situ Neutron Diffraction

In situ neutron diffraction study of fatigue behavior of CrFeCoNiMo0.2 high entropy alloy

2021 ◽  
Vol 139 ◽  
pp. 107371
Author(s):  
Haiyan He ◽  
Bing Wang ◽  
Dong Ma ◽  
Alexandru D. Stoica ◽  
Zhenduo Wu ◽  
...  
Keyword(s):  
Neutron Diffraction ◽  
Diffraction Study ◽  
Fatigue Behavior ◽  
Neutron Diffraction Study ◽  
High Entropy Alloy ◽  
High Entropy ◽  
In Situ Neutron Diffraction
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