The preparation of sub-micron spherical Fe-Ph/Cl-20 by the spray-drying method and its combustion

RSC Advances ◽  
2016 ◽  
Vol 6 (116) ◽  
pp. 115303-115307
Author(s):  
Nai-Meng Song ◽  
Rui-Yi Gan ◽  
Wen-Yuan Zhao ◽  
Guo-Ying Zhang ◽  
Li Yang
Keyword(s):  
Spray Drying ◽  
Spherical Shape ◽  
Composite Particles ◽  
Drying Method ◽  
Drying Technology

This study introduces the preparation of sub-micron composite particles of phloroglucinol-Fe and Cl-20 (Fe-Ph/Cl-20) with a spherical shape using spray drying technology.

Effect of Several Factors on the Synthesis of Calcium Hydroxide Prepared by Spray Drying Method Using Limestone

2007 ◽  
Vol 544-545 ◽  
pp. 733-736
Author(s):  
Moon Kwan Choi ◽  
Jin Sang Cho ◽  
Sung Min Joo ◽  
Jin Koo Park ◽  
Ji Whan Ahn ◽  
...  
Keyword(s):  
Particle Size ◽  
Calcium Carbonate ◽  
Spray Drying ◽  
Feeding Rate ◽  
Spherical Shape ◽  
Initial Reaction ◽  
Outlet Temperature ◽  
Drying Method ◽  
Precipitated Calcium Carbonate ◽  
Carbonation Process

The purpose of this work is to influence of CaO concentrations of 5.0 wt.% and 10.0 wt.%, slurry feeding rate of 200~400 /min, rotating rate of drum of 5,000 and 10,000 rpm, inlet and outlet temperature on the synthesis of Ca(OH)2 powder, and the synthesis of precipitated calcium carbonate by carbonation process using Ca(OH)2 prepared by spray drying method. As the feeding rate of slurry was increased, the particle size of Ca(OH)2 was decreased. Regardless of rotating rate of drum, when the concentration of CaO was 5.0 wt.% and 10.0 wt.%, the morphology of Ca(OH)2 showed spherical shape of 10~30 μm and 20~60 μm, respectively. The specific surface area of synthesized Ca(OH)2 was 27~30 m2/g. When the initial reaction temperature was 11 °C and 30 °C, the shape and particle size of precipitated calcium carbonate synthesized in the carbonation process showed the rectangular shape of 0.1~0.4 μm and the spindle shape of 0.5~1.0 μm, respectively.

scholarly journals Microencapsulation of Pineapple Peel Extract by Spray Drying Using Maltodextrin, Inulin, and Arabic Gum as Wall Matrices

Foods ◽  
2020 ◽  
Vol 9 (6) ◽  
pp. 718 ◽  
Author(s):  
Sofia C. Lourenço ◽  
Margarida Moldão-Martins ◽  
Vítor D. Alves
Keyword(s):  
Antioxidant Activity ◽  
Phenolic Compounds ◽  
Spray Drying ◽  
Spherical Shape ◽  
Large Degree ◽  
Wall Material ◽  
Arabic Gum ◽  
Hausner Ratio ◽  
Pineapple Peel ◽  
Drying Technology

A pineapple peel hydroalcoholic extract rich in phenolic compounds, was stabilized by microencapsulation using spray drying technology, with maltodextrin, inulin, and arabic gum as wall materials. The influence of the type of wall material and drying temperature (150 and 190 °C) on the particles properties was studied. The particles presented a spherical shape with a diameter ranging from approximately 1.3 to 18.2 µm, the exception being the ones with inulin that showed a large degree of agglomeration. All powders produced presented an intermediate cohesiveness and a fair to good flowability according to Carr index and Hausner ratio, which envisages suitable handling properties at an industrial scale. The microencapsulation processes using maltodextrin and arabic gum at 150 °C were the ones that showed higher maintenance of the antioxidant activity of compounds present in the extract before encapsulation during spray drying. In addition, the microparticles obtained were quite efficient in stabilizing the encapsulated phenolic compounds, as their antioxidant activity did not change significantly during six months of storage at 5 °C.

scholarly journals CURCUMIN MICROENCAPSULATION USING CHITOSAN–ETHYL CELLULOSE–GMS MIXTURE FOR PRESERVATION OF MUCOADHESIVE PROPERTIES AND CONTROLLED RELEASE KINETIC

2022 ◽  
pp. 288-294
Author(s):  
DENI RAHMAT ◽  
YUNAHARA FARIDA ◽  
NOVI YANTIH ◽  
GITA SEPTYANA DEWI ◽  
SARAH ANGELA PURNAMA
Keyword(s):  
Particle Size ◽  
Water Content ◽  
Spray Drying ◽  
Spherical Shape ◽  
Release Kinetic ◽  
Drying Method ◽  
Solid Dosage Forms ◽  
Solid Dosage ◽  
Better Than

Objective: This research aimed to prepare curcumin microcapsules by the spray drying method and to evaluate their characteristics. Methods: The microcapsules were prepared by the spray drying method. The generated microcapsules were evaluated for organoleptic, morphology, particle size, the percentage of curcumin and water content. Furthermore, the release of curcumin from the microcapsules was tested in vitro and compared to uncoated curcumin powder. In addition, the mucoadhesive properties of uncoated curcumin powder and curcumin microcapsules were also evaluated. Results: The results showed that the microcapsules had spherical shape with particle size in the range of 100–1009 µm and water content of 9.34% (w/w) (FIII) and 8.09% (w/w) (FVI). The release of curcumin from its uncoated powder and the microcapsules FVI within 8 h were 8.87% and 26.32% (w/w), respectively. It was found that the mucoadhesive properties of microcapsules FVI were better than those of FIII and uncoated curcumin powder. Microcapsules FVI rendered the cumulative amount of curcumin remaining on the intestinal mucosa of 55% (w/w) within 3 h. Conclusion: Accordingly, curcumin microcapsules generated by spray drying could be further formulated into various solid dosage forms for a better therapeutic effect.

scholarly journals Preparation, High-Density Spherical, and Low Sensitivity of RDX/NC/PMMA Composite Particles

2021 ◽  
Vol 2021 ◽  
pp. 1-8
Author(s):  
Xinlei Jia ◽  
Wenshan Peng ◽  
Lanjuan Xu ◽  
Qing Cao ◽  
Shaohua Xing ◽  
...  
Keyword(s):  
Spray Drying ◽  
High Energy ◽  
Safety Performance ◽  
Spherical Particles ◽  
Core Material ◽  
Composite Particles ◽  
Drying Method ◽  
X Ray Diffraction ◽  
Low Sensitivity ◽  
Friction Sensitivity

In order to reduce the mechanical sensitivity of cyclotrimethylenetrinitramine (RDX) and improve its energy density, spherical RDX/PMMA/NC composite particles were prepared by spray drying method, selecting polymethyl methacrylate (PMMA, hydrocarbon binder) with excellent mechanical properties and nitrocellulose (NC, energy-containing binder) with higher density as the desensitizing shell material, RDX as the core material. PMMA/NC composite particles of the same component were prepared by a simple solvent evaporation method at the same time. Structural characterizations and thermal stability of the composites were systematically studied by scanning electron microscopy (SEM), X-ray diffraction (XRD), and differential scanning calorimeter (DSC), respectively. Moreover, the safety performance has been qualitatively tested and analyzed through impact sensitivity and friction sensitivity. The results show that the addition of NC/PMMA binder would not change the original crystal structure of RDX, and the RDX/NC/PMMA composites fabricated by spray drying presented spherical particles with uniform distribution and smooth surface. The Tp0 of RDX/NC/PMMA composite particles increased from 220.3°C to 228.2°C, improving the thermal decomposition performance. The H50 rose from 29.32 cm to 84.3 cm, and the probability of friction explosion decreased from 96% to 8%, significantly enhancing the safety performance. In short, the RDX/NC/PMMA composites prepared via the spray drying method and the improvement of their performance have positive significance for the development of explosives in pursuit of high energy and low sensitivity.

scholarly journals Preparation of LiFePO4 Powders by Ultrasonic Spray Drying Method and Their Memory Effect

Materials ◽  
2021 ◽  
Vol 14 (12) ◽  
pp. 3193
Author(s):  
Tu Lan ◽  
Xiaolong Guo ◽  
De Li ◽  
Yong Chen
Keyword(s):  
Spray Drying ◽  
Memory Effect ◽  
Electrode Materials ◽  
Average Particle Size ◽  
Lithium Ion ◽  
Average Particle ◽  
Preparation Process ◽  
Drying Method ◽  
Drying Temperature ◽  
Ultrasonic Spray

The memory effect of lithium-ion batteries (LIBs) was first discovered in LiFePO4, but its origin and dependence are still not clear, which is essential for regulating the memory effect. In this paper, a home-made spray drying device was used to successfully synthesize LiFePO4 with an average particle size of about 1 μm, and we studied the influence of spray drying temperature on the memory effect of LiFePO4 in LIBs. The results showed that the increasing of spray drying temperature made the memory effect of LiFePO4 strengthen from 1.3 mV to 2.9 mV, while the capacity decreased by approximately 6%. The XRD refinement and FTIR spectra indicate that the enhancement of memory effect can be attributed to the increment of Li–Fe dislocations. This work reveals the dependence of memory effect of LiFePO4 on spray drying temperature, which will guide us to optimize the preparation process of electrode materials and improve the management system of LIBs.

scholarly journals Numerical Study toward Optimization of Spray Drying in a Novel Radial Multizone Dryer

Energies ◽  
2021 ◽  
Vol 14 (5) ◽  
pp. 1233
Author(s):  
Umair Jamil Ur Rahman ◽  
Artur Krzysztof Pozarlik ◽  
Thomas Tourneur ◽  
Axel de Broqueville ◽  
Juray De Wilde ◽  
...  
Keyword(s):  
Spray Drying ◽  
Droplet Size ◽  
Separation Efficiency ◽  
Numerical Study ◽  
Three Dimensional ◽  
Droplet Size Distribution ◽  
Vortex Chamber ◽  
Temperature Pattern ◽  
Multiphase Model ◽  
Drying Technology

In this paper, an intensified spray-drying process in a novel Radial Multizone Dryer (RMD) is analyzed by means of CFD. A three-dimensional Eulerian–Lagrangian multiphase model is applied to investigate the effect of solids outlet location, relative hot/cold airflow ratio, and droplet size on heat and mass transfer characteristics, G-acceleration, residence time, and separation efficiency of the product. The results indicate that the temperature pattern in the dryer is dependent on the solids outlet location. A stable, symmetric spray behavior with maximum evaporation in the hot zone is observed when the solids outlet is placed at the periphery of the vortex chamber. The maximum product separation efficiency (85 wt %) is obtained by applying high G-acceleration (at relative hot/cold ratio of 0.75) and narrow droplet size distribution (45–70 µm). The separation of different sized particles with distinct drying times is also observed. Smaller particles (<32 µm) leave the reactor via the gas outlet, while the majority of big particles leave it via the solids outlet, thus depicting in situ particle separation. The results revealed the feasibility and benefits of a multizone drying operation and that the RMD can be an attractive solution for spray drying technology.

scholarly journals Preparation of Ce-doped yttrium aluminum garnet phosphor particles using spray drying method

2020 ◽  
pp. 1-8
Author(s):  
Shao-Ju Shih ◽  
Lewi Peter Richardo ◽  
Kevin Indrawan Sucipto ◽  
Zhi-Meng Wang
Keyword(s):  
Spray Drying ◽  
Yttrium Aluminum Garnet ◽  
Drying Method ◽  
Yttrium Aluminum

Solid dispersion particles of tolbutamide prepared with fine silica particles by the spray-drying method

2004 ◽  
Vol 141 (3) ◽  
pp. 187-195 ◽  
Author(s):  
Hirofumi Takeuchi ◽  
Shinsuke Nagira ◽  
Hiromitsu Yamamoto ◽  
Yoshiaki Kawashima
Keyword(s):  
Spray Drying ◽  
Solid Dispersion ◽  
Silica Particles ◽  
Drying Method
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