scholarly journals Oscillatory behaviour of the surface reduction process of multilayer graphene oxide at room temperature

RSC Advances ◽  
2016 ◽  
Vol 6 (81) ◽  
pp. 78194-78201 ◽  
Author(s):  
D. N. Voylov ◽  
I. N. Ivanov ◽  
V. I. Bykov ◽  
S. B. Tsybenova ◽  
I. A. Merkulov ◽  
...  
Keyword(s):  
Graphene Oxide ◽  
Redox Reactions ◽  
Room Temperature ◽  
Reduction Process ◽  
Multilayer Graphene ◽  
Oscillatory Behaviour ◽  
Surface Reduction

We report the observation of oscillatory redox reactions on the surface of multilayer graphene oxide (GO) films at room temperature.

Room temperature reduction of multilayer graphene oxide film on a copper substrate: Penetration and participation of copper phase in redox reactions

Carbon ◽  
2014 ◽  
Vol 69 ◽  
pp. 563-570 ◽  
Author(s):  
Dmitry N. Voylov ◽  
Alexander L. Agapov ◽  
Alexei P. Sokolov ◽  
Yuri M. Shulga ◽  
Artem A. Arbuzov
Keyword(s):  
Graphene Oxide ◽  
Oxide Film ◽  
Redox Reactions ◽  
Room Temperature ◽  
Copper Substrate ◽  
Multilayer Graphene ◽  
Temperature Reduction ◽  
Copper Phase

scholarly journals Room-temperature metastability of multilayer graphene oxide films

2012 ◽  
Vol 11 (6) ◽  
pp. 544-549 ◽  
Author(s):  
Suenne Kim ◽  
Si Zhou ◽  
Yike Hu ◽  
Muge Acik ◽  
Yves J. Chabal ◽  
...  
Keyword(s):  
Graphene Oxide ◽  
Room Temperature ◽  
Oxide Films ◽  
Multilayer Graphene

Green synthesis of mixed metallic nanoparticles using room temperature self-assembly

2017 ◽  
Vol 13 (2) ◽  
pp. 4671-4677 ◽  
Author(s):  
A. M. Abdelghany ◽  
A.H. Oraby ◽  
Awatif A Hindi ◽  
Doaa M El-Nagar ◽  
Fathia S Alhakami
Keyword(s):  
Self Assembly ◽  
Metallic Nanoparticles ◽  
Room Temperature ◽  
Bimetallic Nanoparticles ◽  
Reduction Process ◽  
Nano Particles ◽  
Nano Structure ◽  
Small Shift ◽  
Molar Ratios ◽  
Vis Spectroscopy

Bimetallic nanoparticles of silver (Ag) and gold (Au) were synthesized at room temperature using Curcumin. Reduction process of silver and gold ions with different molar ratios leads to production of different nanostructures including alloys and core-shells. Produced nanoparticles were characterized simultaneously with FTIR, UV/vis. spectroscopy, transmission electron microscopy (TEM), and Energy-dispersive X-ray (EDAX). UV/vis. optical absorption spectra of as synthesized nanoparticles reveals presence of surface palsmon resonance (SPR) of both silver at (425 nm) and gold at (540 nm) with small shift and broadness of gold band after mixing with resucing and capping agent in natural extract which suggest presence of bimetallic nano structure (Au/Ag). FTIR and EDAX data approve the presence of bimetallic nano structure combined with curcumin extract. TEM micrographs shows that silver and gold can be synthesized separately in the form of nano particles using curcumin extract. Synthesis of gold nano particles in presence of silver effectively enhance and control formation of bi-metallic structure.

scholarly journals Magnetization of Ultraviolet-Reduced Graphene Oxide Flakes in Composites Based on Polystyrene

Materials ◽  
2021 ◽  
Vol 14 (10) ◽  
pp. 2519
Author(s):  
Alexander N. Ionov ◽  
Mikhail P. Volkov ◽  
Marianna N. Nikolaeva ◽  
Ruslan Y. Smyslov ◽  
Alexander N. Bugrov
Keyword(s):  
Graphene Oxide ◽  
Reduced Graphene Oxide ◽  
Reduction Process ◽  
X Ray Diffraction ◽  
Mesoscopic Structure ◽  
Reduced Graphene ◽  
Study Results ◽  
Edge Defects ◽  
Mesoscopic Level ◽  
Ferromagnetic Hysteresis

This work presents our study results of the magnetization of multilayer UV-reduced graphene oxide (UV-rGO), polymer matrix (polystyrene), and a conjugated composite based on them. The mesoscopic structure of the composites synthesized in this work was studied by such methods as X-ray diffraction, SEM, as well as NMR-, IR- and Raman spectroscopy. The magnetization of the composites under investigation and their components was measured using a vibrating-sample magnetometer. It has been shown that the UV-reduction process leads to the formation of many submicron holes distributed inside rGO flakes, which can create edge defects, causing possibly magnetic order in the graphite samples under investigation on the mesoscopic level. This article provides an alternative explanation for the ferromagnetic hysteresis loop in UV-rGO on the base of superconductivity type-II.

Polyaniline-Reduced Graphene Oxide Nanosheets for Room Temperature NH3 Detection

2021 ◽  
Author(s):  
Junyu Chang ◽  
Xiaobo Zhang ◽  
Zhenming Wang ◽  
Chunsheng Li ◽  
Qi Hu ◽  
...  
Keyword(s):  
Graphene Oxide ◽  
Reduced Graphene Oxide ◽  
Room Temperature ◽  
Graphene Oxide Nanosheets ◽  
Reduced Graphene

scholarly journals High-Tribological-Performance Polymer Nanocomposites: An Approach Based on the Superlubricity State of the Graphene Oxide Agglomerates

Polymers ◽  
2021 ◽  
Vol 13 (14) ◽  
pp. 2237
Author(s):  
Eder H. C. Ferreira ◽  
Angela Aparecida Vieira ◽  
Lúcia Vieira ◽  
Guilhermino J. M. Fechine
Keyword(s):  
Graphene Oxide ◽  
High Viscosity ◽  
Tribological Performance ◽  
Multilayer Graphene ◽  
High Concentration ◽  
Scanning Calorimetry ◽  
Mechanical Reinforcement ◽  
Transmission Electron ◽  
Twin Screw ◽  
Mechanical Tensile

Here, nanocomposites of high-molecular-weight polyethylene (HMWPE) and HMWPE-UHMWPE (80/20 wt.%) containing a low amount of multilayer graphene oxide (mGO) (≤0.1 wt.%) were produced via twin-screw extrusion to produce materials with a higher tribological performance than UHMWPE. Due to the high viscosity of both polymers, the nanocomposites presented a significant concentration of agglomerates. However, the mechanical (tensile) and tribological (volumetric loss) performances of the nanocomposites were superior to those of UHMWPE. The morphology of the nanocomposites was investigated using differential scanning calorimetry (DSC), microtomography, and transmission electron microscopy (TEM). The explanation for these results is based on the superlubricity phenomenon of mGO agglomerates. It was also shown that the well-exfoliated mGO also contained in the nanocomposite was of fundamental importance as a mechanical reinforcement for the polymer. Even with a high concentration of agglomerates, the nanocomposites displayed tribological properties superior to UHMWPE’s (wear resistance up to 27% higher and friction coefficient up to 57% lower). Therefore, this manuscript brings a new exception to the rule, showing that agglomerates can act in a beneficial way to the mechanical properties of polymers, as long as the superlubricity phenomenon is present in the agglomerates contained in the polymer.

scholarly journals Graphene oxide prepared by a room temperature oxidation using a green mechanochemical method.

2021 ◽  
Vol 27 (S1) ◽  
pp. 726-728
Author(s):  
G. Tarango-Rivero ◽  
G. Herrera-Perez ◽  
C. Carreño-Gallardo ◽  
C.G. Garay-Reyes ◽  
I. Estrada-Guel ◽  
...  
Keyword(s):  
Graphene Oxide ◽  
Room Temperature ◽  
Mechanochemical Method ◽  
Temperature Oxidation
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