Facile one-pot solvent-free synthesis of hierarchical ZSM-5 for methanol to gasoline conversion

RSC Advances ◽  
2016 ◽  
Vol 6 (19) ◽  
pp. 15816-15820 ◽  
Author(s):  
Ziyu Liu ◽  
Dan Wu ◽  
Shu Ren ◽  
Xinqing Chen ◽  
Minghuang Qiu ◽  
...  
Keyword(s):  
Surface Area ◽  
High Surface ◽  
High Surface Area ◽  
Solvent Free ◽  
Acidic Properties ◽  
One Pot ◽  
High Crystallinity ◽  
Methanol To Gasoline ◽  
Solvent Free Synthesis

A hierarchical ZSM-5 zeolite with high crystallinity, high surface area, adjustable Si/Al ratio and suitable acidic properties was synthesized by a one-pot solvent-free method.

A high surface area tunnel-type α-MnO2 nanorod cathode by a simple solvent-free synthesis for rechargeable aqueous zinc-ion batteries

2016 ◽  
Vol 650 ◽  
pp. 64-68 ◽  
Author(s):  
Muhammad Hilmy Alfaruqi ◽  
Saiful Islam ◽  
Jihyeon Gim ◽  
Jinju Song ◽  
Sungjin Kim ◽  
...  
Keyword(s):  
Surface Area ◽  
High Surface ◽  
High Surface Area ◽  
Zinc Ion ◽  
Solvent Free ◽  
Solvent Free Synthesis

Solvent-free synthesis of crystalline mesoporous γ-Fe2O3 as an anode material in lithium-ion batteries

RSC Advances ◽  
2016 ◽  
Vol 6 (62) ◽  
pp. 57009-57012 ◽  
Author(s):  
Di Wu ◽  
Jing Ye ◽  
Lie Chen ◽  
Yongzheng Wang ◽  
Kai Fang ◽  
...  
Keyword(s):  
Lithium Ion Batteries ◽  
Surface Area ◽  
Anode Material ◽  
High Surface ◽  
High Surface Area ◽  
Lithium Ion ◽  
Solvent Free ◽  
Lithium Ions ◽  
Solvent Free Synthesis

As an advanced anode material for lithium ions batteries, crystalline mesoporous γ-Fe2O3 with a high surface area was prepared by a novel solvent-free route.

Solvent-free synthesis of a porous thiophene polymer by mechanochemical oxidative polymerization

2018 ◽  
Vol 6 (44) ◽  
pp. 21901-21905 ◽  
Author(s):  
S. Grätz ◽  
M. Oltermann ◽  
E. Troschke ◽  
S. Paasch ◽  
S. Krause ◽  
...  
Keyword(s):  
Surface Area ◽  
Ball Mill ◽  
Oxidative Polymerization ◽  
High Surface ◽  
High Surface Area ◽  
Solvent Free ◽  
Porous Polymer ◽  
Polymerization Reaction ◽  
Free Environment ◽  
Solvent Free Synthesis

An oxidative polymerization reaction was brought into the solvent-free environment of a ball mill, yielding a porous polymer with a defined structure and high surface area.

scholarly journals Dopamine Assisted One-Step Pyrolysis of Glucose for the Preparation of Porous Carbon with A High Surface Area

Nanomaterials ◽  
2018 ◽  
Vol 8 (10) ◽  
pp. 854 ◽  
Author(s):  
Hanbo Xiao ◽  
Cheng-an Tao ◽  
Yujiao Li ◽  
Xianzhe Chen ◽  
Jian Huang ◽  
...  
Keyword(s):  
Surface Area ◽  
Porous Carbon ◽  
Carbon Materials ◽  
High Current Density ◽  
High Surface ◽  
High Surface Area ◽  
Energy Storage Materials ◽  
One Pot ◽  
Component Structure ◽  
Porous Carbon Materials

Herein, a facile dopamine assisted one-pot synthesis approach is proposed for the preparation of porous carbon with a specific surface area (SSA) up to 2593 m2/g through the direct pyrolysis of a mixture of glucose, NH4Cl, and dopamine hydrochloride (DAH). The glucose is adopted as the carbon source and foaming agent, NH4Cl is used as the blowing agent, and DAH is served as collaborative carbon precursor as well as the nitrogen source for the first time. The effect of dopamine on the component, structure, and SSA of the as-prepared porous carbon materials are systematically studied. The moderate addition of dopamine, which influences the condensation and polymerization of glucose, matches better with ammonium salt decomposition. The SSA of porous carbon increases first and then decreases with the increasing amount of dopamine. In our case, the porous carbon produced with 5 wt% dopamine (PC-5) achieves the maximum SSA of up to 2593 m2/g. Accordingly, it also shows the greatest electrochemical performance. The PC-5 shows a capacitance of 96.7 F/g calculated from the discharge curve at 1 A/g. It also has a good capacitive rate capacity, the specific capacitance can still maintain 80%, even at a high current density of 10 A/g. Moreover, PC-5 exhibits a good cycling stability of 98.1% capacitive retention after 1000 cycles. The proposed method may show promising prospects for preparing porous carbon materials as advanced energy storage materials, storage, and catalyst supports.

scholarly journals Impact of Thermal Treatment of Nb2O5 on Its Performance in Glucose Dehydration to 5-Hydroxymethylfurfural in Water

Nanomaterials ◽  
2020 ◽  
Vol 10 (9) ◽  
pp. 1685
Author(s):  
Katarzyna Morawa Eblagon ◽  
Anna Malaika ◽  
Karolina Ptaszynska ◽  
Manuel Fernando R. Pereira ◽  
José Luís Figueiredo
Keyword(s):  
Thermal Treatment ◽  
Surface Area ◽  
Pure Water ◽  
High Surface ◽  
High Surface Area ◽  
Acid Sites ◽  
High Ratio ◽  
Total Acidity ◽  
One Pot ◽  
Niobic Acid

The cascade dehydration of glucose to 5-hydroxymethylfurfural (HMF) was carried out in water over a series of Nb2O5 catalysts, which were derived from the thermal treatment of niobic acid at 300 and 550 °C, under air or inert atmosphere. Amorphous niobic acid showed high surface area (366 m2/g) and large acidity (2.35 mmol/g). With increasing the temperature of the thermal treatment up to 550 °C, the amorphous Nb2O5 was gradually transformed into a pseudohexagonal phase, resulting in a decrease in surface area (27–39 m2/g) and total acidity (0.05–0.19 mmol/g). The catalysts’ performance in cascade dehydration of glucose realized in pure water was strongly influenced by the total acidity of these materials. A remarkable yield of 37% HMF in one-pot reaction in water was achieved using mesoporous amorphous niobium oxide prepared by thermal treatment of niobic acid at 300 °C in air. The best-performing catalyst displayed a total acidity lower than niobic acid (1.69 mmol/g) which afforded a correct balance between a high glucose conversion and limited further conversion of the target product to numerous polymers and humins. On the other hand, the treatment of niobic acid at 550 °C, independently of the atmosphere used during the sample preparation (i.e., air or N2), resulted in Nb2O5 catalysts with a high ratio of Lewis to Brønsted acid sites and poor total acidity. These materials excelled at catalyzing the isomerization step in the tandem process.

One-pot aerobic oxidative sulfonamidation of aromatic thiols with ammonia by a dual-functional β-MnO2 nanocatalyst

2020 ◽  
Vol 56 (14) ◽  
pp. 2095-2098 ◽  
Author(s):  
Eri Hayashi ◽  
Yui Yamaguchi ◽  
Yusuke Kita ◽  
Keigo Kamata ◽  
Michikazu Hara
Keyword(s):  
High Activity ◽  
Surface Area ◽  
High Surface ◽  
High Surface Area ◽  
One Pot ◽  
Dual Functional ◽  
Aromatic Thiols ◽  
The One

High-surface-area β-MnO2 nanoparticles exhibited high activity for the one-pot oxidative sulfonamidation of thiols to sulfonamides using O2 and NH3.

Porous solid acid with high Surface area derived from emulsion templating and hypercrosslinking for efficient one-pot conversion of cellulose to 5-hydroxymethylfurfural

RSC Advances ◽  
2014 ◽  
Vol 4 (103) ◽  
pp. 59175-59184 ◽  
Author(s):  
Jianming Pan ◽  
Heping Gao ◽  
Yunlei Zhang ◽  
Jun Zeng ◽  
Weidong Shi ◽  
...  
Keyword(s):  
Surface Area ◽  
Solid Acid ◽  
High Surface ◽  
High Surface Area ◽  
Porous Solid ◽  
One Pot ◽  
Emulsion Templating

This work addressed efficient one-pot conversion of cellulose to 5-hydroxymethylfurfural by porous solid acid in the presence of [Emim]Cl.

One-Pot Procedure to Synthesize High Surface Area Alumina Nanofibers Using Supercritical Carbon Dioxide

Langmuir ◽  
2010 ◽  
Vol 26 (4) ◽  
pp. 2707-2713 ◽  
Author(s):  
Muhammad B. I. Chowdhury ◽  
Rouhong Sui ◽  
Rahima A. Lucky ◽  
Paul A. Charpentier
Keyword(s):  
Carbon Dioxide ◽  
Supercritical Carbon Dioxide ◽  
Surface Area ◽  
High Surface ◽  
High Surface Area ◽  
One Pot ◽  
Alumina Nanofibers ◽  
Supercritical Carbon
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