New way to multi-shelled hollow spheres for robust battery electrode

2016 ◽  
Vol 3 (8) ◽  
pp. 1004-1006 ◽  
Author(s):  
Hong Jin Fan
Keyword(s):  
Adsorption Mechanism ◽  
Hollow Spheres ◽  
Hollow Microspheres ◽  
Anion Adsorption ◽  
New Synthesis ◽  
Battery Electrode ◽  
Synthesis Approach

The new synthesis approach towards multi-shelled hollow microspheres based on an anion adsorption mechanism is highlighted.

Electrochemical performance and electronic properties of shell LiNi0.5Mn1.5O4 hollow spheres for lithium ion battery

2016 ◽  
Vol 09 (02) ◽  
pp. 1650027 ◽  
Author(s):  
Yongli Cui ◽  
Jiali Wang ◽  
Mingzhen Wang ◽  
Quanchao Zhuang
Keyword(s):  
Activation Energy ◽  
Electrochemical Performance ◽  
Electronic Properties ◽  
Lithium Ion Battery ◽  
Retention Rate ◽  
Hollow Spheres ◽  
Lithium Ion ◽  
Reversible Capacity ◽  
Hollow Microspheres ◽  
Cycle Stability

Shell spinel LiNi[Formula: see text]Mn[Formula: see text]O4 hollow microspheres were successfully synthesized by MnCO3 template, and characterized by XRD, SEM, and TEM. The results show that the hollow LiNi[Formula: see text]Mn[Formula: see text]O4 cathode has good cycle stability to reach 124.5, 119.8, and 96.6[Formula: see text]mAh/g at 0.5, 1, and 5 C, the corresponding retention rate of 98.1%, 98.2%, and 98.0% after 50 cycles at 20[Formula: see text]C, and the reversible capacity of 94.6[Formula: see text]mAh/g can be obtained at 1 C rate at 55[Formula: see text]C, 83.3% retention after 100 cycles. As the temperature decreases from 10[Formula: see text]C to [Formula: see text]C, the resistance of [Formula: see text] increases from 5.5 [Formula: see text] to 135 [Formula: see text], [Formula: see text] from 27 [Formula: see text] to 353.2 [Formula: see text], and [Formula: see text] from 12.7 [Formula: see text] to 73.0 [Formula: see text]. Moreover, the B constant and [Formula: see text] activation energy are 4480[Formula: see text]K and 37.22[Formula: see text]KJ/mol for the NTC spinel material, respectively.

Hierarchical flower-like Bi2WO6 hollow microspheres: facile synthesis and excellent catalytic performance

RSC Advances ◽  
2015 ◽  
Vol 5 (29) ◽  
pp. 23080-23085 ◽  
Author(s):  
Peigen Zhang ◽  
Jian Zhang ◽  
Anjian Xie ◽  
Shikuo Li ◽  
Jiming Song ◽  
...  
Keyword(s):  
Hollow Spheres ◽  
Catalytic Performance ◽  
Hollow Microspheres ◽  
Solvothermal Process ◽  
Facile Synthesis ◽  
Step Method ◽  
Bismuth Tungstate ◽  
One Step ◽  
Excellent Catalytic Performance

A one step method has been developed for the fabrication of hierarchical flower-like bismuth tungstate (Bi2WO6) hollow spheres via a solvothermal process.

Superhydrophobic, highly adhesive arrays of copper hollow spheres produced by electro-colloidal lithography

Soft Matter ◽  
2017 ◽  
Vol 13 (33) ◽  
pp. 5500-5505 ◽  
Author(s):  
Damien Bazin ◽  
Chrystel Faure
Keyword(s):  
Chemical Modification ◽  
Electric Fields ◽  
Hollow Spheres ◽  
Hollow Microspheres ◽  
Colloidal Lithography ◽  
Adhesive Properties

Arrays of copper hollow microspheres produced under electric fields display anti-wetting and super-adhesive properties without resorting to any chemical modification.

A novel electrochemical immunoassay for carcinoembryonic antigen based on glucose oxidase-encapsulated nanogold hollow spheres with a pH meter readout

The Analyst ◽  
2018 ◽  
Vol 143 (21) ◽  
pp. 5271-5277 ◽  
Author(s):  
Yu Jiang ◽  
Zhiying Su ◽  
Jian Zhang ◽  
Meijiao Cai ◽  
Lili Wu
Keyword(s):  
Carcinoembryonic Antigen ◽  
Glucose Oxidase ◽  
Signal Amplification ◽  
Hollow Spheres ◽  
Electrochemical Immunosensor ◽  
Hollow Microspheres ◽  
Electrochemical Immunoassay

A portable electrochemical immunosensor was designed for the detection of CEA on a pH meter by using glucose oxidase-encapsulated gold hollow microspheres for signal amplification.

Improved Dispersion and Ultradeep Activity of HDS Catalyst by New Synthesis Approach

2019 ◽  
Vol 4 (1) ◽  
pp. 370-377 ◽  
Author(s):  
Saheed A. Ganiyu ◽  
Syed Ahmed Ali ◽  
Khalid Alhooshani
Keyword(s):  
New Synthesis ◽  
Synthesis Approach

Study on a New Synthesis Approach of Glyphosate

2012 ◽  
Vol 60 (25) ◽  
pp. 6279-6285 ◽  
Author(s):  
Ji Zhou ◽  
Jian Li ◽  
Ran An ◽  
Hua Yuan ◽  
Faquan Yu
Keyword(s):  
New Synthesis ◽  
Synthesis Approach

scholarly journals Facile Synthesis and Photocatalytic Property of Titania/Carbon Composite Hollow Microspheres with Bimodal Mesoporous Shells

2012 ◽  
Vol 2012 ◽  
pp. 1-9 ◽  
Author(s):  
Guohong Wang ◽  
Bei Cheng ◽  
Jun Zhang ◽  
Lin Xu ◽  
Tingting Yin
Keyword(s):  
Aqueous Solution ◽  
Photocatalytic Activity ◽  
Hollow Spheres ◽  
Photocatalytic Property ◽  
Nitrogen Adsorption ◽  
Carbon Composite ◽  
Hollow Microspheres ◽  
Calcination Time ◽  
One Pot ◽  
Pore Structures

Titania/carbon composite hollow microspheres with bimodal mesoporous shells are one-pot fabricated by hydrothermal treatment of the acidic (NH4)2TiF6aqueous solution in the presence of glucose at180∘C for 24 h and then calcined at450∘C. The as-prepared samples were characterized by XRD, SEM, TEM, HRTEM, UV-visible spectroscopy, and nitrogen adsorption-desorption isotherms. The photocatalytic activity of the as-prepared samples was evaluated by daylight-induced photocatalytic decolorization of methyl orange aqueous solution at ambient temperature. The effects of calcination time on the morphology, phase structure, crystallite size, specific surface area, pore structures, and photocatalytic activity of the microspheres were investigated. The results indicated that the as-obtained TiO2/C composite hollow spheres generally exhibit bimodal mesopore size distribution with their peak intra-aggregated mesopore size in the range of 2.3–4.5 nm and peak interaggregated mesopore size in the range of 5.7–12.7 nm, depending on specific calcination time. The daylight-induced photoactivity of as-obtained hollow TiO2/C microspheres generally exceeds that of Degussa P25. The influences of calcination time on the photoactivity are discussed in terms of carbon content, phase structures, and pore structures.

Fabrication and Characterization of ZrO2 Hollow Spheres

2012 ◽  
Vol 512-515 ◽  
pp. 253-256
Author(s):  
Kai Liu ◽  
Sa Li ◽  
Chang An Wang
Keyword(s):  
Zirconium Dioxide ◽  
Hollow Spheres ◽  
Hollow Microspheres ◽  
Formation Mechanisms ◽  
Thermal Decomposition Process ◽  
The Core ◽  
Eds Analysis ◽  
Fabrication And Characterization ◽  
Wrapping Technique

Zirconium dioxide hollow microspheres were prepared using carbonaceous polysaccharide microspheres as a template through a heterogeneously nucleating wrapping technique. Firstly, carbonaceous microspheres wrapped by ZrO2 were synthesized, and then the obtained precursor was calcinated at 800°C for 2 hours to remove the template. Based on SEM, TEM and EDS analysis, the microstructure, composition and thermal decomposition process of the precursor as well as the final products were investigated. The formation mechanisms of the core-shell structure precursor and the hollow microspheres were also discussed.

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