Sensitivity enhanced 14N/14N correlations to probe inter-beta-sheet interactions using fast magic angle spinning solid-state NMR in biological solids

2016 ◽  
Vol 18 (32) ◽  
pp. 22583-22589 ◽  
Author(s):  
Manoj Kumar Pandey ◽  
Jean-Paul Amoureux ◽  
Tetsuo Asakura ◽  
Yusuke Nishiyama
Keyword(s):  
Solid State ◽  
Solid State Nmr ◽  
Spin Diffusion ◽  
Correlation Method ◽  
Magic Angle Spinning ◽  
Magic Angle ◽  
Beta Sheet ◽  
Biological Solids ◽  
Angle Spinning ◽  
Fast Magic Angle Spinning

Sensitivity enhanced proton-detected 14N/14N correlation method mediated through accelerated 1H–1H spin diffusion at fast magic angle spinning (MAS) solid-state NMR is demonstrated to distinguish inter-beta-sheet interactions in naturally abundant parallel and anti-parallel alanine tripeptides.

Characterization of Polymer Compatibility by1H Dipolar Filter Solid-State NMR under Fast Magic Angle Spinning

2007 ◽  
Vol 40 (25) ◽  
pp. 9018-9025 ◽  
Author(s):  
Xiaoliang Wang ◽  
Qiang Gu ◽  
Qing Sun ◽  
Dongshan Zhou ◽  
Pingchuan Sun ◽  
...  
Keyword(s):  
Solid State ◽  
Solid State Nmr ◽  
Magic Angle Spinning ◽  
Magic Angle ◽  
Polymer Compatibility ◽  
Angle Spinning ◽  
Fast Magic Angle Spinning

Very fast magic angle spinning 1H-14N 2D solid-state NMR: Sub-micro-liter sample data collection in a few minutes

2011 ◽  
Vol 208 (1) ◽  
pp. 44-48 ◽  
Author(s):  
Yusuke Nishiyama ◽  
Yuki Endo ◽  
Takahiro Nemoto ◽  
Hiroaki Utsumi ◽  
Kazuo Yamauchi ◽  
...  
Keyword(s):  
Solid State ◽  
Data Collection ◽  
Solid State Nmr ◽  
Magic Angle Spinning ◽  
Magic Angle ◽  
Sample Data ◽  
Angle Spinning ◽  
Fast Magic Angle Spinning

Homonuclear dipolar recoupling under ultra-fast magic-angle spinning: Probing 19F−19F proximities by solid-state NMR

2010 ◽  
Vol 203 (1) ◽  
pp. 113-128 ◽  
Author(s):  
Qiang Wang ◽  
Bingwen Hu ◽  
Olivier Lafon ◽  
Julien Trébosc ◽  
Feng Deng ◽  
...  
Keyword(s):  
Solid State ◽  
Solid State Nmr ◽  
Magic Angle Spinning ◽  
Magic Angle ◽  
Dipolar Recoupling ◽  
Angle Spinning ◽  
Fast Magic Angle Spinning

Tracking the interdiffusion of polymers at a molecular level by1H dipolar filter solid-state NMR under fast magic angle spinning

Soft Matter ◽  
2011 ◽  
Vol 7 (2) ◽  
pp. 691-697 ◽  
Author(s):  
Qiang Gu ◽  
Xiaoliang Wang ◽  
Pingchuan Sun ◽  
Dongshan Zhou ◽  
Gi Xue
Keyword(s):  
Solid State ◽  
Solid State Nmr ◽  
Molecular Level ◽  
Magic Angle Spinning ◽  
Magic Angle ◽  
Angle Spinning ◽  
Fast Magic Angle Spinning
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