15N spin diffusion rate in solid-state NMR of totally enriched proteins: The magic angle spinning frequency effect

2006 ◽  
Vol 182 (2) ◽  
pp. 339-342 ◽  
Author(s):  
Alexey Krushelnitsky ◽  
Thomas Bräuniger ◽  
Detlef Reichert
Keyword(s):  
Solid State ◽  
Solid State Nmr ◽  
Spin Diffusion ◽  
Diffusion Rate ◽  
Magic Angle Spinning ◽  
Frequency Effect ◽  
Magic Angle ◽  
Angle Spinning

Sensitivity enhanced 14N/14N correlations to probe inter-beta-sheet interactions using fast magic angle spinning solid-state NMR in biological solids

2016 ◽  
Vol 18 (32) ◽  
pp. 22583-22589 ◽  
Author(s):  
Manoj Kumar Pandey ◽  
Jean-Paul Amoureux ◽  
Tetsuo Asakura ◽  
Yusuke Nishiyama
Keyword(s):  
Solid State ◽  
Solid State Nmr ◽  
Spin Diffusion ◽  
Correlation Method ◽  
Magic Angle Spinning ◽  
Magic Angle ◽  
Beta Sheet ◽  
Biological Solids ◽  
Angle Spinning ◽  
Fast Magic Angle Spinning

Sensitivity enhanced proton-detected 14N/14N correlation method mediated through accelerated 1H–1H spin diffusion at fast magic angle spinning (MAS) solid-state NMR is demonstrated to distinguish inter-beta-sheet interactions in naturally abundant parallel and anti-parallel alanine tripeptides.

scholarly journals Combination of solid state NMR and DFT calculation to elucidate the state of sodium in hard carbon electrodes

2016 ◽  
Vol 4 (34) ◽  
pp. 13183-13193 ◽  
Author(s):  
Ryohei Morita ◽  
Kazuma Gotoh ◽  
Mika Fukunishi ◽  
Kei Kubota ◽  
Shinichi Komaba ◽  
...  
Keyword(s):  
Solid State ◽  
Solid State Nmr ◽  
Dft Calculation ◽  
Magic Angle Spinning ◽  
The State ◽  
Mas Nmr ◽  
Magic Angle ◽  
Multiple Quantum ◽  
Hard Carbon ◽  
Angle Spinning

We examined the state of sodium electrochemically inserted in HC prepared at 700–2000 °C using solid state Na magic angle spinning (MAS) NMR and multiple quantum (MQ) MAS NMR.

High resolution triple resonance micro magic angle spinning NMR spectroscopy of nanoliter sample volumes

2016 ◽  
Vol 18 (6) ◽  
pp. 4902-4910 ◽  
Author(s):  
J. Ole Brauckmann ◽  
J. W. G. (Hans) Janssen ◽  
Arno P. M. Kentgens
Keyword(s):  
Solid State ◽  
Nmr Spectroscopy ◽  
High Resolution ◽  
Single Crystals ◽  
Solid State Nmr ◽  
Magic Angle Spinning ◽  
Magic Angle ◽  
Triple Resonance ◽  
Angle Spinning

To be able to study mass-limited samples and small single crystals, a triple resonance micro-magic angle spinning (μMAS) probehead for the application of high-resolution solid-state NMR of nanoliter samples was developed.

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