scholarly journals A novel protocol for the one-pot borylation/Suzuki reaction provides easy access to hinge-binding groups for kinase inhibitors

2016 ◽  
Vol 14 (3) ◽  
pp. 963-969 ◽  
Author(s):  
A. Hooper ◽  
A. Zambon ◽  
C. J. Springer
Keyword(s):  
Kinase Inhibitors ◽  
Suzuki Reaction ◽  
Easy Access ◽  
One Pot ◽  
Microwave Assisted ◽  
The One ◽  
Microwave Assisted Method

This new microwave-assisted method provides a quick one-pot borylation/Suzuki protocol that does not require additional ligands nor double loading of catalyst.

Facile one-pot synthesis of Cu2ZnSnS4 quaternary nanoparticles using a microwave-assisted method

CrystEngComm ◽  
2013 ◽  
Vol 15 (46) ◽  
pp. 9863 ◽  
Author(s):  
Kuo-Chin Wang ◽  
Peter Chen ◽  
Chuan-Ming Tseng
Keyword(s):  
One Pot ◽  
Microwave Assisted ◽  
One Pot Synthesis ◽  
Microwave Assisted Method

scholarly journals Microwave Assisted Three Component Reaction Conditions to Obtain New Thiazolidinones with Different Heterocyclic Skeletons

Proceedings ◽  
2019 ◽  
Vol 41 (1) ◽  
pp. 38
Author(s):  
Fernando J. Lorenzo ◽  
Romina A. Ocampo ◽  
Sandra D. Mandolesi
Keyword(s):  
Microwave Irradiation ◽  
Thioglycolic Acid ◽  
Aldehyde Group ◽  
Green Solvent ◽  
Reaction Products ◽  
Reaction Conditions ◽  
One Pot ◽  
Microwave Assisted ◽  
Three Component Reaction ◽  
The One

We present here a new proposal for the “one pot” generation of new 4-thiazolidinones (9a–e) through a multicomponent reaction under microwave irradiation conditions, using aromatic and heteroaromatic amines (8a–e), absolute ethanol as a “green” solvent and modifying the aldehyde group in the glycosidic residue, synthesized from D-mannitol. The study is focused in the variation of the irradiation times and the concentration of thioglycolic acid in order to study the possibility of controlling the structure and/or stereochemistry of the products formed in the reaction. Thiazolidinones 9a–d were obtained with a 69–82% The generation of the corresponding reaction products were monitored by TLC and CG-MS, taking reaction aliquots. The conditions reaction proved to be chemoselective depending on the excess of acid and irradiation times.

One-pot microwave assisted approach for synthesis of CdSe/CdS core-shell quantum dots (QDs) and investigating optical properties

2016 ◽  
Vol 30 (07) ◽  
pp. 1650074 ◽  
Author(s):  
M. Molaei ◽  
F. Salari Bardsiri ◽  
A. R. Bahador ◽  
M. Karimipour
Keyword(s):  
Core Shell ◽  
Heat Sensitivity ◽  
X Ray Diffraction ◽  
Cdse Qds ◽  
One Pot ◽  
X Ray ◽  
Microwave Assisted ◽  
Transmission Electron ◽  
Core Shell Structure ◽  
Microwave Assisted Method

In this work, CdSe QDs were synthesized using a microwave assisted method and chemical reaction between NaHSe, CdSO4 at the presence of TGA as capping molecule. Thereafter without CdSe extraction, CdS shell was grown subsequently around CdSe cores by a reaction based on the heat sensitivity of Na2S2O3 dissociation. Synthesized QDs were characterized by means of X-ray diffraction spectroscopy (XRD), Fourier transform infrared spectroscopy (FTIR), transmission electron microscopy (TEM), UV–Vis and photoluminescence (PL) spectroscopy. All of these analyzes confirmed formation of CdSe QDs and successfully growth of CdS shell on surface of CdSe to forming CdSe/CdS core-shell structure.

scholarly journals Microwave Assisted One Pot Synthesis of Tetrazole Based 3-hydroxy-4H-chromen-4-ones by modified Algar-Flynn-Oyamada reaction and their Antimicrobial activity

2019 ◽  
Vol 63 (4) ◽  
Author(s):  
ASHOK DONGAMANTI ◽  
Nagaraju Nalaparaju ◽  
Sarasija Madderla ◽  
Vijaya Lakshmi Bommidi
Keyword(s):  
Escherichia Coli ◽  
Antimicrobial Activity ◽  
Klebsiella Pneumonia ◽  
Good Activity ◽  
One Pot ◽  
Microwave Assisted ◽  
One Pot Synthesis ◽  
Antimicrobial Studies ◽  
The One

In the present work, we report the one pot synthesis of tetrazole based 3-hydroxy-4H-chromen-4-ones 3(a-g) from  4-(1H-tetrazol-5-yl)benzaldehyde and 2-hydroxy acetophenone using KOH and H2O2 by modified Algar-Flynn-Oyamada reaction under conventional and microwave irradiation conditions. In this technique, flavonols are synthesized without isolating chalcones, in good yields. All the synthesized compounds were characterized by IR, NMR, MS and elemental. All newly synthesized compounds were screened for their in-vitro antimicrobial activity against strains such as Staphylococcus aurous, Bacillus subtilis, Klebsiella pneumonia, Escherichia coli, Aspergillus Niger, Aspergillus flavus, and Fusarium oxysporum. The results of antimicrobial studies revealed that most of the compounds exhibit good activity.

An expedient microwave assisted regio- and stereoselective synthesis of spiroquinoxaline pyrrolizine derivatives and their AChE inhibitory activity

2017 ◽  
Vol 41 (2) ◽  
pp. 873-878 ◽  
Author(s):  
Adinarayana Murthy Akondi ◽  
Sowmya Mekala ◽  
Mannepalli Lakshmi Kantam ◽  
Rajiv Trivedi ◽  
L. Raju Chowhan ◽  
...  
Keyword(s):  
Inhibitory Activity ◽  
Stereoselective Synthesis ◽  
Facile Synthesis ◽  
One Pot ◽  
Microwave Assisted ◽  
Ache Inhibitory Activity ◽  
The One

We report here an efficient protocol for the one-pot facile synthesis of spiro[indeno[1,2-b]quinoxaline-11,3′-pyrrolizine]heterocyclic scaffolds and their AChE inhibitory studies.

scholarly journals One-pot synthesis of graphene quantum dots and simultaneous nanostructured self-assembly via a novel microwave-assisted method: impact on triazine removal and efficiency monitoring

RSC Advances ◽  
2018 ◽  
Vol 8 (52) ◽  
pp. 29939-29946 ◽  
Author(s):  
Beatriz Fresco-Cala ◽  
M. Laura Soriano ◽  
Alice Sciortino ◽  
Marco Cannas ◽  
Fabrizio Messina ◽  
...  
Keyword(s):  
Quantum Dots ◽  
Quantum Dot ◽  
Self Assembly ◽  
Graphene Quantum Dots ◽  
One Pot ◽  
Graphene Quantum Dot ◽  
Microwave Assisted ◽  
Microwave Reaction ◽  
One Step ◽  
Microwave Assisted Method

Graphene quantum dot (GQDs) assemblies from a one-step microwave reaction as bifunctional materials in remediation of triazines.

Facile one-pot synthesis of multifunctional protamine sulfate-derived carbon dots for antibacterial applications and fluorescence imaging of bacteria

2021 ◽  
Author(s):  
Dan Zhao ◽  
Xuemei Liu ◽  
Rui Zhang ◽  
Xianju Huang ◽  
Xincai Xiao
Keyword(s):  
Fluorescence Imaging ◽  
Carbon Dots ◽  
Protamine Sulfate ◽  
One Pot ◽  
Microwave Assisted ◽  
One Pot Synthesis ◽  
Microwave Assisted Method ◽  
Dual Functions

PS-carbon dots (CDs) were prepared by a microwave-assisted method using protamine sulfate (PS), and they have dual functions of antibacterial and bacterial imaging.

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