Large-scale one pot synthesis of metal oxide nanoparticles by decomposition of metal carbonates or nitrates

CrystEngComm ◽  
2015 ◽  
Vol 17 (27) ◽  
pp. 4977-4981 ◽  
Author(s):  
Byeongyoon Kim ◽  
Jun Kim ◽  
Hionsuck Baik ◽  
Kwangyeol Lee
Keyword(s):  
Metal Oxide ◽  
Large Scale ◽  
Metal Oxide Nanoparticles ◽  
Oxide Nanoparticles ◽  
One Pot ◽  
One Pot Synthesis ◽  
Metal Carbonates

scholarly journals Facile meltPEGylation of flame-made luminescent Tb3+-doped yttrium oxide particles: hemocompatibility, cellular uptake and comparison to silica

2018 ◽  
Vol 54 (23) ◽  
pp. 2914-2917 ◽  
Author(s):  
Kerda Keevend ◽  
Guido Panzarasa ◽  
Fabian H. L. Starsich ◽  
Martin Zeltner ◽  
Anastasia Spyrogianni ◽  
...  
Keyword(s):  
Metal Oxide ◽  
Yttrium Oxide ◽  
Cellular Uptake ◽  
Metal Oxide Nanoparticles ◽  
Oxide Nanoparticles ◽  
One Pot ◽  
Oxide Particles

MeltPEGylation constitutes an elegant one-pot route for the efficient PEGylation of metal oxide nanoparticles with improved hemo- and cytocompatibility.

scholarly journals Mechanochemical synthesis of metal oxide nanoparticles

2021 ◽  
Vol 4 (1) ◽  
Author(s):  
Takuya Tsuzuki
Keyword(s):  
Metal Oxide ◽  
Mechanochemical Synthesis ◽  
Large Scale ◽  
Reaction Pathway ◽  
Metal Oxide Nanoparticles ◽  
Energy Storage And Conversion ◽  
Oxide Nanoparticles ◽  
Synthesis Methods ◽  
Scale Production ◽  
Large Scale Production

AbstractIn the last decades, mechanochemical processing has emerged as a sustainable method for the large-scale production of a variety of nanomaterials. In particular, mechanochemical synthesis can afford well-dispersed metal-oxide nanoparticles, which are used in wide-ranging applications including energy storage and conversion, environmental monitoring, or biomedical uses. This article reviews recent progress in the mechanochemical synthesis of metal-oxide nanoparticles, explores reaction mechanisms, and contrasts the influence of chosen process parameters on the properties of end products. The role of choice of reaction pathway, as well as advantages and limitations compared to other synthesis methods are discussed. A prospect for future development of this synthetic method is proposed.

scholarly journals Synthetic versatility of nanoparticles: A new, rapid, one-pot, single-step synthetic approach to spherical mesoporous (metal) oxide nanoparticles using supercritical alcohols

2014 ◽  
Vol 86 (5) ◽  
pp. 785-800 ◽  
Author(s):  
Pengyu Wang ◽  
Kazuya Kobiro
Keyword(s):  
Metal Oxide ◽  
Metal Oxide Nanoparticles ◽  
Single Step ◽  
Oxide Nanoparticles ◽  
Synthetic Approach ◽  
Organic Additives ◽  
Step Method ◽  
One Pot ◽  
Mesoporous Metal ◽  
Mesoporous Metal Oxide

AbstractA simple, rapid (10 min), one-pot, single-step method for the preparation of solid and hollow spherical porous TiO2 nanoparticles with large surface areas (100–211 m2/g) was developed in supercritical alcohols using carboxylic acids as organic additives. The shell thickness of the hollow TiO2 nanoparticles (20–280 nm) was controlled by adjusting the heating rate (2.0–10.0 °C/min). The preparation of different spherical porous metal oxide nanoparticles, including CeO2, SiO2, TiO2, ZrO2, and ZnO, demonstrated the versatility of the synthetic approach. In addition, several rare earth-doped spherical mesoporous metal oxide nanoparticles, including CeO2:Er, CeO2:Er,Yb, ZrO2:Er, and TiO2:Er, which exhibit energy upconversion emission, were successfully prepared using this one-pot, single-step, supercritical methanol method. The obtained spherical mesoporous CeO2:Er and CeO2:Er,Yb nanoparticles emit green light upon excitation, even when irradiated with a low-power IR laser (980 nm, 10 mW) without calcination. Several other (metal) elements were also easily doped into spherical, mesoporous TiO2 nanoparticles, such as Eu, Ce, Yb, Fe, and N, using a similar procedure. Furthermore, the spherical mesoporous TiO2 nanoparticles were successfully applied as a new material for the transport of DNA via biolistic bombardment.

scholarly journals Metal Oxide Nanoparticles: Large-Scale Synthesis and Medical Applications of Uniform-Sized Metal Oxide Nanoparticles (Adv. Mater. 42/2018)

2018 ◽  
Vol 30 (42) ◽  
pp. 1870319 ◽  
Author(s):  
Hyek Jin Kwon ◽  
Kwangsoo Shin ◽  
Min Soh ◽  
Hogeun Chang ◽  
Jonghoon Kim ◽  
...  
Keyword(s):  
Metal Oxide ◽  
Large Scale ◽  
Metal Oxide Nanoparticles ◽  
Medical Applications ◽  
Oxide Nanoparticles ◽  
Large Scale Synthesis

Large-Scale Synthesis and Medical Applications of Uniform-Sized Metal Oxide Nanoparticles

2018 ◽  
Vol 30 (42) ◽  
pp. 1704290 ◽  
Author(s):  
Hyek Jin Kwon ◽  
Kwangsoo Shin ◽  
Min Soh ◽  
Hogeun Chang ◽  
Jonghoon Kim ◽  
...  
Keyword(s):  
Metal Oxide ◽  
Large Scale ◽  
Metal Oxide Nanoparticles ◽  
Medical Applications ◽  
Oxide Nanoparticles ◽  
Large Scale Synthesis
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