A general one-step approach for in situ decoration of MoS2 nanosheets with inorganic nanoparticles

2015 ◽  
Vol 3 (3) ◽  
pp. 1042-1048 ◽  
Author(s):  
Zehong Cheng ◽  
Benzhao He ◽  
Li Zhou
Keyword(s):  
Inorganic Nanoparticles ◽  
Mos2 Nanosheets ◽  
One Step ◽  
The One

Here we present a general and controllable protocol for the one-step synthesis of various MoS2–INP nanohybrids by employing carboxylic MoS2 nanosheets as a versatile support.

scholarly journals Analysis of the Influence of Fibers on the Formability of Metal Blanks in Manufacturing Processes for Fiber Metal Laminates

2019 ◽  
Vol 3 (1) ◽  
pp. 2 ◽  
Author(s):  
Thomas Mennecart ◽  
Soeren Gies ◽  
Noomane Ben Khalifa ◽  
A. Erman Tekkaya
Keyword(s):  
Contact Forces ◽  
Starting Time ◽  
Fiber Metal Laminate ◽  
Metal Sheets ◽  
Different Types ◽  
One Step ◽  
Fiber Metal ◽  
The One ◽  
Metal Blank

In the one-step manufacturing process for fiber metal laminate parts, the so-called in situ hybridization process, the fabrics are interacting with metal blanks. During deep drawing, the liquid matrix is injected between the metal sheets through the woven fiber layers. The metal blanks can be in contact with dry or with infiltrated fibers. The formability of the blanks is influenced by the variation of the starting time of injection. The reason for that is that, due to high contact forces, the fibers are able to deform the metal surface locally, so that movement and the strain of the blanks is inhibited. To investigate the influence of different fibers on the formability of metals, Nakazima tests are performed. In these tests, two metal blanks are formed with an interlayer of fibers. The results are compared with the formability of two blanks without any interlayer. It is shown that in with fibers between sheets, the formability decreases compared to the formability of two metal blanks without interlayers. Based on a simplified numerical model for different types of fibers, the interactions of the fibers with the metal blank are analyzed. It could be shown that the friction due to contact has more influence than the friction due to the form fit caused by the imprints.

In-situ regeneration mechanisms of hybrid catalysts in the one-step synthesis of dimethyl ether from syngas

2007 ◽  
Vol 115 (1-2) ◽  
pp. 23-26 ◽  
Author(s):  
Youshun Luan ◽  
Hengyong Xu ◽  
Chunying Yu ◽  
Wenzhao Li ◽  
Shoufu Hou
Keyword(s):  
Dimethyl Ether ◽  
Hybrid Catalysts ◽  
In Situ Regeneration ◽  
One Step ◽  
The One ◽  
Synthesis Of Dimethyl Ether

scholarly journals 1-(4-Nitrophenyl)-1H-1,2,3-Triazole-4-carbaldehyde: Scalable Synthesis and Its Use in the Preparation of 1-Alkyl-4-Formyl-1,2,3-triazoles

Organics ◽  
2021 ◽  
Vol 2 (4) ◽  
pp. 404-414
Author(s):  
Tomas Opsomer ◽  
Kaat Valkeneers ◽  
Ana Ratković ◽  
Wim Dehaen
Keyword(s):  
One Pot ◽  
Complete Hydrolysis ◽  
One Step ◽  
Synthetic Intermediates ◽  
Cornforth Rearrangement ◽  
Scalable Synthesis ◽  
The One ◽  
Novel Applications ◽  
Hydrolysis Of

1,2,3-Triazole-4-carbaldehydes are useful synthetic intermediates which may play an important role in the discovery of novel applications of the 1,2,3-triazole moiety. In this work, a one-step multigram scale synthesis of 4-formyl-1-(4-nitrophenyl)-1H-1,2,3-triazole (FNPT) as a preferred reagent for the synthesis of 1-alkyl-4-formyltriazoles is described, making use of the commercially available 3-dimethylaminoacrolein and 4-nitrophenyl azide. Next, the earlier reported reaction of FNPT with alkylamines is further explored, and for hexylamine, the one-pot sequential cycloaddition and Cornforth rearrangement is demonstrated. In addition, a useful protocol for the in situ diazotization of 4-nitroaniline is provided. This facilitated the complete hydrolysis of rearranged 4-iminomethyl-1,2,3-triazoles and allowed for the recycling of 4-nitrophenyl azide.

Pd/meso-CoO derived from in situ reduction of the one-step synthesized Pd/meso-Co3O4: high-performance catalysts for benzene combustion

2019 ◽  
Vol 43 (31) ◽  
pp. 12358-12368 ◽  
Author(s):  
Xingtian Zhao ◽  
Ran Zhang ◽  
Yuxi Liu ◽  
Jiguang Deng ◽  
Peng Xu ◽  
...  
Keyword(s):  
Catalytic Activity ◽  
High Performance ◽  
Oxygen Activation ◽  
In Situ Reduction ◽  
Templating Method ◽  
One Step ◽  
The One

The 0.93Pd/meso-CoO is prepared via in situ reduction of 0.85Pd/meso-Co3O4 derived from KIT-6-templating method. The excellent catalytic activity of 0.93Pd/meso-CoO is related to the formed Pd0 species and good oxygen activation ability.

scholarly journals Low temperature oxidation synthesis of carbon encapsulated Cr2O3 nanocrystals and its lithium storage performance

2018 ◽  
Vol 11 (01) ◽  
pp. 1850008 ◽  
Author(s):  
Yun Zhou ◽  
Boyang Liu ◽  
Yingfeng Shao ◽  
Chunhua Fan ◽  
Runhua Fan ◽  
...  
Keyword(s):  
Reversible Capacity ◽  
Ammonium Persulfate ◽  
Low Temperature Oxidation ◽  
Lithium Storage ◽  
Temperature Oxidation ◽  
One Step ◽  
Explosive Reaction ◽  
The One ◽  
A Current

A highly efficient and convenient strategy is developed for the one-step in-situ synthesis of carbon encapsulated Cr2O3 nanocrystals with core-shell structure (Cr2O3@C). The explosive reaction of chromocene with ammonium persulfate in an autoclave at 200[Formula: see text]C is crucial for the formation of this nanostructure. The Cr2O3 nanocrystals have a diameter of 5 to 20[Formula: see text]nm, which are entirely encapsulated by the amorphous carbon shell. The Cr2O3@C anode can retain a stable reversible capacity of 397[Formula: see text]mAh[Formula: see text]g[Formula: see text] after 50 cycles at a current density of 119[Formula: see text]mA g[Formula: see text].

IN SITU UNZIPPING OF CARBON NANOTUBES TO FORM GRAPHENE NANORIBBONS

NANO ◽  
2014 ◽  
Vol 09 (01) ◽  
pp. 1450010 ◽  
Author(s):  
YONG-SHENG ZHOU ◽  
PAN JIN ◽  
TENG GUO ◽  
YING-CHUN ZHU ◽  
GAO-HUI DU ◽  
...  
Keyword(s):  
Carbon Nanotubes ◽  
Graphene Nanoribbons ◽  
Average Length ◽  
Chemical Vapor ◽  
Chemical Vapor Deposition Method ◽  
Alternative Approach ◽  
Simple Chemical ◽  
One Step ◽  
The One

We report the one step facile synthesis of graphene nanoribbons (GNRs) by unzipping carbon nanotubes (CNTs) from glucose ( C 6 H 12 O 6) precursor, using a simple chemical vapor deposition method. Some nanotubes are partially cut resulting in a GNR–CNT hybrid whereas others are fully cut to form GNRs. The average length of GNRs achieved by this method is typically in the range of 1–10 μm. The formation of GNRs is ascribed to the in situ oxygen-driven unzipping of CNTs. The process is free from aggressive oxidants and utilizes the in situ unzipping. This method offers an alternative approach for making GNRs, compared to previously used techniques to synthesize GNRs.

scholarly journals A Facile Green Fabrication and Characterization of Cellulose-Silver Nanoparticle Composite Sheets for an Antimicrobial Food Packaging

2021 ◽  
Vol 8 ◽  
Author(s):  
Seongyoung Kwon ◽  
Wooseok Lee ◽  
Jung Wook Choi ◽  
Nattinee Bumbudsanpharoke ◽  
Seonghyuk Ko
Keyword(s):  
Photoelectron Spectroscopy ◽  
Food Packaging ◽  
Cellulose Fiber ◽  
Cellulose Fibers ◽  
Hydroxyl Groups ◽  
Green Approach ◽  
Vis Spectroscopy ◽  
One Step ◽  
The One

The present study focused on a facile and green approach for the one-step synthesis of silver nanoparticles (AgNPs) embedded in hard wood bleached kraft fiber. The hydroxyl groups on the cellulose chain induced ionic silver reduction with additional hydrothermal energy, allowing for the in situ formation and deposition of AgNPs on the cellulose fiber. The white color of the bleached fiber transformed to yellow due to the formation of AgNPs. UV-Vis spectroscopy, scanning electron microscopy, and X-ray photoelectron spectroscopy revealed that the AgNPs were uniformly distributed across the surface of the obtained cellulose fibers. The results indicated that the formation and distribution of AgNPs on surface of cellulose fibers was significantly influenced by the amount and concentration of silver nitrate (AgNO3). The antimicrobial activity of the cellulose-AgNP composite sheet against Escherichia coli was found to be inhibiting. These findings imply that cellulose-AgNP composite sheets can be feasibly used as antimicrobial paper for food packaging.

The interlocked in situ fabrication of graphene@prussian blue nanocomposite as high-performance supercapacitor

2018 ◽  
Vol 47 (37) ◽  
pp. 13126-13134 ◽  
Author(s):  
Shi-Cheng Wang ◽  
Minli Gu ◽  
Luqing Pan ◽  
Junfeng Xu ◽  
Lei Han ◽  
...  
Keyword(s):  
Prussian Blue ◽  
High Performance ◽  
Great Promise ◽  
High Quality ◽  
In Situ Fabrication ◽  
Excellent Electrochemical Performance ◽  
One Step ◽  
The One ◽  
Method Show

High-quality graphene@prussian blue (G@PB) nanocomposite sheets fabricated via the one-step in situ hydrothermal method show great promise for energy-storage hybrid electrodes with excellent electrochemical performance.

One-Step in Situ Detection of miRNA-21 Expression in Single Cancer Cells Based on Biofunctionalized MoS2 Nanosheets

2017 ◽  
Vol 10 (1) ◽  
pp. 350-360 ◽  
Author(s):  
Gerile Oudeng ◽  
Manting Au ◽  
Jingyu Shi ◽  
Chunyi Wen ◽  
Mo Yang
Keyword(s):  
Cancer Cells ◽  
Mos2 Nanosheets ◽  
One Step ◽  
Single Cancer ◽  
In Situ Detection
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