A novel, facile, rapid, solvent free protocol for the one pot green synthesis of chromeno[2,3-d]pyrimidines using reusable nano ZnAl2O4– a NOSE approach and photophysical studies

RSC Advances ◽  
2015 ◽  
Vol 5 (9) ◽  
pp. 6578-6587 ◽  
Author(s):  
Balijapalli Umamahesh ◽  
Triveni Rajashekhar Mandlimath ◽  
Kulathu I. Sathiyanarayanan

The preparation of an eco-friendly, highly stable, reusable nano ZnAl2O4was used as an excellent catalyst for the pseudo four component synthesis of a library of fluorescent chromeno[2,3-d]pyrimidine derivatives.

RSC Advances ◽  
2015 ◽  
Vol 5 (67) ◽  
pp. 54124-54124
Author(s):  
Balijapalli Umamahesh ◽  
Triveni Rajashekhar Mandlimath ◽  
Kulathu I. Sathiyanarayanan

Correction for 'A novel, facile, rapid, solvent free protocol for the one pot green synthesis of chromeno[2,3-d]pyrimidines using reusable nano ZnAl2O4 – a NOSE approach and photophysical studies' by Balijapalli Umamahesh et al., RSC Adv., 2015, 5, 6578–6587.


2021 ◽  
Vol 76 (2) ◽  
pp. 85-90
Author(s):  
Abdolkarim Zare ◽  
Manije Dianat

Abstract A highly efficient and green protocol for the synthesis of pyrimido[4,5-b]quinolines has been described. The one-pot multicomponent reaction of dimedone with arylaldehydes and 6-amino-1,3-dimethyluracil in the presence of N,N-diethyl-N-sulfoethanaminium chloride ([Et3N–SO3H][Cl]) as an ionic liquid (IL) catalyst under solvent-free conditions afforded the mentioned compounds in high yields and short reaction times. Our protocol is superior to many of the reported protocols in terms of two or more of these factors: the reaction times, yields, conditions (solvent-free versus usage of organic solvents), temperature and catalyst amount.


2021 ◽  
Vol 18 ◽  
Author(s):  
Abolfazl Olyaei ◽  
Zahra Ghahremany ◽  
Madieh Sadeghpour

: A green and efficient protocol was developed for the one-pot three-component synthesis of novel 2-(4-hydroxy-2-oxo-2H-chromen-3-yl)-2-(arylamino)-1H-indene-1,3(2H)-dione derivatives by the reaction of 4-hydroxycoumarin, ninhydrin and aromatic amines in the presence of guanidine hydrochloride as an organocatalyst under solvent-free conditions. The present approach offers several advantages such as low cost, simple work-up, short reaction times, chromatography-free purification, high yields and greener conditions.


2017 ◽  
Vol 57 (1) ◽  
Author(s):  
Javad Safaei-Ghomi ◽  
Mohammad Ali Ghasemzadeh ◽  
Safura Zahedi

ZnO nanoparticles as a worthwhile and recyclable catalyst have been used for the one-pot synthesis of 1,8-dioxo-decahydroacridines and 1,8-dioxooctahydro-xanthenes via multi-component reactions under solvent-free conditions. The presented method is mild, environmentally friendly, inexpensive and highly effective to give the products in good to excellent yields.


2021 ◽  
Vol 18 ◽  
Author(s):  
Ellahe Sabbaghnasab ◽  
Enayatollah Sheikhhosseini

: NiO nanoparticles are utilized to effectively strengthen annulated pyrano [2, 3- d] pyrimidine synthesis through primary Knoevenagel, following Micheal and ultimate heterocyclization reactions of aldehyde, malononitrile, and barbituric acid. The characteristics of NiO nanoparticles are identified using advanced techniques, such as IR, UV, EDX, XRD, SEM, and TEM. The nano-NiO particles are mostly below < 100 nm in size with uniform spherical shapes. The adopted approach is advantages thanks to its simple processing, relatively short reaction time, often good to high average yields, convenient workability, and environmental friendliness.


ChemInform ◽  
2010 ◽  
Vol 41 (26) ◽  
pp. no-no
Author(s):  
Mohammad Zaman Kassaee ◽  
Hassan Masrouri ◽  
Farnaz Movahedi ◽  
Reza Mohammadi

2015 ◽  
Vol 44 (20) ◽  
pp. 9596-9609 ◽  
Author(s):  
R. Tayebee ◽  
M. M. Amini ◽  
M. Akbari ◽  
A. Aliakbari

A new inorganic–organic nanohybrid material was prepared and performed as an efficient catalyst for the one-pot multi-component synthesis of different substituted 1-amidoalkyl-2-naphthols under solvent-free conditions.


ChemInform ◽  
2007 ◽  
Vol 38 (36) ◽  
Author(s):  
Mazaahir Kidwai ◽  
Kavita Singhal ◽  
Shuchi Kukreja

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