Supercritical CO2 extraction of organic carbonate-based electrolytes of lithium-ion batteries

RSC Advances ◽  
2014 ◽  
Vol 4 (97) ◽  
pp. 54525-54531 ◽  
Author(s):  
Yuanlong Liu ◽  
Deying Mu ◽  
Rujuan Zheng ◽  
Changsong Dai

Supercritical fluid extraction (SFE) was applied to reclaim organic carbonate-based electrolytes of spent lithium-ion batteries.

2009 ◽  
Vol 74 (4) ◽  
pp. 417-425 ◽  
Author(s):  
Zoran Zekovic ◽  
Zika Lepojevic ◽  
Slavica Milic ◽  
Dusan Adamovic ◽  
Ibrahim Mujic

The chemical composition of mentha essential oil and mentha extracts obtained at different pressures/temperatures by supercritical fluid extraction (SFE) were studied by GC-MS. The menthol content was also determined spectrophotometrically. The predominant compounds in the essential oil and in the CO2 extract obtained at 100 bar were L-menthon and menthole but at higher pressures (from 150 to 400 bar), squalene was dominant. The equation of Naik et al. was used for modelling the mentha-supercritical CO2 system.


1995 ◽  
Vol 78 (4) ◽  
pp. 1051-1054 ◽  
Author(s):  
Earl G Alley ◽  
Guozhen Lu

Abstract We present a method that combines the extraction of polychlonnated biphenyls (PCBs) and their separation from relatively large quantities of fat in biological matrixes by combined supercritical fluid extraction and separation. Cyano-functionalized silica gel, silica gel, aluminum oxide, Florisil, 3-aminopropyl- functionalized silica gel, and octadecyl-functionalized silica gel were tested for suitability as chromatographic media for separation of PCBs from lipids. Silica gel, 3-aminopropyl-functionalized silica gel, and Florisil adequately separated PCBs from lipids when eluted with supercritical CO2. Florisil allowed both the extraction of PCBs and their separation from lipids in PCB-spiked chicken egg and fish. Two grams of sample containing PCBs at 0.125 μg/g was sufficient for subsequent separations and the low-level analysis required for the more toxic PCB components.


Author(s):  
Maria Dolores Luque de Castro ◽  
Miguel Valcárcel ◽  
Maria Teresa Tena

2015 ◽  
Vol 14 (2) ◽  
pp. 297-302 ◽  
Author(s):  
Valeriu V. Cotea ◽  
Lucia Cintia Colibaba ◽  
Liliana Rotaru ◽  
Bogdan Nechita ◽  
Marius Niculaua ◽  
...  

Molecules ◽  
2021 ◽  
Vol 26 (8) ◽  
pp. 2366
Author(s):  
Katarzyna Klimek ◽  
Katarzyna Tyśkiewicz ◽  
Malgorzata Miazga-Karska ◽  
Agnieszka Dębczak ◽  
Edward Rój ◽  
...  

Given the health-beneficial properties of compounds from hop, there is still a growing trend towards developing successful extraction methods with the highest yield and also receiving the products with high added value. The aim of this study was to develop efficient extraction method for isolation of bioactive compounds from the Polish “Marynka” hop variety. The modified two-step supercritical fluid extraction allowed to obtain two hop samples, namely crude extract (E1), composed of α-acids, β-acids, and terpene derivatives, as well as pure xanthohumol with higher yield than that of other available methods. The post-extraction residues (R1) were re-extracted in order to obtain extract E2 enriched in xanthohumol. Then, both samples were subjected to investigation of their antibacterial (anti-acne, anti-caries), cytotoxic, and anti-proliferative activities in vitro. It was demonstrated that extract (E1) possessed more beneficial biological properties than xanthohumol. It exhibited not only better antibacterial activity against Gram-positive bacteria strains (MIC, MBC) but also possessed a higher synergistic effect with commercial antibiotics when compared to xanthohumol. Moreover, cell culture experiments revealed that crude extract neither inhibited viability nor divisions of normal skin fibroblasts as strongly as xanthohumol. In turn, calculated selectivity indexes showed that the crude extract had from slightly to significantly better selective anti-proliferative activity towards cancer cells in comparison with xanthohumol.


2021 ◽  
Vol 297 ◽  
pp. 126593
Author(s):  
Ana Carolina Fornereto Soldan ◽  
Sarah Arvelos ◽  
Érika Ohta Watanabe ◽  
Carla Eponina Hori

2021 ◽  
Vol 111 ◽  
pp. 249-260
Author(s):  
Hossein Ahangari ◽  
Jerry W. King ◽  
Ali Ehsani ◽  
Mohammad Yousefi

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