First ligand-free, microwave-assisted, Heck cross-coupling reaction in pure water on a nucleoside – application to the synthesis of antiviral BVDU

RSC Advances ◽  
2014 ◽  
Vol 4 (87) ◽  
pp. 46926-46929 ◽  
Author(s):  
Gwénaëlle Hervé ◽  
Christophe Len
Keyword(s):  
Pure Water ◽  
Coupling Reaction ◽  
Cross Coupling ◽  
Microwave Assisted ◽  
Cross Coupling Reaction ◽  
Ligand Free ◽  
Palladium Catalyzed ◽  
Microwave Assistance ◽  
First Time

For the first time, a palladium catalyzed Heck cross-coupling reaction between 5-iodo-2′-deoxyuridine and various acrylate derivatives was performed using ligand-free conditions and microwave assistance in pure water.

Original access to 5-aryluracils from 5-iodo-2′-deoxyuridine via a microwave assisted Suzuki-Miyaura cross-coupling/deglycosylation sequence in pure water

RSC Advances ◽  
2014 ◽  
Vol 4 (86) ◽  
pp. 46218-46223 ◽  
Author(s):  
T. Lussier ◽  
G. Hervé ◽  
G. Enderlin ◽  
C. Len
Keyword(s):  
Microwave Irradiation ◽  
Pure Water ◽  
Coupling Reaction ◽  
Cross Coupling ◽  
Microwave Assisted ◽  
Cross Coupling Reaction ◽  
Ligand Free

A facile and efficient methodology to obtain various 5-aryluracil derivatives was developed through a two steps sequence: a ligand-free Suzuki-Miyaura cross-coupling reaction starting from totally deprotected 5-iodo-(2′-deoxy)uridine followed by a very simple deglycosylation procedure in pure water with assistance of microwave irradiation.

ChemInform Abstract: Solid-Supported Rhodium(0) Nano-/Microparticles: An Efficient Ligand-Free Heterogeneous Catalyst for Microwave-Assisted Suzuki-Miyaura Cross-Coupling Reaction.

ChemInform ◽  
2013 ◽  
Vol 44 (15) ◽  
pp. no-no
Author(s):  
Nitul Ranjan Guha ◽  
Chennayala Bal Reddy ◽  
Nidhi Aggarwal ◽  
Dharminder Sharma ◽  
Arun K. Shil ◽  
...  
Keyword(s):  
Heterogeneous Catalyst ◽  
Coupling Reaction ◽  
Cross Coupling ◽  
Microwave Assisted ◽  
Cross Coupling Reaction ◽  
Ligand Free

Palladium catalyzed ligand-free Suzuki cross-coupling reaction

2008 ◽  
Vol 9 (4) ◽  
pp. 508-510 ◽  
Author(s):  
Changduo Pan ◽  
Miaochang Liu ◽  
Lin Zhang ◽  
Huayue Wu ◽  
Jinchang Ding ◽  
...  
Keyword(s):  
Coupling Reaction ◽  
Cross Coupling ◽  
Cross Coupling Reaction ◽  
Ligand Free ◽  
Palladium Catalyzed

Microwave-assisted synthesis of new fluorescent indoline-based building blocks by ligand free Suzuki-Miyaura cross-coupling reaction in aqueous media

Tetrahedron ◽  
2016 ◽  
Vol 72 (22) ◽  
pp. 2955-2963 ◽  
Author(s):  
Živilė Žukauskaitė ◽  
Vida Buinauskaitė ◽  
Joana Solovjova ◽  
Lina Malinauskaitė ◽  
Aistė Kveselytė ◽  
...  
Keyword(s):  
Aqueous Media ◽  
Coupling Reaction ◽  
Cross Coupling ◽  
Building Blocks ◽  
Microwave Assisted Synthesis ◽  
Microwave Assisted ◽  
Cross Coupling Reaction ◽  
Ligand Free

Fully π-conjugated, diyne-linked covalent organic frameworks formed via alkyne-alkyne cross-coupling reaction

2022 ◽  
Author(s):  
Xiaoming Liu ◽  
Zhengjie Yao ◽  
Zhenwei Zhang ◽  
Jiali Li ◽  
Ji Jia ◽  
...  
Keyword(s):  
Coupling Reaction ◽  
Cross Coupling ◽  
Covalent Organic Frameworks ◽  
Cross Coupling Reaction ◽  
Palladium Catalyzed ◽  
New Material ◽  
First Time ◽  
Alkyne Coupling

A novel diyne-linked porphyrin-based COF was constructed through palladium catalyzed alkyne-alkyne coupling for the first time. The new material features inherent porosity, moderate crystallinity, excellent durability, full π-conjugation, and can...

Solid-Supported Rhodium(0) Nano-/Microparticles: An Efficient Ligand-Free Heterogeneous Catalyst for Microwave-Assisted Suzuki-Miyaura Cross-Coupling Reaction

2012 ◽  
Vol 354 (16) ◽  
pp. 2911-2915 ◽  
Author(s):  
Nitul Ranjan Guha ◽  
Chennayala Bal Reddy ◽  
Nidhi Aggarwal ◽  
Dharminder Sharma ◽  
Arun K. Shil ◽  
...  
Keyword(s):  
Heterogeneous Catalyst ◽  
Coupling Reaction ◽  
Cross Coupling ◽  
Microwave Assisted ◽  
Cross Coupling Reaction ◽  
Ligand Free

Sustainable Ligand‐Free Heterogeneous Palladium‐Catalyzed Sonogashira Cross‐Coupling Reaction in Deep Eutectic Solvents

ChemCatChem ◽  
2020 ◽  
Vol 12 (7) ◽  
pp. 1979-1984 ◽  
Author(s):  
Francesco Messa ◽  
Giuseppe Dilauro ◽  
Filippo M. Perna ◽  
Paola Vitale ◽  
Vito Capriati ◽  
...  
Keyword(s):  
Coupling Reaction ◽  
Cross Coupling ◽  
Deep Eutectic Solvents ◽  
Cross Coupling Reaction ◽  
Ligand Free ◽  
Palladium Catalyzed
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