Electroanalytical determination of the linuron herbicide using a cathodically pretreated boron-doped diamond electrode: comparison with a boron-doped diamond electrode modified with platinum nanoparticles

2015 ◽  
Vol 7 (2) ◽  
pp. 643-649 ◽  
Author(s):  
Luiz C. S. Figueiredo-Filho ◽  
Elen R. Sartori ◽  
O. Fatibello-Filho
Keyword(s):  
Differential Pulse Voltammetry ◽  
Platinum Nanoparticles ◽  
Differential Pulse ◽  
Boron Doped Diamond ◽  
Diamond Electrode ◽  
Boron Doped ◽  
Boron Doped Diamond Electrode ◽  
Pulse Voltammetry

The determination of linuron using differential-pulse voltammetry (DPV) and a cathodically pretreated boron-doped diamond electrode is proposed.

Voltammetric determination of ciprofloxacin in urine samples and its interaction with dsDNA on a cathodically pretreated boron-doped diamond electrode

2015 ◽  
Vol 7 (8) ◽  
pp. 3411-3418 ◽  
Author(s):  
Gustavo Stoppa Garbellini ◽  
Romeu C. Rocha-Filho ◽  
Orlando Fatibello-Filho
Keyword(s):  
Differential Pulse Voltammetry ◽  
Square Wave Voltammetry ◽  
Differential Pulse ◽  
Boron Doped Diamond ◽  
Diamond Electrode ◽  
Boron Doped ◽  
Wave Voltammetry ◽  
Boron Doped Diamond Electrode ◽  
Pulse Voltammetry

A cathodically pretreated boron-doped diamond electrode is successfully used to determine ciprofloxacin (CIP) by differential pulse voltammetry and to infer the type of binding of CIP to DNA by square-wave voltammetry.

scholarly journals Determination of methiocarb pesticide using differential pulse voltammetry with a boron-doped diamond electrode

2015 ◽  
Vol 7 (11) ◽  
pp. 4671-4677 ◽  
Author(s):  
J. Chýlková ◽  
M. Tomášková ◽  
I. Švancara ◽  
L. Janíková ◽  
R. Šelešovská
Keyword(s):  
Differential Pulse Voltammetry ◽  
Rapid Method ◽  
Differential Pulse ◽  
Voltammetric Determination ◽  
Boron Doped Diamond ◽  
Diamond Electrode ◽  
Boron Doped ◽  
Boron Doped Diamond Electrode ◽  
Pulse Voltammetry

In this article, a simple and rapid method is described for voltammetric determination of methiocarb (MTC, a pesticide of the carbamate type).

Simultaneous voltammetric determination of aspartame and acesulfame-K in food products using an anodically pretreated boron-doped diamond electrode

2015 ◽  
Vol 7 (5) ◽  
pp. 2135-2140 ◽  
Author(s):  
Patrícia B. Deroco ◽  
Roberta A. Medeiros ◽  
Romeu C. Rocha-Filho ◽  
Orlando Fatibello-Filho
Keyword(s):  
Differential Pulse Voltammetry ◽  
Food Products ◽  
Differential Pulse ◽  
Boron Doped Diamond ◽  
Diamond Electrode ◽  
Boron Doped ◽  
Boron Doped Diamond Electrode ◽  
Pulse Voltammetry ◽  
Simultaneous Voltammetric Determination

The sweeteners aspartame and acesulfame-K were successfully determined in food products by coupling differential pulse voltammetry with an anodically pretreated boron-doped diamond electrode.

Simultaneous determination of nifedipine and atenolol in combined dosage forms using a boron-doped diamond electrode with differential pulse voltammetry

2018 ◽  
Vol 96 (1) ◽  
pp. 1-7 ◽  
Author(s):  
Jessica Scremin ◽  
Elen Romão Sartori
Keyword(s):  
Differential Pulse Voltammetry ◽  
Differential Pulse ◽  
Dosage Forms ◽  
Current Response ◽  
Boron Doped Diamond ◽  
Diamond Electrode ◽  
Boron Doped ◽  
Boron Doped Diamond Electrode ◽  
Pulse Voltammetry

Combinations of nifedipine (NIF) and atenolol (ATN) are used for the treatment of arterial hypertension. Dosages values different from those presented on the label of pharmaceuticals can significantly impact a consumer’s health. To control the quality of the pharmaceuticals effectively, a method for the simultaneous determination of these both drugs using an anodically pretreated boron-doped diamond electrode coupled to differential pulse voltammetry technique was developed. The influence of supporting electrolyte, pH and scan rate on the current response of these both antihypertensives was examined to select the optimum experimental conditions. It was found that NIF and ATN provided two well-shaped and reproducible oxidation peaks at 0.97 V and 1.36 V (vs. Ag/AgCl electrode), respectively, in TRIS buffer solution (pH 8.0). At optimized differential pulse voltammetric parameters, the current response of NIF and ATN was proportionally linear in the concentration range of 3.98–107 μmol L–1 and 1.99–47.2 μmol L–1, with detection limit of 0.612 and 0.999 μmol L−1, respectively. The proposed method was successfully applied in analysis of several commercial combined dosage forms, whose accuracy was attested by good agreement of the results (paired t test at a 95% confidence level) with those obtained using high performance liquid chromatography.

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