Improved microwave-assisted ligand-free Suzuki–Miyaura cross-coupling of 5-iodo-2′-deoxyuridine in pure water

2013 ◽  
Vol 37 (7) ◽  
pp. 1989 ◽  
Author(s):  
Shawn Gallagher-Duval ◽  
Gwénaëlle Hervé ◽  
Guillaume Sartori ◽  
Gérald Enderlin ◽  
Christophe Len
Keyword(s):  
Pure Water ◽  
Cross Coupling ◽  
Microwave Assisted ◽  
Ligand Free

ChemInform Abstract: Improved Microwave-Assisted Ligand-Free Suzuki-Miyaura Cross-Coupling of 5-Iodo-2′-deoxyuridine in Pure Water.

ChemInform ◽  
2013 ◽  
Vol 44 (48) ◽  
pp. no-no
Author(s):  
Shawn Gallagher-Duval ◽  
Gwenaelle Herve ◽  
Guillaume Sartori ◽  
Gerald Enderlin ◽  
Christophe Len
Keyword(s):  
Pure Water ◽  
Cross Coupling ◽  
Microwave Assisted ◽  
Ligand Free

First ligand-free, microwave-assisted, Heck cross-coupling reaction in pure water on a nucleoside – application to the synthesis of antiviral BVDU

RSC Advances ◽  
2014 ◽  
Vol 4 (87) ◽  
pp. 46926-46929 ◽  
Author(s):  
Gwénaëlle Hervé ◽  
Christophe Len
Keyword(s):  
Pure Water ◽  
Coupling Reaction ◽  
Cross Coupling ◽  
Microwave Assisted ◽  
Cross Coupling Reaction ◽  
Ligand Free ◽  
Palladium Catalyzed ◽  
Microwave Assistance ◽  
First Time

For the first time, a palladium catalyzed Heck cross-coupling reaction between 5-iodo-2′-deoxyuridine and various acrylate derivatives was performed using ligand-free conditions and microwave assistance in pure water.

Original access to 5-aryluracils from 5-iodo-2′-deoxyuridine via a microwave assisted Suzuki-Miyaura cross-coupling/deglycosylation sequence in pure water

RSC Advances ◽  
2014 ◽  
Vol 4 (86) ◽  
pp. 46218-46223 ◽  
Author(s):  
T. Lussier ◽  
G. Hervé ◽  
G. Enderlin ◽  
C. Len
Keyword(s):  
Microwave Irradiation ◽  
Pure Water ◽  
Coupling Reaction ◽  
Cross Coupling ◽  
Microwave Assisted ◽  
Cross Coupling Reaction ◽  
Ligand Free

A facile and efficient methodology to obtain various 5-aryluracil derivatives was developed through a two steps sequence: a ligand-free Suzuki-Miyaura cross-coupling reaction starting from totally deprotected 5-iodo-(2′-deoxy)uridine followed by a very simple deglycosylation procedure in pure water with assistance of microwave irradiation.

ChemInform Abstract: Solid-Supported Rhodium(0) Nano-/Microparticles: An Efficient Ligand-Free Heterogeneous Catalyst for Microwave-Assisted Suzuki-Miyaura Cross-Coupling Reaction.

ChemInform ◽  
2013 ◽  
Vol 44 (15) ◽  
pp. no-no
Author(s):  
Nitul Ranjan Guha ◽  
Chennayala Bal Reddy ◽  
Nidhi Aggarwal ◽  
Dharminder Sharma ◽  
Arun K. Shil ◽  
...  
Keyword(s):  
Heterogeneous Catalyst ◽  
Coupling Reaction ◽  
Cross Coupling ◽  
Microwave Assisted ◽  
Cross Coupling Reaction ◽  
Ligand Free

Microwave-assisted synthesis of new fluorescent indoline-based building blocks by ligand free Suzuki-Miyaura cross-coupling reaction in aqueous media

Tetrahedron ◽  
2016 ◽  
Vol 72 (22) ◽  
pp. 2955-2963 ◽  
Author(s):  
Živilė Žukauskaitė ◽  
Vida Buinauskaitė ◽  
Joana Solovjova ◽  
Lina Malinauskaitė ◽  
Aistė Kveselytė ◽  
...  
Keyword(s):  
Aqueous Media ◽  
Coupling Reaction ◽  
Cross Coupling ◽  
Building Blocks ◽  
Microwave Assisted Synthesis ◽  
Microwave Assisted ◽  
Cross Coupling Reaction ◽  
Ligand Free

ChemInform Abstract: Microwave-Assisted Solvent- and Ligand-Free Copper-Catalyzed Cross-Coupling Between Halopyridines and Nitrogen Nucleophiles.

ChemInform ◽  
2011 ◽  
Vol 42 (22) ◽  
pp. no-no
Author(s):  
Zhen-Jiang Liu ◽  
Jean-Pierre Vors ◽  
Ernst R. F. Gesing ◽  
Carsten Bolm
Keyword(s):  
Cross Coupling ◽  
Microwave Assisted ◽  
Ligand Free ◽  
Nitrogen Nucleophiles

PdCuCeO–TPAB: a new catalytic system for quasi-heterogeneous Suzuki–Miyaura cross-coupling reactions under ligand-free conditions in water

2017 ◽  
Vol 41 (22) ◽  
pp. 13560-13566 ◽  
Author(s):  
Philani P. Mpungose ◽  
Neo I. Sehloko ◽  
Glenn E. M. Maguire ◽  
Holger B. Friedrich
Keyword(s):  
Catalytic System ◽  
Pure Water ◽  
Cross Coupling ◽  
Coupling Reactions ◽  
Cross Coupling Reactions ◽  
Highly Active ◽  
Ligand Free

PdCuCeO was applied for Suzuki–Miyaura coupling in pure water. The catalyst was highly active (TOF > 3000 h−1) and could be reused.

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