Off-line hyphenation of molecularly imprinted magnetic nanoparticle-based extraction with large volume sample stacking capillary electrophoresis for high-sensitivity detection of trace chloro-phenols

2014 ◽  
Vol 6 (4) ◽  
pp. 1219 ◽  
Author(s):  
Shengda Qi ◽  
Huige Zhang ◽  
Qian Zhu ◽  
Hongli Chen ◽  
Yalei Dong ◽  
...  
2017 ◽  
Vol 89 (22) ◽  
pp. 12375-12382 ◽  
Author(s):  
Amit V. Patel ◽  
Takayuki Kawai ◽  
Liping Wang ◽  
Stanislav S. Rubakhin ◽  
Jonathan V. Sweedler

2003 ◽  
Vol 486 (2) ◽  
pp. 183-190 ◽  
Author(s):  
G Álvarez-Llamas ◽  
A Rodrı́guez-Cea ◽  
M.R Fernández de la Campa ◽  
A Sanz-Medel

2019 ◽  
Vol 11 (11) ◽  
pp. 1558-1565 ◽  
Author(s):  
Yan Zhang ◽  
Yating Zhang ◽  
Luqi Zhu ◽  
Pingang He ◽  
Qingjiang Wang

A sensitive strategy developed for the detection of Escherichia coli (E. coli) by microchip capillary electrophoresis (MCE) combined with laser-induced fluorescence (LIF) is described in this paper.


2018 ◽  
Vol 2018 ◽  
pp. 1-7 ◽  
Author(s):  
Gabriela Islas ◽  
Jose A. Rodriguez ◽  
Irma Perez-Silva ◽  
Jose M. Miranda ◽  
Israel S. Ibarra

Solid-phase extraction in combination with large-volume sample stacking-capillary electrophoresis (SPE-LVSS-CE) was applied to measure chlortetracycline, doxycycline, oxytetracycline, and tetracycline in milk samples. Under optimal conditions, the proposed method had a linear range of 29 to 200 µg·L−1, with limits of detection ranging from 18.6 to 23.8 µg·L−1 with inter- and intraday repeatabilities < 10% (as a relative standard deviation) in all cases. The enrichment factors obtained were from 50.33 to 70.85 for all the TCs compared with a conventional capillary zone electrophoresis (CZE). This method is adequate to analyze tetracyclines below the most restrictive established maximum residue limits. The proposed method was employed in the analysis of 15 milk samples from different brands. Two of the tested samples were positive for the presence of oxytetracycline with concentrations of 95 and 126 µg·L−1. SPE-LVSS-CE is a robust, easy, and efficient strategy for online preconcentration of tetracycline residues in complex matrices.


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