New insight into the nanostructure of ionic liquids: a small angle X-ray scattering (SAXS) study on liquid tri-alkyl-methyl-ammonium bis(trifluoromethanesulfonyl)amides and their mixtures

2009 ◽  
Vol 11 (26) ◽  
pp. 5469 ◽  
Author(s):  
Tanja Pott ◽  
Philippe Méléard
Keyword(s):  
Ionic Liquids ◽  
Small Angle ◽  
X Ray ◽  
X Ray Scattering ◽  
Insight Into ◽  
Ray Scattering

A new insight into the nanostructure of alkylammonium alkanoates based ionic liquids in water

2016 ◽  
Vol 18 (16) ◽  
pp. 11497-11502 ◽  
Author(s):  
Umme Salma ◽  
Paolo Ballirano ◽  
Marianna Usula ◽  
Ruggero Caminiti ◽  
Natalia V. Plechkova ◽  
...  
Keyword(s):  
Ionic Liquids ◽  
Small Angle ◽  
Alkyl Chain ◽  
X Ray ◽  
X Ray Scattering ◽  
Chain Lengths ◽  
Insight Into ◽  
Ray Scattering

In this paper, small angle X-ray scattering has been used to study a series of ionic liquids, alkylammonium alkanoates ([N0 0 0 n][CmCO2]), with varying alkyl chain lengths in the cation and the anion.

Amphiphilic nanostructure in choline carboxylate and amino acid ionic liquids and solutions

2020 ◽  
Vol 22 (6) ◽  
pp. 3490-3498 ◽  
Author(s):  
Shurui Miao ◽  
Rob Atkin ◽  
Gregory G. Warr
Keyword(s):  
Ionic Liquids ◽  
Amino Acid ◽  
Small Angle ◽  
X Ray ◽  
X Ray Scattering ◽  
Ray Scattering

The liquid structures of six choline carboxylate/amino acid ionic liquids (bio-ILs) and their mixtures with water and various n-alkanols have been investigated by small-angle X-ray scattering (SAXS).

Insight into Asphaltene Nanoaggregate Structure Inferred by Small Angle Neutron and X-ray Scattering

2011 ◽  
Vol 115 (21) ◽  
pp. 6827-6837 ◽  
Author(s):  
Joëlle Eyssautier ◽  
Pierre Levitz ◽  
Didier Espinat ◽  
Jacques Jestin ◽  
Jérémie Gummel ◽  
...  
Keyword(s):  
Small Angle ◽  
X Ray ◽  
X Ray Scattering ◽  
Insight Into ◽  
Ray Scattering

Small-Angle X-ray Scattering Study of Water Free Fuel Cell Membranes Containing Ionic Liquids†

2010 ◽  
Vol 22 (3) ◽  
pp. 803-812 ◽  
Author(s):  
S. S. Sekhon ◽  
Jin-Soo Park ◽  
Ji-Suk Baek ◽  
Sung-Dae Yim ◽  
Tae-Hyun Yang ◽  
...  
Keyword(s):  
Ionic Liquids ◽  
Fuel Cell ◽  
Small Angle ◽  
Cell Membranes ◽  
Fuel Cell Membranes ◽  
X Ray ◽  
X Ray Scattering ◽  
Scattering Study ◽  
Ray Scattering

scholarly journals Thermoresponsive polymer assemblies via variable temperature liquid-phase transmission electron microscopy and small angle X-ray scattering

2021 ◽  
Vol 12 (1) ◽  
Author(s):  
Joanna Korpanty ◽  
Lucas R. Parent ◽  
Nicholas Hampu ◽  
Steven Weigand ◽  
Nathan C. Gianneschi
Keyword(s):  
Electron Microscopy ◽  
Transmission Electron Microscopy ◽  
Small Angle ◽  
Variable Temperature ◽  
X Ray ◽  
X Ray Scattering ◽  
Transmission Electron ◽  
Temperature Liquid ◽  
Insight Into ◽  
Ray Scattering

AbstractHerein, phase transitions of a class of thermally-responsive polymers, namely a homopolymer, diblock, and triblock copolymer, were studied to gain mechanistic insight into nanoscale assembly dynamics via variable temperature liquid-cell transmission electron microscopy (VT-LCTEM) correlated with variable temperature small angle X-ray scattering (VT-SAXS). We study thermoresponsive poly(diethylene glycol methyl ether methacrylate) (PDEGMA)-based block copolymers and mitigate sample damage by screening electron flux and solvent conditions during LCTEM and by evaluating polymer survival via post-mortem matrix-assisted laser desorption/ionization imaging mass spectrometry (MALDI-IMS). Our multimodal approach, utilizing VT-LCTEM with MS validation and VT-SAXS, is generalizable across polymeric systems and can be used to directly image solvated nanoscale structures and thermally-induced transitions. Our strategy of correlating VT-SAXS with VT-LCTEM provided direct insight into transient nanoscale intermediates formed during the thermally-triggered morphological transformation of a PDEGMA-based triblock. Notably, we observed the temperature-triggered formation and slow relaxation of core-shell particles with complex microphase separation in the core by both VT-SAXS and VT-LCTEM.

Insight into the nanostructure of anisotropic cellulose aerogels upon compression

Soft Matter ◽  
2019 ◽  
Vol 15 (41) ◽  
pp. 8372-8380 ◽  
Author(s):  
Harald Rennhofer ◽  
Sven F. Plappert ◽  
Helga C. Lichtenegger ◽  
Sigrid Bernstorff ◽  
Michael Fitzka ◽  
...  
Keyword(s):  
Small Angle ◽  
Compressive Strain ◽  
Cellulose Ii ◽  
Stress Strain ◽  
X Ray ◽  
X Ray Scattering ◽  
Insight Into ◽  
Ray Scattering

In this article we report on the nanostructural changes of a cellulose II aerogel network during compressive strain of up to 80%, which are investigated by in situ small angle X-ray scattering and linked to the corresponding stress–strain curves.

Small-Angle X-Ray Scattering of Ionic Liquids

2015 ◽  
pp. 169-213 ◽  
Author(s):  
Joshua A. Hammons ◽  
Jan Ilavsky ◽  
Fan Zhang
Keyword(s):  
Ionic Liquids ◽  
Small Angle ◽  
X Ray ◽  
X Ray Scattering ◽  
Ray Scattering

Lysozyme conformational changes with ionic liquids: Spectroscopic, small angle x-ray scattering and crystallographic study

2021 ◽  
Vol 585 ◽  
pp. 433-443
Author(s):  
Qi Han ◽  
Kate M. Smith ◽  
Connie Darmanin ◽  
Timothy M. Ryan ◽  
Calum J. Drummond ◽  
...  
Keyword(s):  
Ionic Liquids ◽  
Conformational Changes ◽  
Small Angle ◽  
X Ray ◽  
X Ray Scattering ◽  
Crystallographic Study ◽  
Ray Scattering
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