Application of high-energy polarised beam energy dispersive X-ray fluorescence spectrometry to cadmium determination in saline solutions

2008 ◽  
Vol 23 (7) ◽  
pp. 1034 ◽  
Author(s):  
Katleen Van Meel ◽  
Clàudia Fontàs ◽  
René Van Grieken ◽  
Ignasi Queralt ◽  
Manuela Hidalgo ◽  
...  
Keyword(s):  
Beam Energy ◽  
High Energy ◽  
Energy Dispersive ◽  
Fluorescence Spectrometry ◽  
Cadmium Determination ◽  
X Ray ◽  
Saline Solutions

scholarly journals Major and trace element analyses of igneous rocks by polarizing energy dispersive X-ray fluorescence spectrometry (EDXRF)

2014 ◽  
Vol 43 (2) ◽  
pp. 47-53 ◽  
Author(s):  
Toshio MIYAZAKI ◽  
Shin-ichi YAMASAKI ◽  
Noriyoshi TSUCHIYA ◽  
Satoshi OKUMURA ◽  
Ryoichi YAMADA ◽  
...  
Keyword(s):  
Trace Element ◽  
Igneous Rocks ◽  
Energy Dispersive ◽  
Fluorescence Spectrometry ◽  
X Ray

Phase composition depth profiles using spatially resolved energy dispersive X-ray diffraction

2004 ◽  
Vol 37 (6) ◽  
pp. 967-976 ◽  
Author(s):  
Andrew C. Jupe ◽  
Stuart R. Stock ◽  
Peter L. Lee ◽  
Nikhila N. Naik ◽  
Kimberly E. Kurtis ◽  
...  
Keyword(s):  
Phase Composition ◽  
Spatial Resolution ◽  
Zinc Coating ◽  
High Energy ◽  
Sulfate Attack ◽  
Energy Dispersive ◽  
X Ray Diffraction ◽  
X Ray ◽  
Spatially Resolved ◽  
Composition Profiles

Spatially resolved energy dispersive X-ray diffraction, using high-energy synchrotron radiation (∼35–80 keV), was used nondestructively to obtain phase composition profiles along the radii of cylindrical cement paste samples to characterize the progress of the chemical changes associated with sulfate attack on the cement. Phase distributions were acquired to depths of ∼4 mm below the specimen surface with sufficient spatial resolution to discern features less than 200 µm thick. The experimental and data analysis methods employed to obtain quantitative composition profiles are described. The spatial resolution that could be achieved is illustrated using data obtained from copper cylinders with a thin zinc coating. The measurements demonstrate that this approach is useful for nondestructively visualizing the sometimes complex transformations that take place during sulfate attack on cement-based materials. These transformations can be spatially related to microstructure as seen by computed microtomography.

An energy dispersive X-ray fluorescence spectrometry approach for the identification of geographical origin of wheat flour

2021 ◽  
Vol 0 (0) ◽  
Author(s):  
Tong Chen ◽  
Xingpu Qi ◽  
Zaiyong Si ◽  
Qianwei Cheng ◽  
Hui Chen
Keyword(s):  
Principal Component Analysis ◽  
Wheat Flour ◽  
Principal Component ◽  
Component Analysis ◽  
Mineral Elements ◽  
Energy Dispersive ◽  
Fluorescence Spectrometry ◽  
Energy Channel ◽  
X Ray ◽  
Different Origins

Abstract In this work, a method was established for discriminating geographical origins of wheat flour based on energy dispersive X-ray fluorescence spectrometry (ED-XRF) and chemometrics. 68 wheat flour samples from three different origins were collected and analyzed using ED-XRF technology. Firstly, the principal component analysis method was applied to analyze the feasibility of discrimination and reduce data dimensionality. Then, Competitive Adaptive Reweighted Sampling (CARS) was used to further extract feature variables, and 12 energy variables (corresponding to mineral elements) were identified and selected to characterize the geographical attributes of wheat flour samples. Finally, a non-linear model was constructed using principal component analysis and quadratic discriminant analysis (QDA). The CARS-PCA-QDA model showed that the accuracy of five-fold cross-validation was 84.25%. The results showed that the established method was able to select important energy channel variables effectively and wheat flour could be classified based on geographical origins with chemometrics, which could provide a theoretical basis for unveiling the relationship between mineral element composition and wheat origin.

Determination of parts per billion levels of electrodeposited metals by energy dispersive x-ray fluorescence spectrometry

1977 ◽  
Vol 49 (12) ◽  
pp. 1734-1737 ◽  
Author(s):  
John A. Boslett ◽  
Robert L. R. Towns ◽  
Robert G. Megargle ◽  
Karl H. Pearson ◽  
Thomas C. Furnas
Keyword(s):  
Energy Dispersive ◽  
Fluorescence Spectrometry ◽  
X Ray
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