Preconcentration and determination of trace elements with 2,6-diacetylpyridine functionalized Amberlite XAD-4 by flow injection and atomic spectroscopy

The Analyst ◽  
2005 ◽  
Vol 130 (11) ◽  
pp. 1518 ◽  
Author(s):  
Derya Kara ◽  
Andrew Fisher ◽  
Steve J. Hill
Keyword(s):  
Trace Elements ◽  
Flow Injection ◽  
Atomic Spectroscopy

Determination of Trace Elements in Serum Using Inductively Coupled Plasma Atomic Spectroscopy with Hydride Generation and Chelating Resin Preconcentration

1984 ◽  
Vol 38 (5) ◽  
pp. 635-644 ◽  
Author(s):  
Zhuang Mianzhi ◽  
Ramon M. Barnes
Keyword(s):  
Trace Elements ◽  
Inductively Coupled Plasma ◽  
Hydride Generation ◽  
Atomic Spectroscopy ◽  
Chelating Resin ◽  
Plasma Emission ◽  
Inductively Coupled ◽  
Human Sera ◽  
Sera Samples

A procedure is described for the inductively coupled plasma emission spectroscopic determination of Cd, Co, Cu, Fe, Mo, V, and Zn in < 1 mL of serum after digestion in nitric and perchloric acids and preconcentration with a poly(dithiocarbamate) resin Recoveries are 91 to 106% The determination of As and Se in serum by hydride generation and ICP-AES is performed after the interference of Cu on Se hydride generation was reduced by complexation of the Cu with poly(acrylamidoxime) resin Verification with NBS-SRMs as well as with human sera samples is reported

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