Facile synthesis and structural variation of novel heterobimetallic alkali metal–zinc-alkoxide and -siloxide clusters

2003 ◽  
pp. 3365-3369 ◽  
Author(s):  
Klaus Merz ◽  
Stefan Block ◽  
Robert Schoenen ◽  
Matthias Driess
Keyword(s):  
Alkali Metal ◽  
Structural Variation ◽  
Facile Synthesis

Heavy Alkali Metal Arenedithiocarboxylates:  A Facile Synthesis, Dimeric Structure, and Nonbonding Interaction between the Metals and Aromatic Ring Carbons

1999 ◽  
Vol 38 (3) ◽  
pp. 496-506 ◽  
Author(s):  
Shinzi Kato ◽  
Nobuyuki Kitaoka ◽  
Osamu Niyomura ◽  
Yuka Kitoh ◽  
Takahiro Kanda ◽  
...  
Keyword(s):  
Alkali Metal ◽  
Aromatic Ring ◽  
Facile Synthesis ◽  
Dimeric Structure ◽  
Nonbonding Interaction

scholarly journals Facile Synthesis of Nanosized Magnesium-Aluminium Layered Double Hydroxides

2021 ◽  
Vol 42 (1) ◽  
pp. 39-44
Author(s):  
Kedar Nath Dhakal ◽  
Girja Mani Aryal ◽  
Hari Sharan Adhikari ◽  
Rameshwar Adhikari
Keyword(s):  
Layered Double Hydroxides ◽  
Structural Variation ◽  
Practical Importance ◽  
Chemistry Laboratory ◽  
X Ray Diffraction ◽  
Facile Synthesis ◽  
X Ray ◽  
University Level ◽  
Xrd Techniques ◽  
Double Hydroxides

We report facile methods of preparing nanosized hydrotalcite-like compounds, the layered double hydroxides (LDH), with ordinary chemistry laboratory settings to educate the young scientists from high schools to undergraduate university level fostering their research interest in preparing these nanomaterials of practical importance. Coprecipitation and urea hydrolysis methods have been recommended as facile routes of preparing the magnesium-aluminum layered double hydroxides (Mg-Al LDHs). The LDH thus prepared were characterized by Fourier transform infrared (FTIR) spectroscopic and powder X-ray diffraction (XRD) techniques. The observed weakening of some FTIR peaks and XRD planes shifting concerning standard JCPDS 89-5434 data implied the slight structural variation of the compounds and the presence of impurities. The average grain diameter of LDH particles was found in the range of 20 to 60 nm.

Facile Synthesis of Unsolvated Alkali Metal Octahydrotriborate Salts MB 3 H 8 (M=K, Rb, and Cs), Mechanisms of Formation, and the Crystal Structure of KB 3 H 8

2019 ◽  
Vol 131 (9) ◽  
pp. 2746-2750 ◽  
Author(s):  
Xi‐Meng Chen ◽  
Nana Ma ◽  
Xin‐Ran Liu ◽  
Changgeng Wei ◽  
Chong‐Chao Cui ◽  
...  
Keyword(s):  
Crystal Structure ◽  
Alkali Metal ◽  
Facile Synthesis ◽  
Mechanisms Of Formation
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