Segmental dynamics in the crystalline phase of nylon 66: solid state deuterium NMR

1990 ◽  
Vol 23 (8) ◽  
pp. 2153-2169 ◽  
Author(s):  
J. Hirschinger ◽  
H. Miura ◽  
K. H. Gardner ◽  
Alan D. English
Keyword(s):  
Solid State ◽  
Crystalline Phase ◽  
Deuterium Nmr ◽  
Nylon 66 ◽  
Segmental Dynamics

Segmental dynamics in the amorphous phase of nylon 66: solid state deuterium NMR

1990 ◽  
Vol 23 (8) ◽  
pp. 2169-2182 ◽  
Author(s):  
H. Miura ◽  
J. Hirschinger ◽  
Alan D. English
Keyword(s):  
Solid State ◽  
Amorphous Phase ◽  
Deuterium Nmr ◽  
Nylon 66 ◽  
Segmental Dynamics

Segmental Dynamics of Solid-State Poly(methylphenylsilane) by 1D and 2D Deuterium NMR

1998 ◽  
Vol 31 (15) ◽  
pp. 4852-4861 ◽  
Author(s):  
Robert D. O'Connor ◽  
Frank D. Blum ◽  
Eric Ginsburg ◽  
Robert D. Miller
Keyword(s):  
Solid State ◽  
Deuterium Nmr ◽  
Segmental Dynamics

Determination of the charge of Al13 Keggin oligocations intercalated into synthetic hectorite

2019 ◽  
Vol 74 (1) ◽  
pp. 85-90
Author(s):  
Marius Schöttle ◽  
Dominik Schuchardt ◽  
Andreas Edenharter ◽  
Sebastian Koch ◽  
Jürgen Senker ◽  
...  
Keyword(s):  
Reaction Time ◽  
Solid State ◽  
Ir Spectroscopy ◽  
Cation Exchange ◽  
Elemental Analysis ◽  
Crystalline Phase ◽  
Solid State Nmr ◽  
Liquid Crystalline ◽  
A Charge

AbstractApplying a nematic liquid crystalline phase of a synthetic Na-hectorite with layer separations >100 nm, the reaction time for pillaring with Al13 Keggin oligocation could be reduced to seconds ensuring that cation exchange is controlled by thermodynamics. With this material at hand we are able to resolve the long-standing dispute regarding the charge of intercalated Keggin oligocations. Micropore sizes as determined by physisorption isotherms, adsorption isotherms obtained via elemental analysis, and results of 27Al solid-state NMR and pyridine probe IR spectroscopy favor a charge of +7 for the Al13 pillars intercalated into hectorite unaltered.

Dynamic studies of s-trioxane in the solid state and in liquid crystalline solutions by deuterium NMR

1990 ◽  
Vol 94 (25) ◽  
pp. 8845-8850 ◽  
Author(s):  
E. Gelerinter ◽  
Zeev. Luz ◽  
R. Poupko ◽  
H. Zimmermann
Keyword(s):  
Solid State ◽  
Liquid Crystalline ◽  
Deuterium Nmr ◽  
Dynamic Studies

Synthesis of Deuterium-Labeled Plant Sterols and Analysis of Their Side-Chain Mobility by Solid State Deuterium NMR

1996 ◽  
Vol 61 (13) ◽  
pp. 4252-4257 ◽  
Author(s):  
Mary-Pierre Marsan ◽  
William Warnock ◽  
Isabelle Muller ◽  
Yoichi Nakatani ◽  
Guy Ourisson ◽  
...  
Keyword(s):  
Solid State ◽  
Plant Sterols ◽  
Side Chain ◽  
Deuterium Nmr ◽  
Chain Mobility
Sign in / Sign up

Export Citation Format

Share Document