Orientation and Lattice Structure of Microcrystals of Colloidal Silica Particles in Dispersions Observed by Ultra-small-Angle X-ray Scattering

Langmuir ◽  
1997 ◽  
Vol 13 (19) ◽  
pp. 5007-5010 ◽  
Author(s):  
Toshiki Konishi ◽  
Norio Ise
Langmuir ◽  
1996 ◽  
Vol 12 (10) ◽  
pp. 2608-2610 ◽  
Author(s):  
Toshiki Konishi ◽  
Eiji Yamahara ◽  
Norio Ise

2019 ◽  
Vol 92 (4) ◽  
pp. 152-157
Author(s):  
Tomotaka NAKATANI ◽  
Shinji KOHARA ◽  
Taiki HOSHINO ◽  
So FUJINAMI ◽  
Masaki TAKATA

2008 ◽  
Vol 47 (5-6) ◽  
pp. 537-541 ◽  
Author(s):  
Katsumi Hagita ◽  
Takashi Arai ◽  
Hiroyuki Kishimoto ◽  
Norimasa Umesaki ◽  
Hiroya Suno ◽  
...  

1997 ◽  
Vol 30 (5) ◽  
pp. 854-856 ◽  
Author(s):  
T. Konishi ◽  
E. Yamahara ◽  
T. Furuta ◽  
N. Ise

A two-dimensional ultra-small-angle X-ray scattering (USAXS) apparatus was constructed using a rotating-anode X-ray generator and a Bonse–Hart camera. In this camera, two sets of two channel-cut single crystals were used to collimate the X-ray beam in both the horizontal and the vertical planes. The measured intensity profile of the direct beam showed a high small-angle resolution in all directions on the detector plane. The full width at half-maximum was 17′′, indicating that the apparatus can be applied to structural analysis in the range up to 2 μm, even for directionally oriented samples. One- and two-dimensional USAXS profiles from colloidal silica powder agreed well with each other, showing that the desmearing procedure adopted in the previous one-dimensional USAXS experiments were justified.


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