Rapid Screening and Identification of New Soluble Tannin–Salivary Protein Aggregates in Saliva by Mass Spectrometry (MALDI-TOF-TOF and FIA-ESI-MS)

Langmuir ◽  
2014 ◽  
Vol 30 (28) ◽  
pp. 8528-8537 ◽  
Author(s):  
M. R. Perez-Gregorio ◽  
N. Mateus ◽  
V. de Freitas
2019 ◽  
Vol 43 (7) ◽  
pp. 528-535 ◽  
Author(s):  
Fathiah A Zubaidi ◽  
Yeun-Mun Choo ◽  
Guan-Huat Tan ◽  
Hamimah Abd Hamid ◽  
Yap Ken Choy

Abstract A novel mass spectrometry detection technique based on a multi-period and multi- experiment (MRM-EPI-MRM3) with library matching in a single run for fast and rapid screening and identification of amphetamine type stimulants (ATS) related drugs in whole blood, urine and dried blood stain was developed and validated. The ATS-related drugs analyzed in this study include ephedrine, pseudoephedrine, amphetamine, methamphetamine, MDMA (3,4-Methylenedioxymethamphetamine), MDA (3,4-Methylenedioxyamphetamine), MDEA (3,4-Methylenedioxy-N-ethylamphetamine) and phentermine. The relative standard deviation for inter and intraday was less than 15% while recoveries ranged from 80% to 120% for all three matrices, i.e., whole blood, urine and dried blood stain. All compounds gave library matching percentage of more than 85% based on the purity. This method was proven to be simple and robust, and provide high confident results complemented with library matching confirmation.


2016 ◽  
Vol 203 ◽  
pp. 521-529 ◽  
Author(s):  
Sima Kumari ◽  
R. Elancheran ◽  
Jibon Kotoky ◽  
Rajlakshmi Devi

2006 ◽  
Vol 17 (4) ◽  
pp. 490-499 ◽  
Author(s):  
Xu Zhang ◽  
Mark Scalf ◽  
Travis W. Berggren ◽  
Michael S. Westphall ◽  
Lloyd M. Smith

Sign in / Sign up

Export Citation Format

Share Document