Combined Cryogenic Transmission Electron Microscopy and Electron Spin Resonance Studies of Egg Phosphatidylcholine Liposomes Loaded with a Carboranyl Compound Intended for Boron Neutron Capture Therapy

Langmuir ◽  
2003 ◽  
Vol 19 (14) ◽  
pp. 5608-5617 ◽  
Author(s):  
Simona Rossi ◽  
Göran Karlsson ◽  
Giacomo Martini ◽  
Katarina Edwards
Keyword(s):  
Electron Microscopy ◽  
Transmission Electron Microscopy ◽  
Electron Spin Resonance ◽  
Neutron Capture ◽  
Neutron Capture Therapy ◽  
Phosphatidylcholine Liposomes ◽  
Cryogenic Transmission Electron Microscopy ◽  
Boron Neutron Capture ◽  
Transmission Electron ◽  
Spin Resonance

Transmission Electron Microscopy of Shock-Modified and Annealed Rutile

1983 ◽  
Vol 24 ◽  
Author(s):  
M. J. Carr ◽  
R. A. Graham ◽  
B. Morosin ◽  
E. L. Venturini
Keyword(s):  
Electron Microscopy ◽  
Transmission Electron Microscopy ◽  
Electron Spin Resonance ◽  
Electron Spin ◽  
Shock Treatment ◽  
Line Broadening ◽  
Annealing Behavior ◽  
X Ray ◽  
Transmission Electron ◽  
Spin Resonance

ABSTRACTThe annealing behavior of shock modified rutile (TiO2) powder was studied by transmission electron microscopy, x-ray line broadening, and electron spin resonance. Specimens were examined in the as-received and as-shocked conditions, and in shocked and annealed conditions after one hour at 475° or 1000°C. The dislocations generated by the shock treatment were found to persist essentially unaltered through the 475°C anneal. Substantial recovery was observed after the 1000°C anneal.

scholarly journals Probing the Na metal solid electrolyte interphase via cryo-transmission electron microscopy

2021 ◽  
Vol 12 (1) ◽  
Author(s):  
Bing Han ◽  
Yucheng Zou ◽  
Zhen Zhang ◽  
Xuming Yang ◽  
Xiaobo Shi ◽  
...  
Keyword(s):  
Electron Microscopy ◽  
Transmission Electron Microscopy ◽  
Solid Electrolyte ◽  
Solid Electrolyte Interphase ◽  
Metal Electrode ◽  
Liquid Electrolyte ◽  
Battery Materials ◽  
Cryogenic Transmission Electron Microscopy ◽  
Transmission Electron ◽  
Fluoroethylene Carbonate

AbstractCryogenic transmission electron microscopy (cryo-TEM) is a valuable tool recently proposed to investigate battery electrodes. Despite being employed for Li-based battery materials, cryo-TEM measurements for Na-based electrochemical energy storage systems are not commonly reported. In particular, elucidating the chemical and morphological behavior of the Na-metal electrode in contact with a non-aqueous liquid electrolyte solution could provide useful insights that may lead to a better understanding of metal cells during operation. Here, using cryo-TEM, we investigate the effect of fluoroethylene carbonate (FEC) additive on the solid electrolyte interphase (SEI) structure of a Na-metal electrode. Without FEC, the NaPF6-containing carbonate-based electrolyte reacts with the metal electrode to produce an unstable SEI, rich in Na2CO3 and Na3PO4, which constantly consumes the sodium reservoir of the cell during cycling. When FEC is used, the Na-metal electrode forms a multilayer SEI structure comprising an outer NaF-rich amorphous phase and an inner Na3PO4 phase. This layered structure stabilizes the SEI and prevents further reactions between the electrolyte and the Na metal.

scholarly journals Alpha helical surfactant-like peptides self-assemble into pH-dependent nanostructures

Soft Matter ◽  
2021 ◽  
Vol 17 (11) ◽  
pp. 3096-3104
Author(s):  
Valeria Castelletto ◽  
Jani Seitsonen ◽  
Janne Ruokolainen ◽  
Ian W. Hamley
Keyword(s):  
Electron Microscopy ◽  
Transmission Electron Microscopy ◽  
Small Angle ◽  
Self Assembly ◽  
X Ray ◽  
Cryogenic Transmission Electron Microscopy ◽  
X Ray Scattering ◽  
Transmission Electron ◽  
Ph Dependent ◽  
Ray Scattering

A designed surfactant-like peptide is shown, using a combination of cryogenic-transmission electron microscopy and small-angle X-ray scattering, to have remarkable pH-dependent self-assembly properties.

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