A Simple Continuous Flow Microwave Reactor

2005 ◽  
Vol 70 (17) ◽  
pp. 7003-7006 ◽  
Author(s):  
Mark C. Bagley ◽  
Robert L. Jenkins ◽  
M. Caterina Lubinu ◽  
Christopher Mason ◽  
Robin Wood
Keyword(s):  
Continuous Flow ◽  
Microwave Reactor

ChemInform Abstract: Petasis Olefination in a Continuous-Flow Microwave Reactor: exo-Glycals from Sugar Lactones.

ChemInform ◽  
2011 ◽  
Vol 43 (2) ◽  
pp. no-no
Author(s):  
Stefan Koch ◽  
Holger Loewe ◽  
Horst Kunz
Keyword(s):  
Continuous Flow ◽  
Microwave Reactor

scholarly journals Sonochemical preparation of alumina-spheres loaded with Pd nanoparticles for 2-butyne-1,4-diol semi-hydrogenation in a continuous flow microwave reactor

RSC Advances ◽  
2018 ◽  
Vol 8 (13) ◽  
pp. 7029-7039 ◽  
Author(s):  
Emanuela Calcio Gaudino ◽  
Maela Manzoli ◽  
Diego Carnaroglio ◽  
Zhilin Wu ◽  
Giorgio Grillo ◽  
...  
Keyword(s):  
Heterogeneous Catalysis ◽  
Continuous Flow ◽  
Flow Reactor ◽  
Pd Nanoparticles ◽  
Microwave Assisted ◽  
Continuous Flow Reactor ◽  
Microwave Reactor

A novel protocol for microwave-assisted alkyne semi-hydrogenation under heterogeneous catalysis in a continuous flow reactor is reported herein.

A Commercial Continuous Flow Microwave Reactor Evaluated for Scale-Up

2010 ◽  
Vol 14 (4) ◽  
pp. 926-930 ◽  
Author(s):  
Fabio Bergamelli ◽  
Mauro Iannelli ◽  
Jameel A. Marafie ◽  
Jonathan D. Moseley
Keyword(s):  
Continuous Flow ◽  
Scale Up ◽  
Microwave Reactor

Petasis Olefination in a Continuous-Flow Microwave Reactor: exo-Glycals from Sugar Lactones

Synlett ◽  
2011 ◽  
Vol 2011 (14) ◽  
pp. 1978-1982 ◽  
Author(s):  
Horst Kunz ◽  
Stefan Koch ◽  
Holger Löwe
Keyword(s):  
Continuous Flow ◽  
Microwave Reactor

Environmentally Benign Procedures for the Preparation and Isolation of 3-Methylcyclopent-2-en-1-one

1997 ◽  
Vol 50 (9) ◽  
pp. 921 ◽  
Author(s):  
Laurence Bagnell ◽  
Marianne Bliese ◽  
Teresa Cablewski ◽  
Christopher R. Strauss ◽  
John Tsanaktsidis
Keyword(s):  
Anion Exchange ◽  
Continuous Flow ◽  
Exchange Resin ◽  
Anion Exchange Resin ◽  
Batch Reactor ◽  
Environmentally Benign ◽  
Isolation Method ◽  
Preferential Adsorption ◽  
Microwave Reactor ◽  
Higher Temperature

A moderately yielding (50±4%) method for obtaining 3-methylcyclopent-2-en-1-one from hexane-2,5-dione in ≥99·5% purity was developed, using 2·1% (w/v) of aqueous KOH at reflux. However, the yield was increased to 80±5% by using considerably lower concentrations of base (<0·1%) and higher temperature (200°C) with a conventionally heated autoclave or a microwave batch reactor. The preparation was scaled up with a larger autoclave and also with a continuous flow microwave reactor. The dione impurity was removed from the enone by preferential adsorption on an anion-exchange resin in the bisulfite form. The product was recovered from the aqueous phase with a hydrophobic resin. This environmentally benign, non-extractive isolation method has potential for broad applicability in cleaner production.

scholarly journals Continuous flow synthesis of α-aryl-α-aminophosphonates

2019 ◽  
Vol 91 (1) ◽  
pp. 67-76 ◽  
Author(s):  
Erika Bálint ◽  
Ádám Tajti ◽  
Katalin Ladányi-Pára ◽  
Nóra Tóth ◽  
Béla Mátravölgyi ◽  
...  
Keyword(s):  
Continuous Flow ◽  
Reaction Times ◽  
Primary Amines ◽  
Flow Process ◽  
Flow Synthesis ◽  
Microwave Reactor ◽  
Dialkyl Phosphites ◽  
Benzaldehyde Derivatives

AbstractThe synthesis of α-aryl-α-aminophosphonates was performed by the three-component Kabachnik-Fields reaction of primary amines, benzaldehyde derivatives and dialkyl phosphites in a continuous flow microwave reactor. The target compounds could be obtained in high (~90%) yields without any catalyst in simple alcohols as the solvent. The flow process elaborated required shorter reaction times and lower excess of the reagent, as compared to the “traditional” batch reactions, and allowed the synthesis of the α-aminophosphonates on a somewhat larger scale.

Biodiesel production in a novel continuous flow microwave reactor

2015 ◽  
Vol 83 ◽  
pp. 25-29 ◽  
Author(s):  
I. Choedkiatsakul ◽  
K. Ngaosuwan ◽  
S. Assabumrungrat ◽  
S. Mantegna ◽  
G. Cravotto
Keyword(s):  
Continuous Flow ◽  
Biodiesel Production ◽  
Microwave Reactor

scholarly journals Translation of microwave methodology to continuous flow for the efficient synthesis of diaryl ethers via a base-mediated SNAr reaction

2011 ◽  
Vol 7 ◽  
pp. 1360-1371 ◽  
Author(s):  
Charlotte Wiles ◽  
Paul Watts
Keyword(s):  
Reaction Time ◽  
Continuous Flow ◽  
Stopped Flow ◽  
Efficient Synthesis ◽  
Diaryl Ethers ◽  
Microwave Reactor ◽  
Starting Point ◽  
Microreaction Technology ◽  
Snar Reaction ◽  
Rapid Reaction

Whilst microwave heating has been widely demonstrated as a synthetically useful tool for rapid reaction screening, a microwave-absorbing solvent is often required in order to achieve efficient reactant heating. In comparison, microreactors can be readily heated and pressurised in order to “super-heat” the reaction mixture, meaning that microwave-transparent solvents can also be employed. To demonstrate the advantages associated with microreaction technology a series of SNAr reactions were performed under continuous flow by following previously developed microwave protocols as a starting point for the investigation. By this approach, an automated microreaction platform (Labtrix® S1) was employed for the continuous flow synthesis of diaryl ethers at 195 °C and 25 bar, affording a reduction in reaction time from tens of minutes to 60 s when compared with a stopped-flow microwave reactor.

Single-Mode Microwave Reactor Used for Continuous Flow Reactions under Elevated Pressure

2013 ◽  
Vol 52 (12) ◽  
pp. 4683-4687 ◽  
Author(s):  
Masateru Nishioka ◽  
Masato Miyakawa ◽  
Yohei Daino ◽  
Haruki Kataoka ◽  
Hidekazu Koda ◽  
...  
Keyword(s):  
Continuous Flow ◽  
Single Mode ◽  
Elevated Pressure ◽  
Microwave Reactor
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