Paramagnetic Ions Enable Tuning of Nuclear Relaxation Rates and Provide Long-Range Structural Restraints in Solid-State NMR of Proteins

2009 ◽  
Vol 131 (23) ◽  
pp. 8108-8120 ◽  
Author(s):  
Philippe S. Nadaud ◽  
Jonathan J. Helmus ◽  
Stefanie L. Kall ◽  
Christopher P. Jaroniec
Keyword(s):  
Solid State ◽  
Long Range ◽  
Solid State Nmr ◽  
Nuclear Relaxation ◽  
Relaxation Rates ◽  
Paramagnetic Ions ◽  
Structural Restraints

Paramagnetic Ions Provide Structural Restraints in Solid-State NMR of Proteins

2007 ◽  
Vol 129 (8) ◽  
pp. 2218-2219 ◽  
Author(s):  
Stéphane Balayssac ◽  
Ivano Bertini ◽  
Moreno Lelli ◽  
Claudio Luchinat ◽  
Massimiliano Maletta
Keyword(s):  
Solid State ◽  
Solid State Nmr ◽  
Paramagnetic Ions ◽  
Structural Restraints

Selective measurements of long-range homonuclear J-couplings in solid-state NMR

2013 ◽  
Vol 231 ◽  
pp. 90-94 ◽  
Author(s):  
Pierre Thureau ◽  
Giulia Mollica ◽  
Fabio Ziarelli ◽  
Stéphane Viel
Keyword(s):  
Solid State ◽  
Long Range ◽  
Solid State Nmr

Proton Clouds to Measure Long-Range Contacts between Nonexchangeable Side Chain Protons in Solid-State NMR

2014 ◽  
Vol 136 (12) ◽  
pp. 4452-4455 ◽  
Author(s):  
Tessa Sinnige ◽  
Mark Daniëls ◽  
Marc Baldus ◽  
Markus Weingarth
Keyword(s):  
Solid State ◽  
Long Range ◽  
Solid State Nmr ◽  
Side Chain

scholarly journals Unraveling the complexity of protein backbone dynamics with combined 13C and 15N solid-state NMR relaxation measurements

2015 ◽  
Vol 17 (34) ◽  
pp. 21997-22008 ◽  
Author(s):  
Jonathan M. Lamley ◽  
Matthew J. Lougher ◽  
Hans Juergen Sass ◽  
Marco Rogowski ◽  
Stephan Grzesiek ◽  
...  
Keyword(s):  
Solid State ◽  
Magnetic Fields ◽  
Solid State Nmr ◽  
Nmr Relaxation ◽  
Backbone Dynamics ◽  
Relaxation Rates ◽  
Protein Backbone ◽  
Combined Analysis ◽  
Protein Backbone Dynamics ◽  
Relaxation Measurements

Combined analysis of 13C′ and 15N R1 and R1ρ relaxation rates measured at two magnetic fields leads to improved modeling of backbone dynamics in crystalline protein and provides unique insights into how the same motions contribute differently to relaxation rates in solution and solid state.

scholarly journals Homogeneity of doping with paramagnetic ions by NMR

2016 ◽  
Vol 18 (14) ◽  
pp. 9752-9757 ◽  
Author(s):  
Wenyu Li ◽  
Vinicius R. Celinski ◽  
Johannes Weber ◽  
Nathalie Kunkel ◽  
Holger Kohlmann ◽  
...  
Keyword(s):  
Solid State ◽  
Solid State Nmr ◽  
Paramagnetic Ions

Paramagnetic doping homogeneity can be elucidated by quantitative solid-state NMR experiments.

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