Proton Clouds to Measure Long-Range Contacts between Nonexchangeable Side Chain Protons in Solid-State NMR

2014 ◽  
Vol 136 (12) ◽  
pp. 4452-4455 ◽  
Author(s):  
Tessa Sinnige ◽  
Mark Daniëls ◽  
Marc Baldus ◽  
Markus Weingarth
Keyword(s):  
Solid State ◽  
Long Range ◽  
Solid State Nmr ◽  
Side Chain

Thermosetting Mechanism Study of Organosilicon Polymer Containing Carborane by Solid-State NMR Spectroscopy

1999 ◽  
Vol 576 ◽  
Author(s):  
H. Kimura ◽  
K. Okita ◽  
M. Ichitani ◽  
M. Yonezawa ◽  
T. Sugimoto
Keyword(s):  
Solid State ◽  
Solid State Nmr ◽  
Nmr Spectra ◽  
Main Chain ◽  
Addition Reaction ◽  
Side Chain ◽  
Mechanism Study ◽  
Nmr Method ◽  
Organosilicon Polymer ◽  
Thermal Stable

ABSTRACTThe thermosetting mechanism of an organosilicon polymer containing carborane has been studied utilizing the 13and 29Si solid-state NMR method. The polymer having C≡C bonds in the main chain and CH═CH2, Si-H bonds, and carborane in the bulky side chain, shows a very highly thermal stability in air by curing. From 13C and 29Si NMR spectra of the polymer, it was found that the intermolecular cross-linking reactions of the polymer was due to (1) the diene reaction between Ph-C≡C and C≡C and (2) the addition reaction between side chain terminal and Ph-C≡C and between CH═CH2 and Si–H, and a very highly thermal stable structure is formed.

scholarly journals Corrigendum: Solid-State NMR Measurements of Asymmetric Dipolar Couplings Provide Insight into Protein Side-Chain Motion

2012 ◽  
Vol 51 (40) ◽  
pp. 9959-9959
Author(s):  
Paul Schanda ◽  
Matthias Huber ◽  
Jérôme Boisbouvier ◽  
Beat H. Meier ◽  
Matthias Ernst
Keyword(s):  
Solid State ◽  
Solid State Nmr ◽  
Dipolar Couplings ◽  
Side Chain ◽  
Side Chain Motion ◽  
Insight Into

Morphology and side-chain dynamics in hydrated hard α-keratin fibres by 1H solid-state NMR

2009 ◽  
Vol 480 (4-6) ◽  
pp. 300-304 ◽  
Author(s):  
Claudiu Melian ◽  
Dan E. Demco ◽  
Monica Istrate ◽  
Andreea Balaceanu ◽  
Dumitrita Moldovan ◽  
...  
Keyword(s):  
Solid State ◽  
Solid State Nmr ◽  
Side Chain ◽  
Chain Dynamics ◽  
Side Chain Dynamics ◽  
Keratin Fibres

scholarly journals Side Chain and Backbone Dynamics of Phospholamban in Phospholipid Bilayers Utilizing2H and15N Solid-State NMR Spectroscopy†

Biochemistry ◽  
2007 ◽  
Vol 46 (42) ◽  
pp. 11695-11706 ◽  
Author(s):  
Shadi Abu-Baker ◽  
Jun-Xia Lu ◽  
Shidong Chu ◽  
Clarke C. Brinn ◽  
Christopher A. Makaroff ◽  
...  
Keyword(s):  
Solid State ◽  
Nmr Spectroscopy ◽  
Solid State Nmr ◽  
Phospholipid Bilayers ◽  
Backbone Dynamics ◽  
Side Chain ◽  
Solid State Nmr Spectroscopy

Solid-State NMR Measurements of Asymmetric Dipolar Couplings Provide Insight into Protein Side-Chain Motion

2011 ◽  
Vol 50 (46) ◽  
pp. 11005-11009 ◽  
Author(s):  
Paul Schanda ◽  
Matthias Huber ◽  
Jérôme Boisbouvier ◽  
Beat H. Meier ◽  
Matthias Ernst
Keyword(s):  
Solid State ◽  
Solid State Nmr ◽  
Dipolar Couplings ◽  
Side Chain ◽  
Side Chain Motion ◽  
Insight Into

scholarly journals An Efficient Labelling Approach to Harness Backbone and Side-Chain Protons in1H-Detected Solid-State NMR Spectroscopy

2015 ◽  
Vol 54 (52) ◽  
pp. 15799-15803 ◽  
Author(s):  
Deni Mance ◽  
Tessa Sinnige ◽  
Mohammed Kaplan ◽  
Siddarth Narasimhan ◽  
Mark Daniëls ◽  
...  
Keyword(s):  
Solid State ◽  
Nmr Spectroscopy ◽  
Solid State Nmr ◽  
Side Chain ◽  
Solid State Nmr Spectroscopy
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