Solution-State Dynamic Nuclear Polarization at High Magnetic Field

2002 ◽  
Vol 124 (30) ◽  
pp. 8808-8809 ◽  
Author(s):  
Nikolaus M. Loening ◽  
Melanie Rosay ◽  
Volker Weis ◽  
Robert G. Griffin
Keyword(s):  
Magnetic Field ◽  
High Magnetic Field ◽  
Dynamic Nuclear Polarization ◽  
Nuclear Polarization ◽  
Solution State ◽  
State Dynamic

Large volume liquid state scalar Overhauser dynamic nuclear polarization at high magnetic field

2019 ◽  
Vol 21 (38) ◽  
pp. 21200-21204 ◽  
Author(s):  
Thierry Dubroca ◽  
Sungsool Wi ◽  
Johan van Tol ◽  
Lucio Frydman ◽  
Stephen Hill
Keyword(s):  
Magnetic Field ◽  
Nuclear Magnetic Resonance ◽  
Magnetic Resonance ◽  
Magnetic Fields ◽  
High Magnetic Field ◽  
Dynamic Nuclear Polarization ◽  
Large Volume ◽  
Liquid State ◽  
Nuclear Polarization ◽  
High Magnetic Fields

Dynamic Nuclear Polarization (DNP) can increase the sensitivity of Nuclear Magnetic Resonance (NMR), but it is challenging in the liquid state at high magnetic fields.

High-field liquid state NMR hyperpolarization: a combined DNP/NMRD approach

2014 ◽  
Vol 16 (35) ◽  
pp. 18781-18787 ◽  
Author(s):  
Petr Neugebauer ◽  
Jan G. Krummenacker ◽  
Vasyl P. Denysenkov ◽  
Christina Helmling ◽  
Claudio Luchinat ◽  
...  
Keyword(s):  
Magnetic Field ◽  
High Magnetic Field ◽  
Dynamic Nuclear Polarization ◽  
Liquid State ◽  
High Field ◽  
Nuclear Polarization ◽  
Nmr Relaxation ◽  
Relaxation Dispersion ◽  
Liquid Solutions ◽  
High Fields

Dynamic nuclear polarization and NMR relaxation dispersion measurements have been performed on liquid solutions of TEMPOL radicals in solvents with different viscosities at a high magnetic field of 9.2 T. The results indicate that fast dynamics significantly contribute to DNP enhancements at high fields.

Dynamic Nuclear Polarization-Enhanced Biomolecular NMR Spectroscopy at High Magnetic Field with Fast Magic-Angle Spinning

2018 ◽  
Vol 130 (25) ◽  
pp. 7580-7584 ◽  
Author(s):  
Kristaps Jaudzems ◽  
Andrea Bertarello ◽  
Sachin R. Chaudhari ◽  
Andrea Pica ◽  
Diane Cala-De Paepe ◽  
...  
Keyword(s):  
Magnetic Field ◽  
Nmr Spectroscopy ◽  
High Magnetic Field ◽  
Dynamic Nuclear Polarization ◽  
Nuclear Polarization ◽  
Magic Angle Spinning ◽  
Magic Angle ◽  
Biomolecular Nmr ◽  
Angle Spinning ◽  
Fast Magic Angle Spinning

Portable X-band system for solution state dynamic nuclear polarization

2008 ◽  
Vol 191 (2) ◽  
pp. 273-281 ◽  
Author(s):  
Brandon D. Armstrong ◽  
Mark D. Lingwood ◽  
Evan R. McCarney ◽  
Elliott R. Brown ◽  
Peter Blümler ◽  
...  
Keyword(s):  
Dynamic Nuclear Polarization ◽  
Nuclear Polarization ◽  
Band System ◽  
Solution State ◽  
State Dynamic ◽  
X Band

scholarly journals Optimization and prediction of the electron–nuclear dipolar and scalar interaction in1H and13C liquid state dynamic nuclear polarization

2015 ◽  
Vol 6 (11) ◽  
pp. 6482-6495 ◽  
Author(s):  
X. Wang ◽  
W. C. Isley III ◽  
S. I. Salido ◽  
Z. Sun ◽  
L. Song ◽  
...  
Keyword(s):  
Intermolecular Interactions ◽  
Dynamic Nuclear Polarization ◽  
Liquid State ◽  
Nuclear Polarization ◽  
Scalar Interaction ◽  
Solution State ◽  
State Dynamic

Solution-state dynamic nuclear polarization (DNP) is a powerful tool for hyperpolarization and the study of intermolecular interactions in solution.

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