Straightforward Method for Synthesis of Highly Alkyl-Substituted Naphthacene and Pentacene Derivatives by Homologation

2000 ◽  
Vol 122 (51) ◽  
pp. 12876-12877 ◽  
Author(s):  
Tamotsu Takahashi ◽  
Masanori Kitamura ◽  
Baojian Shen ◽  
Kiyohiko Nakajima
Keyword(s):  
Straightforward Method ◽  
Pentacene Derivatives

ChemInform Abstract: Straightforward Method for Synthesis of Highly Alkyl-Substituted Naphthacene and Pentacene Derivatives by Homologation.

ChemInform ◽  
2001 ◽  
Vol 32 (16) ◽  
pp. no-no
Author(s):  
Tamotsu Takahashi ◽  
Masanori Kitamura ◽  
Baojian Shen ◽  
Kiyohiko Nakajima
Keyword(s):  
Straightforward Method ◽  
Pentacene Derivatives

Direct Plan View FIB Liftout for Near-Surface Defect Analysis in TEM

2013 ◽  
Author(s):  
Max L. Lifson ◽  
Carla M. Chapman ◽  
D. Philip Pokrinchak ◽  
Phyllis J. Campbell ◽  
Greg S. Chrisman ◽  
...  
Keyword(s):  
Failure Analysis ◽  
Silicon Germanium ◽  
Focused Ion Beam ◽  
Surface Defects ◽  
Ion Beam ◽  
Misfit Dislocations ◽  
Tem Analysis ◽  
Plan View ◽  
Near Surface ◽  
Straightforward Method

Abstract Plan view TEM imaging is a powerful technique for failure analysis and semiconductor process characterization. Sample preparation for near-surface defects requires additional care, as the surface of the sample needs to be protected to avoid unintentionally induced damage. This paper demonstrates a straightforward method to create plan view samples in a dual beam focused ion beam (FIB) for TEM studies of near-surface defects, such as misfit dislocations in heteroepitaxial growths. Results show that misfit dislocations are easily imaged in bright-field TEM and STEM for silicon-germanium epitaxial growth. Since FIB tools are ubiquitous in semiconductor failure analysis labs today, the plan view method presented provides a quick to implement, fast, consistent, and straightforward method of generating samples for TEM analysis. While this technique has been optimized for near-surface defects, it can be used with any application requiring plan view TEM analysis.

scholarly journals Co-Translational Insertion of Aquaporins into Liposome for Functional Analysis via an E. coli Based Cell-Free Protein Synthesis System

Cells ◽  
2019 ◽  
Vol 8 (11) ◽  
pp. 1325 ◽  
Author(s):  
Ke Yue ◽  
Tran Nam Trung ◽  
Yiyong Zhu ◽  
Ralf Kaldenhoff ◽  
Lei Kai
Keyword(s):  
Functional Analysis ◽  
Membrane Proteins ◽  
Fluorescent Protein ◽  
Water Channel ◽  
New Approach ◽  
E Coli ◽  
Straightforward Method ◽  
Lipid Environment ◽  
Green Fluorescent ◽  
Eukaryotic Organisms

Aquaporins are important and well-studied water channel membrane proteins. However, being membrane proteins, sample preparation for functional analysis is tedious and time-consuming. In this paper, we report a new approach for the co-translational insertion of two aquaporins from Escherichia coli and Nicotiana tabacum using the CFPS system. This was done in the presence of liposomes with a modified procedure to form homogenous proteo-liposomes suitable for functional analysis of water permeability using stopped-flow spectrophotometry. Two model aquaporins, AqpZ and NtPIP2;1, were successfully incorporated into the liposome in their active forms. Shifted green fluorescent protein was fused to the C-terminal part of AqpZ to monitor its insertion and status in the lipid environment. This new fast approach offers a fast and straightforward method for the functional analysis of aquaporins in both prokaryotic and eukaryotic organisms.

scholarly journals A Versatile Approach to Access Trimetallic Complexes Based on Trisphosphinite Ligands

Molecules ◽  
2020 ◽  
Vol 25 (3) ◽  
pp. 593
Author(s):  
Juan Miranda-Pizarro ◽  
Macarena G. Alférez ◽  
M. Dolores Fernández-Martínez ◽  
Eleuterio Álvarez ◽  
Celia Maya ◽  
...  
Keyword(s):  
Coordination Chemistry ◽  
Late Transition Metal ◽  
X Ray Diffraction ◽  
X Ray ◽  
Full Characterization ◽  
Metal Precursors ◽  
Straightforward Method ◽  
One Step ◽  
Late Transition

A straightforward method for the preparation of trisphosphinite ligands in one step, using only commercially available reagents (1,1,1-tris(4-hydroxyphenyl)ethane and chlorophosphines) is described. We have made use of this approach to prepare a small family of four trisphosphinite ligands of formula [CH3C{(C6H4OR2)3], where R stands for Ph (1a), Xyl (1b, Xyl = 2,6-Me2-C6H3), iPr (1c), and Cy (1d). These polyfunctional phosphinites allowed us to investigate their coordination chemistry towards a range of late transition metal precursors. As such, we report here the isolation and full characterization of a number of Au(I), Ag(I), Cu(I), Ir(III), Rh(III) and Ru(II) homotrimetallic complexes, including the structural characterization by X-ray diffraction studies of six of these compounds. We have observed that the flexibility of these trisphosphinites enables a variety of conformations for the different trimetallic species.

scholarly journals The feasibility of measuring the nuclear reaction cross sections at energies of several KeV in a target under laser compression

1987 ◽  
Vol 5 (2) ◽  
pp. 399-404 ◽  
Author(s):  
V. I. Kukulin ◽  
V. M. Krasnopol'sky ◽  
V. T. Voronchev
Keyword(s):  
Nuclear Reaction ◽  
Cross Sections ◽  
Nuclear Reactions ◽  
Velocity Distribution Function ◽  
Reaction Cross ◽  
Straightforward Method ◽  
Energy Behaviour ◽  
Low Energies ◽  
Ion Velocity Distribution Function ◽  
Reaction Cross Sections

The work proposes a straightforward method for determining the nuclear reaction cross sections at extremely low energies (E ≃ 1–100 keV) on the basis of the measurements of the relative yield of fast particles which are products of the nuclear reactions in a target under laser compression. On the other hand, the proposed method makes it possible to find the averaged form of the ion velocity distribution function if the low-energy behaviour of the respective cross sections is known.

Qualifications of Adhesives for Marine Composite-to-Steel Bonded Applications

2009 ◽  
Vol 25 (04) ◽  
pp. 198-205
Author(s):  
George W. Ritter ◽  
David R. Speth ◽  
Yu Ping Yang
Keyword(s):  
Mechanical Property ◽  
Structural Integrity ◽  
Adhesively Bonded ◽  
Load Bearing Capacity ◽  
Property Evaluation ◽  
Marine Industry ◽  
Straightforward Method ◽  
Bonded Composite ◽  
Steel Joints ◽  
Marine Composite

This paper describes a straightforward method for the design and certification of adhesively bonded composite to steel joints for the marine industry. Normally, certification is based on documented service at sea. Since these joints have not been previously deployed at sea, no data on their performance exist. Using an integrated combination of mechanical property evaluation and finite element modeling, the load- bearing capacity of a joint can be compared with the anticipated seaway loads. Calculated factors of safety for the sandwich design used here show that the joint has adequate strength to maintain structural integrity even after severe environmental exposure.

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