Colorimetric Determination of Low Concentrations of Sodium Nitrate in Sodium Nitrite

1942 ◽  
Vol 14 (5) ◽  
pp. 420-422 ◽  
Author(s):  
William Seaman ◽  
A Norton ◽  
W Mader ◽  
J Hugonet
1955 ◽  
Vol 27 (12) ◽  
pp. 2012-2014 ◽  
Author(s):  
C. Stafford ◽  
J. E. Puckett ◽  
M. D. Grimes ◽  
B. J. Heinrich

1987 ◽  
Vol 70 (3) ◽  
pp. 568-571 ◽  
Author(s):  
Mohamed E El-Sadek ◽  
Hisham E Abdel Latef ◽  
Afaf A Aboul Khier

Abstract A colorimetric method is proposed for determination of terbutaline sulfate, orciprenaline sulfate, and their dosage forms. The suggested method depends on nitrosation of the 2 drugs by using sodium nitrite and hydrochloric acid. Addition of sodium hydroxide increases the intensity of the color developed. The difference between absorption values measured in acid and alkaline media is taken as a measure of concentration. Variables were carefully studied and optimized. Results for both compounds adhered to Beer's law over the range 2- 28 μg/mL. The method has proved to be accurate and precise for analysis of pharmaceutical dosage forms.


1963 ◽  
Vol 41 (3) ◽  
pp. 667-670 ◽  
Author(s):  
Frances E. Piercy ◽  
D. E. Ryan

5-(p-Dimethylaminobenzylidene)-rhodanine is used to determine 0.5 to 6 p.p.m. of platinum colorimetrically, after reduction of platinum IV with ascorbic acid. Platinum can be determined in the presence of a 10-fold excess of palladium; low concentrations of the other platinum metals, except rhodium, do not seriously interfere.


1955 ◽  
Vol 27 (9) ◽  
pp. 1401-1404 ◽  
Author(s):  
L. S. Buchoff ◽  
N. M Ingber ◽  
J. H. Brady

Author(s):  
MURALI D ◽  
PURNA CHANDRA RAO G

Objective: The present study represents the development of two spectrophotometric methods for the determination of carisoprodol (CCP) in pure and formulations using ferric chloride, o-phenanthroline, and p-nitroaniline (PNA), sodium nitrate as analytical reagents. Methods: The proposed spectrophotometric methods were developed based on oxidation of Fe3+ by CCP, and then, the resultant product was reacted with o-phenanthroline in acidic condition forms an orange-colored complex and diazotization of PNA followed by coupling with CCP in an alkaline medium forms yellow-colored complex. Results: Under the optimized conditions, the absorbance of CCP concentration obeyed the Beer’s law in the ranges of 10–60 μg/mL with good correlation coefficient values of 0.9992 and 0.9990 with the limit of detection values of 1.286 and 2.408 μg/mL, respectively. Conclusion: The proposed methods were successfully applied for the determination of CCP in pure and in their formulations.


Sign in / Sign up

Export Citation Format

Share Document