scholarly journals Synthesis and Characterization of Biobased Polyesters with Tunable Tg by ROCOP of Beta-Elemene Oxides and Phthalic Anhydride

2021 ◽  
Vol 9 (7) ◽  
pp. 2619-2625
Author(s):  
Francesco Della Monica ◽  
Arjan W. Kleij
Keyword(s):  
Phthalic Anhydride ◽  
Synthesis And Characterization

Synthesis and Characterization of Alkyd Resin Based on Soybean Oil Polyols

2011 ◽  
Vol 239-242 ◽  
pp. 1721-1724 ◽  
Author(s):  
Xiao Qing Zheng ◽  
Li Ting Yang ◽  
Kun Peng Wang
Keyword(s):  
Maleic Anhydride ◽  
Soybean Oil ◽  
Phthalic Anhydride ◽  
Alkyd Resin ◽  
Ring Opening ◽  
Molar Ratio ◽  
Synthesis And Characterization ◽  
Hydroxyl Value

Soybean oil-based alkyd resin was prepared using soy-based polyol, maleic anhydride and phthalic anhydride. The soy-based polyol was obtained through the epoxidization of soybean oil, followed by ring-opening with methanol and, the hydroxyl values of soybean oil-based polyols used in this reaction is 169.93 mgKOH/g. In the reactions of soy-based polyol, maleic anhydride and phthalic anhydride, the molar ratio of hydroxyl value is equal to carboxyl value and the molar ratio of maleic anhydride to phthalic anhydride is 2:1, 1:1 and 1:2, respectively. 1% hydroquinone based on total reactants was used as inhibitor of polymerization, 1% dibutyltin oxide was used as catalyst.

scholarly journals Synthesis and Characterization of Pentaerythritol Phthalic Anhydride Resin from Soybean Oil

2018 ◽  
Vol 30 (3) ◽  
pp. 572-574
Author(s):  
Ayyaz Muhammad ◽  
Shafqat Abbas ◽  
Amir Shafeeq ◽  
Hamad Al-Turaif ◽  
Aqeel Ahmed Taimoor ◽  
...  
Keyword(s):  
Soybean Oil ◽  
Phthalic Anhydride ◽  
Synthesis And Characterization

Synthesis and characterization of chitosan-G-phthalic anhydride with different drugs

2020 ◽  
Author(s):  
Sana Hitur Awad ◽  
Selvana Adwar Yousif ◽  
Wasan Abdul Razzaq Mahmood ◽  
Tamador Ali Mahmood
Keyword(s):  
Phthalic Anhydride ◽  
Synthesis And Characterization

Synthesis and Characterization of some 2-Azetidinones Derived from 3-Nitro Phthalic Anhydride and Evaluation their Biological against Bacteria and Fungi

2020 ◽  
Vol 1002 ◽  
pp. 360-368
Author(s):  
Ahmood Kh. Jebur Al-Joubory ◽  
Rabiha Hameed Saleh ◽  
Omar Abdulrahman Mohammed
Keyword(s):  
Phthalic Anhydride ◽  
Acetyl Chloride ◽  
Bacterial Activity ◽  
Synthesis And Characterization ◽  
Inhibition Activity ◽  
Gram Negative ◽  
H Nmr ◽  
Bacteria And Fungi ◽  
High Inhibition

Reaction of the moiety 3-nitro phthalic anhydride with p- Phenylene diamine in (40 ml) acetic acid to give compound (p-amino phenyl)-3-nitro phthalimide (A1).Which that react with different aromatic aldehyde in ethanol absolute to give compounds hydrazone (A2-A5), then react this compounds (A2-A5) with chloro acetyl chloride in presence of TEA by using DMF as solvent to obtain 2-azetidinones (A6-A9).The compounds of all the newly synthesized structures were confirmed by and ,IR, 1H NMR as well as melting point. Some of these new structures showed antimicrobial activity (A7-A8) and anti-bacterial activity (A7-A8).Antibacterial activity of some prepared compounds against two types of bacteria: Staphylococcus aureus (Gram positive) and E.coli (Gram negative). Some the compounds showed high inhibition activity against bacteria and two fungi (Candida albicans) and (Candida tropicalis.).

scholarly journals Synthesis and Characterization of Some New Monemer and Polymers Containing Hetero Cyclic Rings With Study of Their Physical Properties.

2016 ◽  
Vol 13 (2) ◽  
pp. 172-180
Author(s):  
Baghdad Science Journal
Keyword(s):  
Acetic Acid ◽  
Schiff Base ◽  
Maleic Anhydride ◽  
Phthalic Anhydride ◽  
Sodium Azide ◽  
Heterocyclic Compounds ◽  
Synthesis And Characterization ◽  
X Ray ◽  
Ft Ir

Number of new polyester and polyamide are prepared as derivatives from 5,5`-(1,4-phenylene)-bis-(1,3,4-thiadiazole-2-amine) [C1], three series of heterocyclic compounds were synthesized.The first series includes the Schiff base [C2] prepared from the reaction between compound [C1] with p-hydroxy benzaldehyde in presence of acetic acid and absolute ethanol , then these derivatives have reaction with maleic anhydride , phthalic anhydride and sodium azide, respectively to obtain the compounds [C3-5] contaning (oxazepine and tetrazole) rings.The third series of compounds [C1-5] has transformed to their polymers [C6-15] by reaction with adipoyl chloride and glutroyl chloride , respectively. The reaction was followed by T.L.C and identified by FT-IR , 1H-NMR ,C.H.N analysis , softening point , viscosity, TGA , DSC and X-ray.

scholarly journals Efficient Synthesis and Characterization of 4- (1, 3-Dioxoisoindolin-2yl) Benzaldehyde

2017 ◽  
Vol 6 (2) ◽  
pp. 31
Author(s):  
Sharad S. Sankhe ◽  
Nitesh R. Chindarkar
Keyword(s):  
1H Nmr ◽  
Phthalic Anhydride ◽  
Synthesis And Characterization ◽  
Efficient Synthesis

<em>The titled 4-(1,3-dioxo-2,3-dihydro-1H-inden-2-yl)benzaldehyde has been synthesized from phthalic anhydride and p-toluidene followed by use of H<sub>2</sub>O<sub>2</sub> in ethanol. Compounds characterized on the basis of 1H-NMR. </em>

Sign in / Sign up

Export Citation Format

Share Document