Insight into Fast Nucleation and Growth of Zeolitic Imidazolate Framework-71 by In Situ Static Light Scattering at Variable Temperature and Kinetic Modeling

2018 ◽  
Vol 18 (8) ◽  
pp. 4653-4661 ◽  
Author(s):  
Sanjib Saha ◽  
Michael Wiebcke ◽  
Klaus Huber
Keyword(s):  
Light Scattering ◽  
Kinetic Modeling ◽  
Variable Temperature ◽  
Nucleation And Growth ◽  
Static Light Scattering ◽  
Zeolitic Imidazolate Framework ◽  
Insight Into

Controlling Zeolitic Imidazolate Framework Nano- and Microcrystal Formation: Insight into Crystal Growth by Time-Resolved In Situ Static Light Scattering

2011 ◽  
Vol 23 (8) ◽  
pp. 2130-2141 ◽  
Author(s):  
Janosch Cravillon ◽  
Roman Nayuk ◽  
Sergej Springer ◽  
Armin Feldhoff ◽  
Klaus Huber ◽  
...  
Keyword(s):  
Crystal Growth ◽  
Light Scattering ◽  
Static Light Scattering ◽  
Zeolitic Imidazolate Framework ◽  
Time Resolved ◽  
Insight Into

Insight into Fast Nucleation and Growth of Zeolitic Imidazolate Framework-71 by In Situ Time-Resolved Light and X-ray Scattering Experiments

2016 ◽  
Vol 16 (4) ◽  
pp. 2002-2010 ◽  
Author(s):  
Sanjib Saha ◽  
Sergej Springer ◽  
Maria E. Schweinefuß ◽  
Diego Pontoni ◽  
Michael Wiebcke ◽  
...  
Keyword(s):  
Nucleation And Growth ◽  
Zeolitic Imidazolate Framework ◽  
Time Resolved ◽  
X Ray ◽  
X Ray Scattering ◽  
Insight Into ◽  
Ray Scattering

scholarly journals Nucleation and Growth of Supported Metal Clusters at Defect Sites on Mgo and NaCl (001) Surfaces: The Cases of Pd and Ag

1999 ◽  
Vol 570 ◽  
Author(s):  
J. A. Venables ◽  
G. Haas ◽  
H. Brune ◽  
J.H. Harding
Keyword(s):  
Deposition Temperature ◽  
Metal Clusters ◽  
Variable Temperature ◽  
Nucleation And Growth ◽  
Force Microscopy ◽  
Atomic Force ◽  
Defect Sites ◽  
Wide Range ◽  
Adsorption Surface

ABSTRACTNucleation and growth of metal clusters at defect sites is discussed in terms of rate equation models, which are applied to the cases of Pd and Ag on MgO(001) and NaCl(001) surfaces. Pd/MgO has been studied experimentally by variable temperature atomic force microscopy (AFM). The island density of Pd on Ar-cleaved surfaces was determined in-situ by AFM for a wide range of deposition temperature and flux, and stays constant over a remarkably wide range of parameters; for a particular flux, this plateau extends from 200 K ≤ T ≤ 600 K, but at higher temperatures the density decreases. The range of energies for defect trapping, adsorption, surface diffusion and pair binding are deduced, and compared with earlier data for Ag on NaCl, and with recent calculations for these metals on both NaCl and MgO

In-Situ Light-Scattering Measurements During the CVD of Polycrystalline Silicon Carbide

1991 ◽  
Vol 250 ◽  
Author(s):  
Brian W. Sheldon ◽  
Philip A. Reichle ◽  
Theodore M. Besmann
Keyword(s):  
Silicon Carbide ◽  
Light Scattering ◽  
Polycrystalline Silicon ◽  
Chemical Vapor ◽  
Nucleation And Growth ◽  
Scattering Spectrum ◽  
Angular Scattering ◽  
Polycrystalline Silicon Carbide ◽  
Scattering Spectra

AbstractLight-scattering was used to monitor the chemical vapor deposition of silicon carbide from methyltrichlorosilane. The nucleation and growth of the SiC features caused changes in the surface topography that altered the angular scattering spectrum that was generated with a He-Ne laser. These scattering spectra were then analyzed to obtain information about the nucleation and growth processes that are occurring.

In situ observation of silicalite nucleation and growth: A light-scattering study

Zeolites ◽  
1994 ◽  
Vol 14 (3) ◽  
pp. 162-168 ◽  
Author(s):  
T.A.M. Twomey ◽  
M. Mackay ◽  
H.P.C.E. Kuipers ◽  
R.W. Thompson
Keyword(s):  
Light Scattering ◽  
Nucleation And Growth ◽  
In Situ Observation ◽  
Scattering Study

Small-angle static light scattering of concentrated silica suspensions during in situ destabilization

2004 ◽  
Vol 271 (2) ◽  
pp. 388-399 ◽  
Author(s):  
Hans M. Wyss ◽  
Josef Innerlohinger ◽  
Lorenz P. Meier ◽  
Ludwig J. Gauckler ◽  
Otto Glatter
Keyword(s):  
Light Scattering ◽  
Small Angle ◽  
Static Light Scattering ◽  
Silica Suspensions

scholarly journals Colloidal nanoparticle size control: experimental and kinetic modeling investigation of the ligand–metal binding role in controlling the nucleation and growth kinetics

Nanoscale ◽  
2017 ◽  
Vol 9 (36) ◽  
pp. 13772-13785 ◽  
Author(s):  
Saeed Mozaffari ◽  
Wenhui Li ◽  
Coogan Thompson ◽  
Sergei Ivanov ◽  
Soenke Seifert ◽  
...  
Keyword(s):  
Kinetic Model ◽  
Kinetic Modeling ◽  
Growth Kinetics ◽  
Metal Binding ◽  
Size Control ◽  
Pd Nanoparticles ◽  
Nucleation And Growth ◽  
Nanoparticle Size

In situ SAXS and ligand-based kinetic model are used for predictive synthesis of ligand-protected Pd nanoparticles in different solvents.

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