Mass Spectrometer Used as Detector and Analyzer for Effluent Emerging from a Capillary Gas Liquid Chromatography Column.

1965 ◽  
Vol 37 (3) ◽  
pp. 435-436 ◽  
Author(s):  
Ragnar. Ryhage ◽  
Sten. Wikstrom ◽  
G. R. Waller
Author(s):  
A.A. Parshutina ◽  
◽  
A.A. Solovyova ◽  
L.P. Satyukova ◽  
E.G. Shubina ◽  
...  

The article shows the importance of the study of feed for broiler chickens on the content of organochlorine pesticides. These substances in significant concentrations can disrupt the development of birds and cause mass poisoning. The study of formula feed for broiler chickens «prestart» and «start» by two methodswas conducted: a certified method for the determination of organochlorine pesticides in feed and formula feed (thin layer chromatography) and a method for detecting pesticides not certified for feed (gas-liquid chromatography with mass spectrometer detector). During the experiment, the presence of organochlorine pesticides in several formulafeed samples was revealed.


1981 ◽  
Vol 64 (4) ◽  
pp. 884-888
Author(s):  
Charles C Clark

Abstract Gas-liquid chromatography (GLC) using a mass spectrometer (MS) as a detector is used for the quantitative determination of cocaine HCl in powders. After the sample is dissolved in methanol containing deuterated cocaine HCl internal standard, an aliquot is injected into the GLC-MS system with the mass spectrometer operating in the scan mode. The cocaine HCl concentration is calculated from the 303/308 m/e ratio. The procedure has a relative deviation of approximately 2.3% and is applicable to samples containing a wide variety of diluents and adulterants.


1974 ◽  
Vol 24 (11) ◽  
pp. 645-654 ◽  
Author(s):  
F. Alan Barbour ◽  
Richard V. Barbour ◽  
J. Claine Peterson

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